• 한국재료학회지
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• 제25권8호
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• pp.417-422
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• 2015

In this study, low-carbon hypoeutectoid steels with different ferrite-pearlite microstructures were fabricated by varying transformation temperature. The microstructural factors such as pearlite fraction and interlamellar spacing, and cementite thickness were quantitatively measured and then Charpy impact tests conducted on the specimens in order to investigate the correlation of the microstructural factors with impact toughness and ductile-brittle transition temperature. The microstructural analysis results showed that the pearlite interlamellar spacing and cementite thickness decreases while the pearlite fraction increases as the transformation temperature decreases. Although the specimens with higher pearlite fractions have low absorbed energy, on the other hand, the absorbed energy is higher in room temperature than in low temperature. The upper-shelf energy slightly increases with decreasing the pearlite interlamellar spacing. However, the ductile-brittle transition temperature is hardly affected by the pearlite interlamellar spacing because there is an optimum interlamellar spacing dependent on lamellar ferrite and cementite thickness and because the increase in pearlite fraction and the decrease in interlamellar spacing with decreasing transformation temperature have a contradictory role on absorbed energy.

• 한국재료학회지
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• 제24권1호
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• pp.13-18
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• 2014

In order to clarify the effect of Nb addition on the ductile-brittle transition property of sintered TiC, TiC-10 mol% Nb composites were researched using a three-point bending test at temperatures from room temperature to 2020 K, and the fracture surface was observed by scanning electron microscopy. It was found that the Nb addition decreases the ductile-brittle transition temperature of sintered TiC by 300 K and increases the ductility. The room temperature bending strength was maintained at up to 1800 K, but drastically dropped at higher temperatures in pure TiC. The strength increased moderately to a value of 320MPa at 1600 K in TiC-10 mol% Nb composites, which is 40% of the room temperature strength. Pores were observed in both the grains and the grain boundaries. It can be seen that, as Nb was added, the size of the grain decreased. The ductile-brittle transition temperature in TiC-10 mol% Nb composites was determined to be 1550 K. Above 1970 K, yieldpoint behavior was observed. When the grain boundary and cleavage strengths exceed the yield strength, plastic deformation is observed at about the same stress level in bending as in compression. The effect of Nb addition is discussed from the viewpoint of ability for plastic deformation.

• 한국재료학회지
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• 제23권7호
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• pp.385-391
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• 2013

The influence of Cu and Ni on the ductile-brittle transition behavior of metastable austenitic Fe-18Cr-10Mn-N alloys with N contents below 0.5 wt.% was investigated in terms of austenite stability and microstructure. All the metastable austenitic Fe-18Cr-10Mn-N alloys exhibited a ductile-brittle transition behavior by unusual low-temperature brittle fracture, irrespective of Cu and/or Ni addition, and deformation-induced martensitic transformation occasionally occurred during Charpy impact testing at lower temperatures due to reduced austenite stability resulting from insufficient N content. The formation of deformation-induced martensite substantially increased the ductile-brittle transition temperature(DBTT) by deteriorating low-temperature toughness because the martensite was more brittle than the parent austenite phase beyond the energy absorbed during transformation, and its volume fraction was too small. On the other hand, the Cu addition to the metastable austenitic Fe-18Cr-10Mn-N alloy increased DBTT because the presence of ${\delta}$-ferrite had a negative effect on low-temperature toughness. However, the combined addition of Cu and Ni to the metastable austenitic Fe-18Cr-10Mn-N alloy decreased DBTT, compared to the sole addtion of Ni or Cu. This could be explained by the fact that the combined addition of Cu and Ni largely enhanced austenite stability, and suppressed the formation of deformation-induced martensite and ${\delta}$-ferrite in conjunction with the beneficial effect of Cu which may increase stacking fault energy, so that it allows cross-slip to occur and thus reduces the planarity of the deformation mechanism.

• 한국재료학회지
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• 제31권9호
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• pp.519-524
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• 2021

The impact properties of two austenitic Fe-23Mn-0.4C steels with different Al contents for cryogenic applications are investigated in this study. The 4Al steel consists mostly of austenite single-phase microstructure, while the 5Al steel exhibits a two-phase microstructure of austenite and delta-ferrite with coarse and elongated grains. Charpy impact test results reveal that the 5Al steel with duplex phases of austenite and delta-ferrite exhibits a ductile-to-brittle transition behavior, while the 4Al steel with only single-phase austenite has higher absorbed energy over 100 J at -196 ℃. The SEM fractographs of Charpy impact specimens show that the 4Al steel has a ductile dimple fracture regardless of test temperature, whereas the 5Al steel fractured at -100 ℃ and -196 ℃ exhibits a mixed fracture mode of both ductile and brittle fractures. Additionally, quasi-cleavage fracture caused by crack propagation of delta-ferrite phase is found in some regions of the brittle fracture surface of the 5Al steel. Based on these results, the delta-ferrite phase hardly has a significant effect on absorbed energy at room-temperature, but it significantly deteriorates low-temperature toughness by acting as the main site of the propagation of brittle cracks at cryogenic-temperatures.

