• Steel and Composite Structures
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• v.19 no.6
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• pp.1531-1548
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• 2015

The aim of this study is to investigate the relationship between Barcol hardness (H) and flexural modulus (E) degradation of composite sheets subjected to flexural fatigue. The resin transfer molding (RTM) method was used to produce 3-mm-thick composite sheets with fiber volume fraction of 44%. The composite sheets were subjected to flexural fatigue tests and Barcol scale hardness measurements. After these tests, the stiffness and hardness degradations were investigated in the composite sheets that failed after around one million cycles (stage III). Flexural modulus degradation values were in the range of 0.41-0.42 with the corresponding measured hardness degradation values in the range of 0.25-0.32 for the all fatigued composite sheets. Thus, a 25% reduction in the initial hardness and a 41% reduction in the initial flexural modulus can be taken as the failure criteria. The results showed that a reasonably well-defined relationship between Barcol hardness and flexural modulus degradation in the distance range.

• The Journal of Korean Academy of Prosthodontics
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• v.42 no.4
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• pp.344-355
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• 2004

Statement of problem: For a long time, many of denture base acrylic resins have been used for edentulous and partial edentulous patients because of easy manipulation and good mechanical properties, but its esthetic aspect has not been commented enough. Denture base acrylic resins also has caused esthetic problems due to discoloration or staining as in esthetic restoration. Many researches and reports have treated the problems and accomplished esthetic improvement. But these researches and reports dealt with general food colors or beverages, not with fermented foods. Purpose: This study is designed to assess what fermented foods, such as soy sauce, gochujang, and toenjang that many of Koreans have taken in, influence on the color and hardness variation of denture base acrylic resins. Materials and methods: For the procedure, twelve disks per 4 denture base acrylic resins were fabricated with a thickness of 2mm and 16mm in diameter. Each seven specimen were measured for discoloration with spectrophotometer, while the others, five specimen, for surface hardness change with Barcol hardness tester, over time. Each 12 specimen were immersed into the 4 beakers of fermented foods(soy sauces, gochujangs, toenjangs, deionized water), and $L^{*},a^{*}$, and $b^*$ values were measured for the color difference$({\Delta}E^*)$, on the 1st, 7th, and 28th day with spectrophotometer, with the measurement of surface hardness change. Each data observed was processed statistically. Results: The findings are as follows; Discoloration 1. All of denture base resins was not influenced by the kind of fermented foods, except for $QC20^{(R)}$ 2. Soy sauce and red pepper paste caused more change for denture base resins than deionized water and soy bean paste, except for Perform$^{(R)}$ 3. Most significant change was shown in Lucitone 199$^{(R)}$, whereas Perform$^{(R)}$ results in the least change for all immersed solution, with no statistical significance. Hardness change 1. Barcol hardness values in deposited specimens have been changed low degree, but with significant statistical change according to the kind of food and duration. 2. Lucitone$^{(R)}$ 199 as significantly lower Barcol hardness value than others do. Conclusion: Based on the above results, it suggests that the habitual intake of fermented foods is not helpful for the color stability of denture base acrylic resins because Soy sauce and red pepper paste mainly caused discoloration and surface hardness change. Particularly $Lucitone199^{(R)}$ shows specific discoloration and low surface hardness values. Therefore, it is recommended giving caution patients with denture of $Lucitone199^{(R)}$ especially against the habitual intake of fermented foods like soy sauce and red pepper paste.

• Journal of Ocean Engineering and Technology
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• v.27 no.4
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• pp.45-54
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• 2013

In this study, various types of composite materials and adhesives that are actually used in the shipbuilding field for small ships, leisure boats, and fishing boats were applied in the hand lay-up method and vacuum infusion method to manufacture specimens. Then the tensile strength, tensile modulus, flexural strength, and flexural modulus values of these specimens were obtained. In addition, the barcol hardness and fiber content were obtained from the specimens. The results showed that the strengths of the specimens manufactured using the vacuum infusion method were higher than those manufactured using the hand lay-up method. Moreover, the barcol hardness and fiber content were also higher in those manufactured using the vacuum infusion method. The specimens manufactured using the vacuum infusion method were thinner despite their large fiber content.

