• 대한금속재료학회지
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• 제47권12호
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• pp.811-818
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• 2009

In order to meet increasingly complex and rigorous technical specifications, extensive effort has been devoted to fabricate clad materials with multi-layered metal plates. In this study, novel stainless steel/aluminum/copper (STS/Al/Cu) three-ply clad materials were fabricated by a hot rolling process for cookware applications. The effect of the testing temperature on the mechanical properties of the clad materials and on each component metal was investigated during the tensile tests. The interface properties of the clad materials were also examined by optical microscopy (OM) and an electron probe micro-analyzer (EPMA). The best mechanical and interfacial properties for a warm working process were found in a sample annealed at a temperature of $300^{\circ}C$. For the sample annealed at $400^{\circ}C$, the results of the tensile test indicated that interface delamination occurred only in the region of the Al/Cu interfaces. This was due to the formation of the thick and brittle intermetallic compound of $Al_2Cu$ in the Al/Cu interface. In contrast, no interface delamination was observed in the STS/Al interface, most likely due to its strong bond strength.

• 대한금속재료학회지
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• 제48권8호
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• pp.691-698
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• 2010

A study has been carried out to evaluate the interaction behavior between a lanthanide element and clad material in order to analyze the effect of the lanthanide element on the fuel cladding chemical interaction (FCCI). A diffusion couple test between Misch metal (70Ce-30La) and ferritic-martensitic steel (Gr.92) was performed at $660^{\circ}C$, followed by a microstructural analysis of the coupled sample. The results showed that Ce in the Misch metal, rather than La, reacted with the ferritic-martensitic steel (FMS) to form an interaction layer that penetrated the clad thickness. Fe diffused outside the clad interface to form an $Fe_2Ce$ compound, leaving a depletion of Fe caused by excess diffusion as well as by the formation of Cr-rich precipitation inside the interaction layer. The rate of growth followed the cubic rate law, which indicated that Fe depletion was caused by the diffusion of Fe and that the associated Cr-rich phase formation controlled the whole diffusion process.

• 대한기계학회논문집A
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• 제41권4호
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• pp.307-312
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• 2017

레이저 클래딩은 아크 용접 및 용사와 같은 기존 클래딩 기술보다 우수한 장점을 가진다. 레이저 클래딩으로 형성한 클래드 층의 희석률은 낮으며 모재와의 결합력이 우수하고 결함이 거의 존재하지 않는다. 이러한 특징을 가진 레이저 클래딩을 실제 선박용 배기밸브에 적용하기에 위해 지난 제1보의 논문에서 조사한 공정변수에 따른 1 패스 클래드 층의 특성을 통해 넓은 면적에 클래딩 시 1 패스 클래드 층의 중첩이 필수적이라는 것을 알 수 있었다. 따라서 본 논문에서는 중첩률에 따른 멀티패스 클래드 층의 형상 차이를 비교하고 일정 중첩률 조건에서 EDS 및 EPMA를 통해 합금 성분 분포를 파악하였다. 실험결과, 중첩률이 증가할수록 클래드 층의 길이가 감소하고 높이가 증가하였으며 동일한 조건의 1 패스 클래드 층보다 높이가 상승하였다. 성분 분석을 통해 모재 희석이 많이 발생한 첫 번째 클래드 층에서 Fe이 높게 측정되었으나 나머지 영역에서는 희석이 감소하여 Co가 증가하고 Fe이 감소하였으며 균일한 성분 분포가 관찰되었다.

• 대한금속재료학회지
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• 제50권4호
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• pp.316-323
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• 2012

The aim of this study is to investigate the effect of post heat treatment on bonding properties of roll cladded Ti/MS/Ti materials. First grade Ti sheets and SPCC mild steel sheets were prepared and then Ti/MS/Ti clad materials were fabricated by a cold rolling and post heat treatment process. Microstructure and point analysis of the Ti/MS interfaces were performed using the SEM and EDX Analyser. Diffusion bonding was observed at the interfaces of Ti/MS. The thickness of the diffusion layer increased with post heat treatment temperature and the diffusion layer was verified as having $({\epsilon}+{\zeta})+({\zeta}+{\beta}-Ti)$ intermetallic compounds at $700^{\circ}C$ and an $({\zeta}+{\beta}-Ti)$ intermetallic compound at $800^{\circ}C$, respectively. The micro Knoop hardness of mild steel decreased with post heat treatment temperature; however, those of Ti decreased at a range of $500{\sim}600^{\circ}C$ and showed a uniform value until $800^{\circ}C$ and then increased rapidly up to $900^{\circ}C$. The micro Knoop hardness value of the diffusion layer increased up to $700^{\circ}C$ and then saturated with post heat treatment. A T-type peel test was used to estimate the bonding forces of Ti/Mild steel interfaces. The bonding forces decreased up to $800^{\circ}C$ and then increased slightly with post heat treatment. The optimized temperature ranges for post heat treatment were $500{\sim}600^{\circ}C$ to obtain the proper formability for an additional plastic deformation process.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2006년도 춘계학술발표회 초록집
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• pp.49-49
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• 2006

