• 한국세라믹학회지
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• 제50권6호
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• pp.523-527
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• 2013

Ti-based coatings following laser ablation were studied to compare degradation behaviors by thermomechanical stress. TiN, TiCN, and TiAlN coatings were degraded by a Nd:YAG pulsed laser with an increase in the laser pulses. A decrease in the hardness was identified as the pulses increased, and the hardness levels were in the order of TiAlN > TiCN > TiN. The TiN showed cracks on the surface, and cracks with pores formed along the cracks were observed in the TiCN. The dominant degradation behavior of the TiAlN was surface pore formation. EDS results revealed that diffusion of substrate atoms to the coating surface occurred in the TiN. Delamination occurred in the TiN and TiCN, while the TiAlN which has higher thermal stability than the TiN and TiCN maintained adhesion to the substrate. It was considered that the decrease in the hardness of the Ti-based hard coatings is attributed to surface cracking and the diffusion of substrate atoms.

• 대한의용생체공학회:의공학회지
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• 제26권5호
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• pp.319-330
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• 2005

Over the past few decades, much effort has been made to improve the mechanical and biological performance of HA, in order to extend its range of applications. As a major inorganic component of human hard tissues, hydroxyapatite bioceramic is regarded as being one of the most biocompatible materials. Numerous in vitro and in vivo studies have confirmed its excellent bioactivity, osteoconductivity and bone forming ability. However, because of its poor mechanical properties, its use in hard tissue applications has been restricted to those areas in which it can be used in the form of small sized powders/granules or in the non-load bearing sites. A number of researchers have focused on improving the mechanical and biological performance of HA, as well as on the formulation of hybrid and composite systems in order to extend its range of applications. In this article, we reviewed our recent works on HA-based biomaterials; i) the strengthening of HA with ceramic oxides, ii) HA-based bioactive coatings on metallic implants, iii) HA-based porous scaffolds and iv) HA-polymer hybrids/composites.

• Journal of Ceramic Processing Research
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• 제19권5호
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• pp.434-438
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• 2018

The sintering behavior of $BaFe_{12}O_{19}$ with the addition of one and three weight % of $CuWO_4$ as a liquid phase sintering aid is studied. Samples are sintered in the temperature range $900-1250^{\circ}C$ and the effect of $CuWO_4$ addition on density, microstructure, phase composition and magnetic properties is examined. Compared to $BaFe_{12}O_{19}$ with no sintering aid addition, addition of 1 wt % $CuWO_4$ retards densification. Addition of 3 wt % $CuWO_4$ promotes densification at lower sintering temperatures but retards densification at temperatures > $1050^{\circ}C$. Three wt % $CuWO_4$ addition induces the formation of $BaWO_4$ and $Ba_3WFe_2O_9$ secondary phases at temperatures ${\geq}1100^{\circ}C$. Addition of $CuWO_4$ causes a decrease in saturation magnetization, remanent magnetization and coercivity.

• 자동차안전학회지
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• 제11권1호
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• pp.23-29
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• 2019

Recently, use of composite materials has been increasing for body structures and chassis parts in the car industry because of weight reduction effect and excellent mechanical thermal characteristics. However, application of composite materials in brake system is very difficult because it is hard to obtain enough brake performance due to low heat storage capacity of the composite materials. In this paper, we will present new carbon ceramic composite disc with high flow characteristic. To obtain this characteristic, new vent structures were designed by using ARIZ method and substance-field model analysis. The flow effect of these vent structures on the brake performance was verified by pugh matrix and cooling test. The test results show improvement of cooling performance up to $30^{\circ}C$. Finally, These results will improve brake the reliability of the brake performance for the high performance vehicles and electric vehicles.

• Journal of Ceramic Processing Research
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• 제19권5호
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• pp.439-443
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• 2018

The outstanding characteristics of high quality GaN single crystal substrates make it possible to apply the manufacture of high brightness light emitting diodes and power devices. However, it is very difficult to obtain high quality GaN substrate because the process conditions are hard to control. In order to effectively control the formation of GaN polycrystals during the bulk GaN single crystal growth by the HVPE (hydride vapor phase epitaxy) method, a quartz ring was introduced in the edge of substrate. A variety of evaluating method such as high resolution X-ray diffraction, Raman spectroscopy and photoluminescence was used in order to measure the effectiveness of the quartz ring. A secondary ion mass spectroscopy was also used for evaluating the variations of impurity concentration in the resulting GaN single crystal. Through the detailed investigations, we could confirm that the introduction of a quartz ring during the GaN single crystal growth process using HVPE is a very effective strategy to obtain a high quality GaN single crystal.