• Structural Engineering and Mechanics
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• 제16권6호
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• pp.713-730
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• 2003

This paper contains the results of the study on the development of fracture and crack propagation in quasi-brittle materials, such as concrete or rocks, using the Discrete Element Method (DEM). A new discrete element numerical model is proposed as the basis for analyzing the inelastic evolution and growth of cracks up to the point of gross material failure. The model is expected to predict the fracture behavior for the quasi-brittle material structure using the elementary aggregate level, the interaction between aggregate materials, and bond cementation. The algorithms generate normal and shear forces between two interfacing blocks and contains two kinds of contact logic, one for connected blocks and the other one for blocks that are not directly connected. The Mohr-Coulomb theory has been used for the fracture limit. In this algorithm the particles are moving based on the connected block logic until the forces increase up to the fracture limit. After passing the limit, the particles are governed by the discrete block logic. In setting up a discrete polygon element model, two dimensional polygons are used to investigate the response of an assembly of different shapes, sizes, and orientations with blocks subjected to simple applied loads. Several examples involving assemblies of particles are presented to show the behavior of the fracture and the failure process.

• 한국신뢰성학회지:신뢰성응용연구
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• 제16권2호
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• pp.104-109
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• 2016

Purpose: The purpose of this study is to analyze fracture behavior and failure mechanism of porous titanium for dental implant fabricated by space holder process. Method: Three porous titanium specimens with a specific volume fraction of open pore were test by 3 point bending and compression stress condition, respectively. Fracture appearance was observed by scanning electron microscope and discussed in relation with oxygen content. Results: For compression-tested specimens, two specimen showed brittle failure, while the other one showed normal failure after deformation. High oxygen content was detected in the brittle-fractured specimen. Several micro-cracks initiated at the struts propagated down to the bottom of the specimen resulting in normal failure. Conclusion: Oxygen contamination during the fabrication process can leads brittle premature failure, and hence quality problem of the porous titanium for dental implant.

• International Journal of Precision Engineering and Manufacturing
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• 제4권1호
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• pp.30-36
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• 2003

Brittle materials such as glasses and ceramics, which are very weak under impact loading, show fragile failure mode due to their low fracture toughness and crack sensitivity. When brittle materials are subjected to impact by small spheres, high contact pressure occurs at the impacted surface causing local damage on the specimen. This damage is a dangerous factor in causing the final fracture of structures. In this research, the crack propagation process of soda-lime glass by the impact of small spheres is explained and the effects of several constraint conditions for impact damage were studied by using soda-lime glass; that is, the effects for the materials and sizes of impact ball, thickness of specimen and residual strength were evaluated. Especially, this research has focused on the damage behavior of ring cracks, cone cracks and several other kinds of cracks.

• 한국공작기계학회논문집
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• 제13권2호
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• pp.104-111
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• 2004

Ultrasonic machining is a non-thermal, non-chemical, md non-electorial material removal process, and thus results in minimum modifications in mechanical properties of the brittle material during the process. Also, ultrasonic machining is a non-contact process that utilize ultrasonic vibration to impact a brittle material. In this research characteristics of micro-hole machining for brittle materials by ultrasonic machining(USM) process have been investigated. And the effect of ultrasonic vibration on the machining conditions is analyzed when machining fir non-conductive brittle materials using tungsten carbide tools with a view to improve form and machining accuracy.

• Structural Engineering and Mechanics
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• 제29권3호
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• pp.301-310
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• 2008

Applications of fracture mechanics in the strength analysis of ceramic materials have been lately studied by many researchers. Various test specimens have been proposed in order to investigate the fracture resistance of cracked bodies under mixed mode conditions. Double Cleavage Drilled Compression (DCDC) specimen, with a hole offset from the centerline is a configuration that is frequently used in subcritical crack growth studies of ceramics and glasses. This specimen exhibits a strong crack path stability that is due to the strongly negative T-stress term. In this paper the maximum tensile stress (MTS) criterion is employed for investigating theoretically the initiation of brittle fracture in the DCDC specimen under mixed mode conditions. It is shown that the T-stress has a significant influence on the predicted fracture load and the crack initiation angle. The theoretical results suggest that brittle fracture in the DCDC specimen is controlled by a combination of the singular stresses (characterized by KI and KII) and the non-singular stress term, T-stress.

• 한국재료학회지
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• 제23권11호
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• pp.649-654
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• 2013

The effect of interstitial elements on the ductile-brittle transition behavior of austenitic Fe-18Cr-10Mn-2Ni alloys with different nitrogen and carbon contents was investigated in this study. All the alloys exhibited ductile-brittle transition behavior because of unusual low-temperature brittle fracture, even though they have a faced-centered cubic structure. With the same interstitial content, the combined addition of nitrogen and carbon, compared to the sole addition of nitrogen, improved the low-temperature toughness and thus decreased the ductile-brittle transition temperature (DBTT) because this combined addition effectively enhances the metallic component of the interatomic bonds and is accompanied by good plasticity and toughness due to the increased free electron concentration. The increase in carbon content or of the carbon-to-nitrogen ratio, however, could increase the DBTT since either of these causes the occurrence of intergranular fracture that lead to the deterioration of the toughness at low temperatures. The secondary ion mass spectroscopy analysis results for the observation of carbon and nitrogen distributions confirms that the carbon and nitrogen atoms were significantly segregated to the austenite grain boundaries and then caused grain boundary embrittlement. In order to successfully develop austenitic Fe-Cr-Mn alloys for low-temperature application, therefore, more systematic study is required to determine the optimum content and ratio of carbon and nitrogen in terms of free electron concentration and grain boundary embrittlement.