• Title/Summary/Keyword: Analytical performance

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Quantitative Analysis of Lysophosphatidyl Choline (LPC) in Wheat Starch Lipids by High Performance Liquid Chromatography (고속액체크로마토그래피에 의한 밀전분 지방질에 함유된 리소레시친의 정량)

  • Shin, Myung Gon;Min, Bong Kee;Chang, Pahn Shick
    • Analytical Science and Technology
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    • v.5 no.3
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    • pp.339-343
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    • 1992
  • The content of lysophosphatidyl choline (LPC) in wheat starch lipids from six cultivar representing three classes of wheat was determined by a high performance liquid chromatography using UV-detection (HPLC-UV). The HPLC-UV assay had a sensitivity of LPC concentrations above $5{\mu}g/50{\mu}l$ and required 80 minutes per chromatogram.

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The Analytical Bias of Total Hydrocarbon (THC) Measurements in Relation to the Selection of Standard Gas Compound (총탄화수소의 계측에서 표준시료성분의 선택에 따른 오차 발생 연구)

  • Kim, Ki-Hyun
    • Journal of Korean Society for Atmospheric Environment
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    • v.26 no.4
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    • pp.449-452
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    • 2010
  • In this article, the performance of the THC analyzer was inspected using two different span gases of methane ($CH_4$) and propane ($C_3H_8$). To explore the effect of standard gas selection, MicroFID system was tested by the following procedures. Initially, the system is spanned by propane gas of 60 ppm (or 180 ppmC). The system is then run against methane standards prepared at 5 different concentrations of 200, 250, 300, 400, and 500 ppm. According to the suggestion of the KMOE's test procedure to use multiplying a factor of 3 (for propane), the resulting THC values derived by methane standards were systematically biased with ~500% error relative to true value. This paper discusses the interpretation procedures to obtain the least biased THC values for a given span set-up.

Analytical & Experimental Study on Microvibration Effects of Satellite (인공위성의 미소 진동 영향성에 관한 해석 및 실험적 연구)

  • Park, Geeyong;Lee, Dae-Oen;Yoon, Jae-San;Han, Jae-Hung
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2013.04a
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    • pp.533-539
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    • 2013
  • Number of components and payload systems installed in satellites were found to be exposed to various disturbance sources such as the reaction wheel assembly, the control moment gyro, coolers, and others. A micro-level of vibration can introduce jitter problems into an optical payload system and cause significant degradation of the image quality. Moreover, the prediction of on-orbit vibration effects on the performance of optical payloads during the development process is always important. However, analyzing interactions between subsystems and predicting the vibration level of the payloads is extremely difficult. Therefore, this paper describes the analytical and experimental approach to microvibration effects on satellite optical payload performance with integrated jitter analysis framework, micro vibration emulator and satellite structure testbed.

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Comparison of Extraction Procedures for the Determination of Capsaicinoids in Peppers

  • Jeon, Geonuk;Lee, Jun-Soo
    • Food Science and Biotechnology
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    • v.18 no.6
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    • pp.1515-1518
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    • 2009
  • The objective of this study was to compare 3 extraction methods including, solid phase extraction (SPE), acetonitrile extraction, and methanol extraction, for their usefulness as extraction methods to determine capsaicinoids. The determination of capsaicinoids in the extracts was carried out on a reverse-phased high performance liquid chromatography (HPLC) using a fluorescence detector. Three extraction methods, i.e., SPE, acetonitrile extraction, and methanol extraction were compared for the quantification of capsaicinoids using raw peppers and pepper powder. The highest analytical values were observed using methanol extraction and the lowest values using SPE. Also, the analytical method validation parameters such as accuracy, precision, limit of detection, limit of quantitation, and specificity were calculated to ensure the method's validity. This method provides a fast and accurate approach for the determination of capsaicinoids in peppers.

Comparative Study for Long Span Beams built up with Sub-marine High Strength Structural Steels at High Temperature using Analytical Method (고강도 용접구조용 강재 적용 장스팬 보부재의 해석적 내화성능 비교 연구)

  • Kwon, In-Kyu
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2016.05a
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    • pp.120-121
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    • 2016
  • Recently, the building has been changed into high-rise and long span and this yields a development of high performance structural steels in construction market. According to this effect, the SM 520 and the SM 570 were developed and utilized into steel building industry. However, the study for fire resistance of them were not done actively. In this study, to know and comparative the fire resistance performance of long span beams built up with high strength structural steels an analytical method is going to applied using mechanical and thermal properties at high temperature.