• Composites Research
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• v.14 no.2
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• pp.33-42
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• 2001

The cure kinetic equation fur 52-glass/polyester prepreg composites was established through DSC (differential scanning calorimetry). Using the established kinetic equation, the temperature distribution of the thick composite was calculated considering the change of heat transfer resistance due to resin impregnation of bleeder plies used. In order to reduce the overheat during cure of thick glass fiber composites, the cure cycle was modified by introducing the cooling and reheating steps. Then the thick glass composites were cured both by the conventional cycle without any cooling or reheating step and the modified cure cycle. The mechanical properties of the thick composites cured by the both cycles were tested by the short beam shear test and the Barcol hardness test, and then their results were compared.

• Polymer(Korea)
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• v.35 no.6
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• pp.565-573
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• 2011

The nanocomposites containing graphene oxide (GO) were prepared in order to improve the mechanical properties of poly(methyl methacrylate)/aluminum hydroxide (PMMA/AH) composites. GO was prepared from graphite by oxidation of Hummers method followed by exfoliation with thermal treatment. The surface of GO was modified by oxygen plasma in various exposure times from 0 to 70 min to improve interfacial compatibility. Compared with PMMA/AH composites, the nanocomposites containing GO modified with oxygen plasma for the exposure time up to 50 min showed significant increases in flexural strength, flexural modulus, Rockwell hardness, Barcol hardness, and Izod impact strength. The morphology of fracture surface showed an improved interfacial adhesion between PMMA/AH composites and GO, which was properly treated with oxygen plasma. The mechanical properties of nanocomposites were deteriorated by increasing the content of GO above 0.07 phr due to the nonuniform dispersion of GO.

• The Journal of Korean Academy of Prosthodontics
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• v.33 no.3
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• pp.569-583
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• 1995

Disinfection of dental impressions are necessary due to contamination with patient’s saliva and blood, which is a potential for cross-infection. The purpose of this study was to evaluate the effects of disinfection of four hydrophilic rubber impression materials with three disinfecting solutions, on the dimensional stability and surface hardness of improved stone casts. Three hydrophilic vinyl polysiloxane impression materials(Express, Reprosil, Exafine) and one polyether impression material(Impregum-F) were mixed according to the manufacturer’s directions and impressions were made on a ADA specification No. 19 stainless-steeldie. On removal of the impressions, each impression was immersed in one of the disinfectants(Banicide, Potadine, Clorox) for 10 minutes. After disinfection, type IV improved stone. casts were poured. On this cast, the linear dimension and surface hardness were measuredusing a Measurescope(Nikon, Japan) and a Barcol hardness tester(Barber, Colman Co U. S. A). The results were as follows : 1. The improved stone casts from disinfected Reprosil and Impregum-F impression material did not show dimensional changes(P>0.01). Those from disinfected Express and Exafine impression material showed dimensional changes(P<0.01). The amount of shrinkage was not clinically significant. 2. The improved stone casts from disinfected Express impression material did not exhibit changes in surface hardness(P>0.01), but those from disinfected Reprosil, Exafine, Imp regnum-F impression material showed changes in surface hardness(P<0.01). 3. The dimensinal stability and surface hardness of the improved stone casts were satisfactory using Banicide on Express, all disinfectants used in this study on Reprosil, Potadin and Clorox on Exafine, Banicide and Clorox on Impregum-F. According to these results, immersion disinfection of hydrophilic rubber impression mate rials did not adversely affect the resultant casts. Nevertheless compatibility tests of impression materials and disinfectants should be done when disinfecting impressions.