• 한국재료학회:학술대회논문집
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• 한국재료학회 2011년도 춘계학술발표대회
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• pp.53.2-53.2
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• 2011

Ti metal has superior mechanical properties along with biocompatibility, but it still has the problem of bio-inertness thus forming weaker bond in bone/implant interface and long term clinical performance as orthopaedic and dental devices are restricted for stress shielding effect. On the other hand, despite the excellent biodegradable behavior as being an integral constituent of the natural bone, the mechanical properties of ${\beta}$-tricalcium phosphate $(Ca_3(PO_4)_2;\;{\beta}-TCP)$ ceramics are not reliable enough for post operative load bearing application in human hard tissue defect site. One reasonable approach would be to mediate the features of the two by making a composite. In this study, ${\beta}$-TCP/Ti ceramic-metal composites were fabricated by spark plasma sintering in inert atmosphere to inhibit the formation of $TiO_2$. Composites of 30 vol%, 50 vol% and 70 vol% ${\beta}$-TCP with Ti were fabricated. Detailed microstructural and phase characteristics were investigated by FE-SEM, EDS and XRD. Material properties like relative density, hardness, compressive strength, elastic modulus etc. were characterized. Cell viability and biocompatibility were investigated using the MTT assay and by examining cell proliferation behavior.

• 한국세라믹학회지
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• 제46권1호
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• pp.102-107
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• 2009

This study has been focused on an effective surface finishing method combining ELID (ELectrolytic In-process Dressing) and MAP (Magnetic Assisted Polishing) for the nano-precision mirror grinding of glass-lens molding mould. ELID grinding is an excellent technique for mirror grinding of various advanced metallic or nonmetallic materials. A polishing process is also required for elimination of scratches present on ELID grinded surfaces. MAP has been used as polishing method due to its high polishing efficiency and superior surface quality. It also presents some techniques for achieving the nanometer roughness of the hard material such as WC-Co, which are extensively used in precision tooling material.

• 박물관보존과학
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• 제17권
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• pp.101-116
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• 2016

기존의 석고복원재로 복원한 문화재는 대기 중의 수분을 반복하여 흡·방출하면서 물성이 약화되어 형태가 변형되고 채색층 박락이 진행된다. 본 논문에서는 이러한 단점을 보완하기 위해 일반석고보다 더 강한 초경석고를 실험대상으로 두었으며 메타카올린(Metakaolin)을 혼합하여 도자기 복원재료로 적합하도록 물성을 개선하였다. 초경석고와 메타카올린 혼합재료의 압축강도(119MPa)는 일반석고(26MPa)보다 월등히 높았으며, 마모율(0.88％)은 일반석고의 마모율 2.53％ 보다 낮게, 흡수율(2.9％)은 일반석고(17.2％) 보다 약 5배 낮게 측정되었다. 특히, 주사전자현미경 관찰결과 혼합재료의 경화치밀도가 단미의 초경석고보다 높았다. 즉, 메타카올린을 첨가함으로써 초경석고의 강도와 수분저항성을 높이고 표면을 치밀하게 하여 도자기 복원재료로서 적합하게 물성을 개선시켰다. 그리고 이 혼합재료를 실재 문화재인 토제수반(신안18892), 분청사기조화문병(접수2034), 분청사기 국문내인화문대접(접수1730)의 결손부 복원에 적용해봄으로써, 혼합재료가 주입 및 적층성형에 유리하고 경화표면이 균질하여 자연스러운 채색이 가능한 재료임을 확인하였다.

• 한국재료학회지
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• 제13권11호
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• pp.725-731
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• 2003

The effect of organic processing parameters on the dispersion stability of the BaTiO$_3$-based dielectric particles and borosilicate glass particulate suspensions was investigated in a system where organic solvents, dispersant, binder and modifier were used as processing additives in a low temperature cofired ceramic fabrication processes. Two- and three-component organic solvents were used to disperse ceramic particles and it was found the better stability in the particulate suspension prepared in a bi-solvent, which was consists of toluene and ethanol in a non-azeotropic composition. The addition amount of organic additives had a great impact on dispersion in the present investigation. The flow curves of the suspensions prepared with binder and modifier were fitted according to the power-law equation, which indicates that the internal structure of the suspension could be disturbed under the applied shear stress. Finally, the LTCC green tapes were successfully tape-cast based upon the optimum formulation of LTCC suspension and its microstructure was compared with that of the hard-agglomerates.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 1996년도 춘계학술대회 논문집
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• pp.526-530
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• 1996

In this paper, three different types of commercially tools-P20, NC123K and ceramic-have been used to working austempered ductile iron(ADI). In the austempered condition the materials are hard, strong and difficult to machine. Thus, we selected a optimum tool material among three different types of used tools in machining of austempered ductile iron. It was used acoustic emission(AE) to know cutting characteristic for selected tool and flank wear land of the ceramic too. The obtained results are as follows; (1) The ceramic tool among three different types of tools is the best in machining austempered ductile iron. (2) In case of ceramic tool, the amplitude level of AE signal(AErms) is mainly affected bycutting speed in cutting speed in cutting condition and it is proportioned to cutting speed. (3) There have the relationship of direct proportion between the amplitude level of AE signal and flank wear land of the tool. (4) If it find the value of AErms at each cutting speed, the in-process detection to ceramic tool's wear is possible