• 제목/요약/키워드: Clad

검색결과 408건 처리시간 0.028초

폴리이미드와 Cu/Ni층과의 계면결합력에 미치는 플라즈마 처리 시간 효과 (Effect of Plasma Treatment Times on the Adhesion of Cu/Ni Thin Film to Polyimide)

  • 우태규;박일송;정광희;전우용;설경원
    • 대한금속재료학회지
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    • 제49권8호
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    • pp.657-663
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    • 2011
  • This study represents the results of the peel strength and surface morphology according to the preprocessing times of polyimide (PI) in a Cu/Ni/PI structure flexible copper clad laminate production process based on the polyimide. Field emission scanning electron microscopy, X-ray diffraction, and X-ray photoelectron spectroscopy were used to analyze the surface morphology, crystal structure, and interface binding structure of sputtered Ni, Cu, and electrodeposited copper foil layers. The surface roughness of Ni, Cu deposition layers and the crystal structure of electrodeposited Cu layers were varied according to the preprocessing times. In the RF plasma times that were varied by 100-600 seconds in a preprocessing process, the preprocessing applied by about 300-400 seconds showed a homogeneous surface morphology in the metal layers and that also represented high peel strength for the polyimide. Considering the effect of peel strength on plastic deformation, preprocessing times can reasonably be at about 400 seconds.

분광타원법을 이용한 Pr 첨가 Ge-Sb-Se 계열 셀레나이드 유리의 굴절률 결정 (Determination of optical properties of Pr3+-doped selenide glasses of Ge-Sb-Se system using spectroscopic ellipsometry)

  • 신상균;김상준;김상열;최용규;박봉제;서홍석
    • 한국광학회지
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    • 제14권6호
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    • pp.594-599
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    • 2003
  • 1.6 $\mu\textrm{m}$ 파장대의 U밴드 광증폭기용 광섬유 소재인 Pr첨가 Ge-Sb-Se 계열 셀레나이드 유리의 굴절률을 분광타원법을 이용하여 결정하였다. 시료의 광물성을 조사하기 위해 투과 파장 영역에서의 타원 스펙트럼을 Sellmeier 분산관계식에 기반한 공기/미시 거칠기층/표면층/기층으로 구성된 4상계의 모델에 적용하여 굴절률과 분산계수 및 박막구조상수를 동시에 얻을 수 있었다. 디스크 형태로 가공된 각 시료의 양면을 대상으로 위치에 따라 수회 반복 측정을 통하여 시료의 표면 거칠기의 영향을 파악함으로써 조성 변화에 대한 굴절률 변화 양상을 보다 정확히 파악하였다. 시료의 표면 거칠기가 굴절률 측정치의 편차에 주된 영향을 미쳤으나 1 몰%에 해당하는 소량의 조성변화에 따른 굴절률 변화를 신뢰할 수 있는 수준으로 결정할 수 있었다. 실험적으로 결정된 조성변화와 굴절률과의 관계식은 단일모드의 셀레나이드 광섬유 제작에 있어 코어와 클래드의 조성을 결정하는데 직접적으로 활용될 수 있다.

중성자 조사에 따른 Ni도금피복재에서의 He발생량평가 (He Generation Evaluation on Electrodeposited Ni After Neutron Exposure)

  • 황성식;권준현;김동진;김성우
    • Corrosion Science and Technology
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    • 제20권5호
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    • pp.308-314
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    • 2021
  • Neutron dose level at bottom head of a reactor pressure vessel (RPV) was calculated using reactor vessel neutron transport for a Korean nuclear power plant A. At 34 EFPY with a 40-year (2042) design life after plating repair, irradiation fast neutron effect was 6.6x1015 n/cm2. As helium(He) gas can be generated by Ni only at 1/106 level of 5 × 1021 n/cm2, He generation possibility in the Ni plating layer is very little during 40 years of operation (2042, 34 EFPY). Thermal neutrons can significantly affect the generation of He from Ni metal. At 10 years after a repair, He can be generated at a level of about 0.06 appm, a level that can add general welding repair without any consideration. After 40 years of repair, 9.8 appm of He may be generated. Although this is a rather high value, it is within the range of 0.1 to 10 appm when welding repair can be applied. Clad repair by Ni electroplating technology is expected to greatly improve the operation efficiency by improving the safety and shortening the maintenance period of the nuclear power plant.