• Restorative Dentistry and Endodontics
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• v.12 no.1
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• pp.85-93
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• 1986

The purpose of this study was to investigate the curing effect of visible light through tooth substance, 0.5mm, 1.0mm thickness of enamel and dentin were prepared. Experimental specimen were made by Bisfil M & Silux packing into cylindrical brass mold 6.0mm in diameter, 2.0mm and 3.0mm, in height. All specimen were irradiated by visible light (Grip type) model No. SDL-50 Shofu Co.) for 30 seconds through tooth substance. Experimental groups were classified into enamel group (group 1) and dentin group (group 2) according to the thickness of tooth materials and then were divided into 2 subgroups (0.5mm group and 1.0mm group). In experimental groups, visible light irradiated to the specimen through either 0.5mm in thick or 1.0mm in think of tooth material. In Control group specimen were prepared by direct irradiation on the specimen surface of visible light without through tooth substance. The hardness was measured with a Barcol hardness tester (Barber-Colman Co. U.S.A.) for each prepared specimen. The results were as follows: 1. In control group, there were higher hardness values than those of in experimental group. 2. In experimental groups, 0.5mm groups had higher hardness values than 1.0mm groups did. 3. The hardness value at top surface of the specimen were higher than the hardness of bottom surface in each group. 4. Bisfil M had higher hardness values than Silux. 5. In all specimen of 3.0mm height polymerization effect was not occurred at bottom surface except Bisfil M in control group.

• Polymer(Korea)
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• v.36 no.3
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• pp.251-261
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• 2012

The nanocomposites containing graphene oxide flakes were prepared in order to improve the mechanical properties of artificial marbles based on poly(methyl methacrylate)(PMMA) matrix. Graphene oxide flakes were prepared from graphite by oxidation with Hummers method followed by exfoliation with thermal treatment. Surface of graphene oxide flakes were modified with oxyfluorination in various oxygene:fluorine compositions to improve the interfacial compatibility. The nanocomposites containing graphenes modified with oxyfluorination in the oxygen content of 50% and higher showed the significant increase in flexural strength, flexural modulus, Rockwell hardness, Barcol hardness, and Izod impact strength. The morphology of fractured surface showed the improved interfacial adhesion between PMMA matrix and the graphenes which were properly treated with oxyfluorination. The mechanical properties of nanocomposite were deteriorated by increasing the content of graphene above 0.07 phr due to the nonuniform dispersion of graphenes.

• Korean Journal of Materials Research
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• v.30 no.1
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• pp.22-30
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• 2020

Small fishing vessels are manufactured using FRP. Various studies have been conducted to increase the strength of the composite material by mixing alumina powder with resin. Tensile tests and flexural strength tests are conducted to examine the effect of alumina powder on the strength of GFRP. In the current study, resin/alumina composites at different alumina contents (i.e., 0, 1, 5, and 10 vol%) have been prepared. The physical and mechanical properties of the prepared composites have been investigated. From the results, the tensile strength of the specimen with alumina powder mixed in at 10% shows the highest value of 155.66 MPa. The tensile strength of the specimen mixed with alumina powder increases with the amount of alumina powder impregnated. In the flexural strength test, the flexural strength of neat resin without alumina powder has a highest value of 257.7 MPa. The flexural modulus of ALMix-5 has a highest value of 12.06 GPa. Barcol hardness of ALMix-10 has a highest value of 51. We show that alumina powder leads to decreasing cracks on the surface and decreasing length area of delamination.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.16 no.7
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• pp.4388-4397
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• 2015

The purpose of this study was to research the property change of acrylic resins depending on the induced-beam change and research the improved physical property of dry-heat and microwave-cured dental place acrylic resin in order to develop the acrylic resins with the optimum characteristic. As a result of observing flexural rigidity, hardness and color difference, the dry-heat-cured specimens of Vertex RS and Paladent 20 showed ideal property at 5, 15, and 25 kGy irradiation. The microwave-cured specimens of Vertex RS and Paladent 20 showed ideal property at 5 kGy irradiation. The correlation analysis showed a positive correlation among ARD, flexural rigidity (0 418), E coefficient (0.675) and Barcol hardness (0 588). The radiation cure technology is helpful for relieving the contamination caused by the manufacture of polymer composite. It can significantly contribute to the fusion of ultra violet cure technology and nano technology and the improvement of mechanical property without giving effect to the workability of polymer.