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The Performance Analysis of the Mobile Ad-Hoc Network Considering the Mobility of Nodes (이동성을 고려한 이동 애드혹 네트워크 성능분석)

  • Jeong, Seo-Kyun;Hur, Sun;Nam, Jin-Gyu
    • Journal of Korean Society of Industrial and Systems Engineering
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    • v.29 no.1
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    • pp.18-25
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    • 2006
  • In mobile ad-hoc networks(MANETs), nodes are mobile and network topology changes very frequently. The mobility of nodes does affect the system performance. There has been considerable attention on the mobility models, however, most work is confined to the simulation or test-bed. In this paper, we propose an analytical method to evaluate the performances of MANETs such as the average radio range dwell time of mobile nodes, link holding time, and transmission failure probability considering the node's mobility. In the proposed model, MANETs consist of the multi-hop and multicasting routing paths. A simulation is done to validate our proposed analytical model.

Analytical Model for Transfer Bond Performance of Prestressing Strands (PS 강선의 정착부착성능에 관한 해석 모델)

  • 유승룡
    • Magazine of the Korea Concrete Institute
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    • v.6 no.4
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    • pp.92-101
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    • 1994
  • A new analytical model is proposed to better understand the transfer bond performance in a prestressed pretensioned concrete beam. The transfer length is divided into an elastic and a plas tic zones in this model. The bond stress is assumed t.o increase proportionally with the slip t.o the lirnit of maximum bond stress within the elastic zone and remains at a constant maximum value wthin the plastic zone. Four main stress patterns: bond stress, slip, steel stress, and concrete stress distributions within the transfer length are obtained precisely. The total transfer length al\ulcornerd free-end slip obtained here give a close comparison to the test results by Cousins et al.

Exact Error and Outage Probability Formulas for Alamouti Space Time Code 2 $\times$ J

  • Kong, Hyung-Yun;Khuong, Ho-Van;Nam, Doo-Hee
    • Journal of Communications and Networks
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    • v.9 no.2
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    • pp.177-184
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    • 2007
  • Alamouti space-time code (STC) is a part of the UMTS-WCDMA standard. However, up to the best of our knowledge no exact closed-form outage and bit error probability (BEP) formulas for this famous code exists. Evaluating its performance through simulations is time-consuming and therefore, there should be analytical performance graphs to serve as a reference which are derived in this paper for coherently MPSK-modulated data. Additionally, analytical results take into account different channel fading levels from transmit antennas to receive ones.

Analytical Study on Performance Evaluation of Superdetonative Mode Ram Accelerator (초폭굉 모드 램가속기의 성능해석에 대한 이론적 연구)

  • Sung, Kunmin;Jeung, In-Seuck
    • Journal of the Korean Society of Combustion
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    • v.19 no.1
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    • pp.1-10
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    • 2014
  • An analytical study on performance evaluation of superdetonative mode ram accelerator was conducted for understanding the experimental result. The quasi-one dimensional continuum, momentum, energy equations were solved under the assumption of inviscid flow. It would be noticeable that experimental result could be analytically simulated with the assumptions of inlet shockwave, temperature dependent specific heat, and additional aluminum combustion due to ablation of aluminum projectile in superdetonative operation mode. The acceleration of ram accelerator was comparable to experimental result with the consideration of the additional aluminum combustion energy by ablation of projectile. As result, the experimental result with the aluminum projectile could be affected by heat of aluminum.

A New Model for Effectiveness Analysis of Government- supported R&D Institutes Evaluation System (정부출연연구기관 기관평가시스템 유효성 분석 모형: 유효성 분석을 위한 새로운 접근방법)

  • 이민형
    • Journal of Technology Innovation
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    • v.13 no.3
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    • pp.175-196
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    • 2005
  • This Paper examines analytic studies of the evaluation system used for evaluating government-supported R&D Institutes (GSRIs), and designs a new model for analyzing the evaluation system's effectiveness. The analytic models in existing studies use the meta evaluation and balanced scorecard (BSC) models. However, theses studies focused on the structure and elements of the evaluation system for examples, the appropriateness of the elements within the evaluation system and the balance of the evaluation index. Accordingly, the effectiveness of the GSRI evaluation system, that is, the evaluation's influence on GSRI performance improvement was not analyzed. This study uses the institution theory and contingency theory perspectives as related to government organization management to develop an analytical model of GSRI evaluation system effectiveness. The new model proposes an analytical approach for improving the effectiveness of the GSRI evaluation system in an institutionalized environment.

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