근대 초 조선민족성과 조선미의식 담론의 논리화 방식 : 안확(安廓)과 야나기 무네요시(柳宗悅)를 중심으로 (A Study on the discourse about Chosǒn national character and Chosǒn aesthetic consciousness : focusing on the An Hwak and Yanagi Muneyoshi's discourse)

  • 이선이
    • 비교문화연구
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    • 제25권
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    • pp.267-290
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    • 2011
  • The purpose of this study is examining a circulation and conflict of concepts and logics of the $Chos{\check{o}}n$-ness by analysing the $Chos{\check{o}}n$ national character and $Chos{\check{o}}n$ aesthetic consciousness. As entering the modern period, we understood the nations as a unit of the artistic awareness. So, national art is defined as a national character expression from this period. The $Chos{\check{o}}n$ aesthetic consciousness by raising in this period, which is connected with the discourse of national character, carry out a discussional practice defining the Korean originality. However, there is a circulation and conflict of concepts and logics about the $Chos{\check{o}}n$ aesthetic consciousness in the process of a discussion. For the most representative examples are 'the white-clad folk' and 'the beauty of sorrow'. An Hwak and Yanagi Muneyoshi are representative debaters who try to establish the $Chos{\check{o}}n$-ness and their discussion supports these facts. As An Hwak regressing of the respect for high antiquity, he demolished the historical character from the $Chos{\check{o}}n$-ness and overlooked aesthetic differences by a periodical change. Yanagi Muneyoshi totally separates arts from politics and disposes of Korean arts in an abstract timeless-space. The function of such an early-modern period's discourse about $Chos{\check{o}}n$ aesthetic consciousness is that $Chos{\check{o}}n$ national character makes the dehistoricization and depoliticization.

냉간압연접합법에 의해 제조된 AA6061/AA5052/AA6061 복합판재의 미세조직 및 기계적 성질 (Microstructure and Mechanical Properties of AA6061/AA5052/AA6061 Complex Sheet Fabricated by Cold-Roll Bonding Process)

  • 황주연;이성희
    • 한국재료학회지
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    • 제29권6호
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    • pp.392-397
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    • 2019
  • A cold roll-bonding process is applied to fabricate an AA6061/AA5052/AA6061 three-layer clad sheet. Two AA6061 and one AA5052 sheets of 2 mm thickness, 40 mm width, and 300 mm length are stacked, with the AA5052 sheet located in the center. After surface treatment such as degreasing and wire brushing, sample is reduced to a thickness of 1.5 mm by multi-pass cold rolling. The rolling is performed at ambient temperature without lubricant using a 2-high mill with a roll diameter of 400 mm at rolling speed of 6.0 m/sec. The roll bonded AA6061/AA5052/AA6061 complex sheet is then hardened by natural aging(T4) and artificial aging(T6) treatments. The microstructures of the as-roll bonded and age-hardened Al complex sheets are revealed by optical microscopy; the mechanical properties are investigated by tensile testing and hardness testing. After rolling, the roll-bonded AA6061/AA5052/AA6061 sheets show a typical deformation structure in which grains are elongated in the rolling direction. However, after T4 and T6 aging treatment, there is a recrystallization structure consisting of coarse equiaxed grains in both AA5052 and AA6061 sheets. The as roll-bonded specimen shows a sandwich structure in which an AA5052 sheet is inserted into two AA6061 sheets with higher hardness. However, after T4 and T6 aging treatment, there is a different sandwich structure in which the hardness of the upper and lower layers of the AA6061 sheets is higher than that of the center of the AA5052 sheet. The strength values of the T4 and T6 age-treated specimens are found to increase by 1.3 and 1.4 times, respectively, compared to that value of the starting material.