• Nuclear Engineering and Technology
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• 제50권5호
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• pp.724-730
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• 2018

Chromium and chromium nitride were selected as potential barriers to prevent fuel-clad chemical interaction (FCCI) between the cladding and the fuel material. In this study, ferritic/martensitic HT-9 steel and misch metal were used to simulate the reaction between the cladding and fuel fission product, respectively. Radio frequency magnetron sputtering was used to deposit Cr and CrN films onto the cladding, and the gas flow rates of argon and nitrogen were fixed at certain values for each sample to control the deposition rate and the crystal structure of the films. The samples were heated for 24 h at 933 K through the diffusion couple test, and considerable amount of interdiffusion (max. thickness: $550{\mu}m$) occurred at the interface between HT-9 and misch metal when the argon and nitrogen were used individually. The elemental contents of misch metal were detected at the HT-9 through energy dispersive X-ray spectroscopy due to the interdiffusion. However, the specimens that were sputtered by mixed gases (Ar and $N_2$) exhibited excellent resistance to FCCI. The thickness of these CrN films were only $4{\mu}m$, but these films effectively prevented the FCCI due to their high adhesion strength (frictional force ${\geq}1,200{\mu}m$) and dense columnar microstructures.

• Journal of Welding and Joining
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• 제17권4호
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• pp.46-52
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• 1999

Some of the pressurized reactor pressure vessels used in many chemical plants are made of low alloy carbon steel plates internally clad with an austenitic stainless steel for improved anti-corrosion properties. In this study, metallurgic structure of the weld interface of A 387 Grade12Class1 low alloy carbon steel claded with A182-F321 austenitic stainless steel after thermal exposure simulation heat treatment was investigated to display a characteristic behavior of dissimilar metal weld interface with thermal exposure during service at high temperature and pressure. EPMA, STEM, vickers-hardness test were performed and the results were correlated with the microstructure. To estimate the depth of the carburized/decarburized bands quantitatively, a model for carbon diffusion was proposed. The validity of the proposed theoretical relationships was confirmed by the directly measured data from the welded parts failed during service.

• 마이크로전자및패키징학회지
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• 제22권3호
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• pp.67-72
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• 2015

히트 싱크용 소재에 응용할 목적으로 단층금속과 2층금속 클래드메탈에 대해 열전도 특성에 대한 연구를 하였다. 단층시편으로는 스테인리스강과 알루미늄을 선택하였으며, 2층 금속으로는 스테인리스강과 알루미늄을 압연해서 제조한 클래드메탈을 사용하였다. 열전도도는 섬광법으로 측정한 열확산계수와 비열 및 밀도를 사용해 얻었다. 실험을 통해 얻은 측정값을 참고문헌에 보고된 자료를 사용해 얻은 계산값과 비교하였다. 단층시편의 경우, 실험을 통해 얻는 열확산계수와 열전도도는 계산값보다 작았다. 스테인리스강의 경우, 측정한 열전도도는 계산값에 비해 6% 정도 작았으며, 알루미늄의 경우 18% 정도 작았다. 반면, 2층 금속인 스테인리스강과 알루미늄의 클래드메탈은 측정한 열전도도가 계산값에 비해 55% 정도 낮게 나타났다. 섬광법으로 측정한 열전도도가 계산값보다 55% 정도 낮게 나타난 이유는 스테인리스강과 알루미늄의 사이에 존재하는 계면의 영향 때문이다. 스테인리스강과 알루미늄의 사이에 존재하는 계면은 열전도 특성을 지배하는 전자와 탄성파의 이동을 어렵게 하기 때문이다. 우수한 방열특성을 갖는 다층구조 방열모듈을 개발하기 위해서는 열전도 특성에 결정적으로 영향을 주는 계면 특성의 조절이 중요하다.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2002년도 춘계학술대회 논문집
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• pp.844-847
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• 2002

This paper is to investigate the wear behavior of submerged-arc clad materials by the wear test with a ball-on-disk type wear testing machine in air. The specimens were clad with Stoody105 alloy wire on a carbon steel (SM45C) substrate by submerged-arc cladding process under different welding parameters. The wear behavior of the cladding through ball-en-disk test has been studied under the wear load from 5N to 16N and sliding speed from 8cm/s to 35cm/s. The weight of the specimen loss was measured. Scanning electron micrographs of the worn surface show a layer of oxide film formed on the worn surface. Oxidation wear mechanism controls the wear process. The spalling of the oxide is caused by the repeated rubbing fatigue mechanism.

• 전기학회논문지P
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• 제58권2호
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• pp.178-183
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• 2009

The developed in-flex system completed the wiring work with the plug-in connection. To maintain electrical and mechanical stability, and an insulation between the conductors was strengthened by forming a partition. Moreover, the error according to a bad connection was prevented by separating the inlet from the outlet of the electric trace and thus the quick construction become possible. The metal reinforcing material was added outside the upper case and lower case. The fire-resistance efficiency was maximized in order to minimize a damage by the fire. As to the developed system, we found that it takes shorter time to complete installation than the rigid steel conduit wiring work, and that about 25 % of construction cost was saved because the labor costs decrease due to the shorter construction period of time.