금속연료-피복재 상호확산 거동에 미치는 기상증착법의 영향 (Effect of Vapor Deposition on the Interdiffusion Behavior between the Metallic Fuel and Clad Material)

  • 김준환;이병운;이찬복;지승현;윤영수
    • 대한금속재료학회지
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    • 제49권7호
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    • pp.549-556
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    • 2011
  • This study aimed to evaluate the performance of diffusion barriers in order to prevent fuel-cladding chemical interaction (FCCI) between the metallic fuels and the cladding materials, a potential hazard for nuclear fuel in sodium-cooled fast reactors. In order to prevent FCCI, Zr or V metal is deposited on the ferritic-martensitic stainless steel surface by physical vapor deposition with a thickness up to $5{\mu}m$. The diffusion couple tests using uranium alloy (U-10Zr) and a rare earth metal such as Ce-La alloy and Nd were performed at temperatures between 660~800$^{\circ}C$. Microstructural analysis using SEM was carried out over the coupled specimen. The results show that significant interdiffusion and an associated eutectic reaction ocurred in the specimen without a diffusion barrier. However, with the exception of the local dissolution of the Zr layer in the Ce-La alloy, the specimens deposited with Zr and V exhibited superior eutectic resistance to the uranium alloy and rare earth metal.

다층 PCB의 두께 예측을 위한 실험식 도출 연구 (An Empirical Formulation for Predicting the Thickness of Multilayer PCB)

  • 김남훈;한관희;이민수;김현호;신광복
    • Composites Research
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    • 제35권3호
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    • pp.182-187
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    • 2022
  • 본 논문은 다층 PCB에 사용되는 프리프레그의 물성을 파악하여 제시한 두께 실험식을 통해 PCB의 두께를 예측하기 위한 연구를 수행하였다. 프리프레그는 물성과 동박 잔존율에 의해서 PCB 제작시 두께가 감소하기 때문에 두께 실험식을 통한 정확한 PCB의 두께 예측이 필요하다. 두께 실험식에 사용되는 프리프레그의 밀도를 파악하기 위해 질량 및 두께를 측정하여 밀도를 도출하였다. 이후 CCL을 제작하기 위해 프리프레그와 동박을 적층하여 핫 프레스기를 사용하였고 광학현미경과 마이크로미터를 사용하여 두께를 측정하였다. 또한 동박 잔존율에 따른 두께 변화를 측정하기 위해 회로밀도를 다르게 구성하여 8층 PCB를 설계하였고 두께 측정 결과와 두께 실험식으로 도출된 두께를 비교하여 두께 실험식을 검증하였다. 비교 결과 CCL의 경우 2.56%, 다층 PCB의 경우 4.48%의 오차를 보였고 이를 통해 두께실험식의 신뢰성을 확인하였다.

나노압입시험법을 이용한 후열처리된 Ti/Al 클래딩재의 잔류 응력 평가 (Characterizing Residual Stress of Post-Heat Treated Ti/Al Cladding Materials Using Nanoindentation Test Method)

  • 유상규;김지원;오명훈;최인철
    • 열처리공학회지
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    • 제36권2호
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    • pp.61-68
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    • 2023
  • Ti and Ti alloys are used in the automobile and aerospace industries due to their high specific strength and excellent corrosion resistance. However their application is limited due to poor formability at room temperature and high unit cost. In order to overcome these issues, dissimilarly jointed materials, such as cladding materials, are widely investigated to utilize them in each industrial field because of an enhanced plasticity and relatively low cost. Among various dissimilar bonding processes, the rolled cladding process is widely used in Ti alloys, but has a disadvantage of low bonding strength. Although this problem can be solved through post-heat treatment, the mechanical properties at the bonded interface are deteriorated due to residual stress generated during post-heat treatment. Therefore, in this study, the microstructure change and residual stress trends at the interfaces of Ti/Al cladding materials were studied with increasing post-heat treatment temperature. As a result, compared to the as-rolled specimens, no difference in microstructure was observed in the specimens after postheat treatment at 300, 400, and 500℃. However, a new intermetallic compound layer was formed between Ti and Al when post-heat treatment was performed at a temperature of 600℃ or higher. Then, it was also confirmed that compressive residual stress with a large deviation was formed in Ti due to the difference in thermal expansion coefficient and modulus of elasticity between Ti Grade II and Al 1050.

냉간압연접합된 층상 AA6061/AA5052/AA6061/AA5052 알루미늄합금판재의 미세조직 및 기계적 성질 (Microstructure and Mechanical Properties of Cold Roll-Bonded Layered AA6061/AA5052/AA6061/AA5052 Aluminum Alloy Sheet)

  • 조상현;박보배;이성희
    • 한국재료학회지
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    • 제32권3호
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    • pp.161-167
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    • 2022
  • A cold roll-bonding process is applied to fabricate an AA6061/AA5052/AA6061/AA5052 layered sheet. Two AA6061 and one AA5052 sheets of 2mm thickness, 40mm width and 300mm length are alternately stacked, then reduced to a thickness of 2.0 mm by multi-pass cold rolling after surface treatment such as degreasing and wire brushing. The rolling is performed at ambient temperature without lubricant using a 2-high mill with a roll diameter of 400 mm at a rolling speed of 6.0 m/sec. The roll-bonded AA6061/AA5052/AA6061/AA5052 layered sheet is then hardened by natural aging (T4) and artificial aging (T6) treatments. The microstructure of the as-roll bonded and the age-hardened Al sheets was revealed by SEM observation; the mechanical properties were investigated by tensile testing and hardness testing. After T4 and T6 aging treatment, the specimens had a recrystallization structure consisting of coarse equiaxed grains in both AA5052 and AA6061 regions. The as-roll-bonded specimen showed a clad structure in which the hardness of AA5052 regions was higher than that of AA6061 regions. However, after T4 and T6 aging treatment, specimens exhibited different structures, with hardness of AA6061 regions higher than that of AA5052 regions. Strengths of T6 and T4 age-treated specimens were found to increase by 1.55 and 1.36 times, respectively, compared to the value of the starting material.

Nitric Oxide-Induced Downregulation of a NAD(P)-Binding Rossmann-Fold Superfamily Gene Negatively Impacts Growth and Defense in Arabidopsis thaliana

  • Tiba Nazar Ibrahim Al Azawi;Murtaza Khan;Bong-Gyu Mun;Song-Uk Lee;Da-sol Lee;Waqas Rahim;Anjali Pande;Nusrat Jahan Methela;Cho-Jun Ho;Byung-Wook Yun
    • 한국작물학회:학술대회논문집
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    • 한국작물학회 2022년도 추계학술대회
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    • pp.143-143
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    • 2022
  • Plant defense systems against pathogens have been studied extensively and are currently a hot topic in plant science. Using a reverse genetics technique, this study looked into the involvement of the NO-downregulated NAD(P)-binding Rossmann-fold superfamily gene in plant growth and defense in Arabidopsis thaliana. For this purpose, the knockout and overexpressing plant of the candidate gene along with the relevant controls were exposed to control, oxidative and nitro-oxidative stresses. The results showed that candidate gene negatively regulates plants' root and shoot lengths. To investigate the role of the candidate gene in plant basal defense, R-gene-mediated resistance and systemic acquired resistance (SAR) plants were challenged with virulent or avirulent strains of Pseudomonas syringae pathovar tomato (Psf) DC3000. The results showed that the candidate gene negatively regulates plants' basal defense, R-gene-mediated resistance and SAR. Further characterization via GO analysis associated the candidate gene with metabolic and cellular processes and response to light stimulus, nucleotide binding and cellular location in the cytosol and nucleus. Protein structure analysis indicated the presence of a canonical Oxidoreductase family NAD (P)-binding Rossmann fold domain of 120 amino acids with a total of 121 plant homologs across 35 different plant species in the clad streptophyta. Arabidopsis eFP browser showed its expression in almost all the above-ground parts. Protein analysis indicated C225 and C359 as potential targets for S-Nitrosylation by NO. SMART analysis indicated possible interactions with mevalonate/galactokinase, galacturonic acid kinase, arabinose kinase, putative xylulose kinase, GroES-like zinc-binding alcohol dehydrogenase and various glyceraldehyde-3-phosphate dehydrogenases.

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