• 제목/요약/키워드: Aluminum particles

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Aluminum Nitride - Yttrium Aluminum Garnet 분말 특성과 플라즈마 용사 코팅층의 미세조직 (Microstructural Evolution of Aluminum Nitride - Yttrium Aluminum Garnet Composite Coatings by Plasma Spraying from Different Feedstock Powders)

  • 소웅섭;백경호
    • 한국재료학회지
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    • 제21권2호
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    • pp.106-110
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    • 2011
  • A high thermal conductive AlN composite coating is attractive in thermal management applications. In this study, AlN-YAG composite coatings were manufactured by atmospheric plasma spraying from two different powders: spray-dried and plasma-treated. The mixture of both AlN and YAG was first mechanically alloyed and then spray-dried to obtain an agglomerated powder. The spray-dried powder was primarily spherical in shape and composed of an agglomerate of primary particles. The decomposition of AlN was pronounced at elevated temperatures due to the porous nature of the spray-dried powder, and was completely eliminated in nitrogen environment. A highly spherical, dense AlN-YAG composite powder was synthesized by plasma alloying and spheroidization (PAS) in an inert gas environment. The AlN-YAG coatings consisted of irregular-shaped, crystalline AlN particles embedded in amorphous YAG phase, indicating solid deposition of AlN and liquid deposition of YAG. The PAS-processed powder produced a lower-porosity and higher-hardness AlN-YAG coating due to a greater degree of melting in the plasma jet, compared to that of the spray-dried powder. The amorphization of the YAG matrix was evidence of melting degree of feedstock powder in flight because a fully molten YAG droplet formed an amorphous phase during splat quenching.

알루미늄 전극의 용출에 따른 해성점토의 개량에 관한 실험적 연구 (A Experimental Study on Improvement of Marine Clay through the Electrolytic Leaching Effect in Aluminum Electrode)

  • 김종윤;윤명석;정승용;김수삼
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2006년도 춘계 학술발표회 논문집
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    • pp.1173-1180
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    • 2006
  • In this study, aluminum electrodes were put in marine clay which was taken from the south coast in Korea to increase the undrained shear strength by inducing the densification and cementation between clay particles and precipitates which were developed by electric decomposition in an electrode. To raise the cementation rate and reduce treatment time, high electric current (2.5A) was applied in each electrode at a semi-pilot scale soil box with marine clay. After the tests, the undrained shear strength was measured at designated points using a static cone penetration test device and sampling was conducted simultaneously in order to measure water content, pH and electric conductivity which would be the key for configuring the cementation effects indirectly. In the results of electric decomposition in aluminum electrode, the measured shear strength was increased considerably compared to the initial shear strength because of the cementation effect between iron ions and soil particles.

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알루미나입자로 강화된 알루미늄합금 복합재료의 미세조직과 기계적 성질 (Microstructure and Mechanical Properties of Aluminum Alloy Composites Strengthened with Alumina Particles)

  • 오창섭;한창석
    • 한국재료학회지
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    • 제23권3호
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    • pp.199-205
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    • 2013
  • The mechanical properties and microstructures of aluminum-matrix composites fabricated by the dispersion of fine alumina particles less than $20{\mu}m$ in size into 6061 aluminum alloys are investigated in this study. In the as-quenched state, the yield stress of the composite is 40~85 MPa higher than that of the 6061 alloy. This difference is attributed to the high density of dislocations within the matrix introduced due to the difference in the thermal expansion coefficients between the matrix and the reinforcement. The difference in the yield stress between the composite and the 6061 alloy decreases with the aging time and the age-hardening curves of both materials show a similar trend. At room temperature, the strain-hardening rate of the composite is higher than that of the 6061 alloy, most likely because the distribution of reinforcements enhances the dislocation density during deformation. Both the yield stress and the strain-hardening rate of the T6-treated composite decrease as the testing temperature increases, and the rate of decrease is faster in the composite than in the 6061 alloy. Under creep conditions, the stress exponents of the T6-treated composite vary from 8.3 at 473 K to 4.8 at 623 K. These exponents are larger than those of the 6061 matrix alloy.

Pulse도금법에 의한 Ag주입 양극산화 알루미늄 합금의 항균특성에 관한 기초연구 (A Study on the Antibacterial Properties of Ag Electropulsed Anodized Aluminium Alloy)

  • 임기영;기준서;장용석;이우민;윤정모
    • 한국재료학회지
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    • 제16권10호
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    • pp.639-646
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    • 2006
  • Over the last two decades, microbiologically influenced corrosion (MIC) of metallic materials has received considerable attention due to its serious effects on industrial field. In this context, it is important to devise control methods which inhibit biofilm formation on various metallic compounds and are compatible with environment. It was change of various conditions (duty cycle, current density, $AgNO_3$ concentration and pH) for injection of Ag particles in anodized Aluminum alloy pore using pulsed current. Optimal condition was obtained by means of FE-SEM, ICP analysis etc. The antibacterial metal's specimen were manufactured under optimal condition and this specimen were tested the antibacterial characterization and anticorrosion characterization. In result of test, we can confirmed that the antibacterial characterization and anticorrosion characterization of the specimens of injected Ag particles in anodized Aluminum alloy pore using pulsed current were better than the anodized Aluminum alloy specimens.

하이브리드 로켓용 파라핀/알루미늄 연료의 알루미늄 입자크기에 따른 열적·유변학적 특성 연구 (Thermal and Rheological Characteristics of Paraffin Based Fuel on Aluminum Particle Size for Hybrid Rocket Application)

  • 한승주;김진곤;문희장;김준형;고승원
    • 한국추진공학회지
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    • 제22권2호
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    • pp.108-114
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    • 2018
  • 본 연구에서는 유입후퇴율 거동에 대한 정성적인 예측을 위하여 나노 및 마이크로 알루미늄 입자가 10 wt.% 첨가된 파라핀/알루미늄 연료에 대해 열적특성 및 유변학적 특성에 관한 분석을 수행하였다. 측정결과, 알루미늄 입자 혼합연료에 대하여 열적특성 대비 유변학적 특성에 입자첨가 여부 및 입자크기의 영향이 존재함을 확인하였다. 또한, 열적특성에 나타난 변화에 비해 유변학적 특성에 나타난 변화가 유입후퇴율에 큰 영향을 미치고 민감함을 확인하였다.

고체추진제 연소 중 알루미늄 응집 모델 연구 (Study of Aluminum Agglomeration Model During Solid Propellant Combustion)

  • 윤지상;이국진;김대유;박남호;고승원;윤웅섭
    • 한국추진공학회지
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    • 제23권2호
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    • pp.78-86
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    • 2019
  • 복합 고체추진제에 포함된 금속 연료인 알루미늄은 산화피막에 의해 연소 표면에서 점화, 연소되지 못하고 일부분 녹아 주위 알루미늄 입자들과 응집한다. 추진제 성능 평가 및 설계를 위해 응집된 입자의 크기 및 분포를 예측하기 위해 모델링을 수행하였으며 직접 실험을 통해 응집된 입자의 크기 및 분포를 비교 및 검증하였다. 예측값은 실험과 동일하게 압력에 따라 평균직경이 감소하는 경향을 나타내었으나 압력이 증가할수록 오차가 증가하였다. 응집 입자 분포그래프는 최고점에서의 직경이 일치했지만 체적 분률에서 차이가 나타났다.

질화알루미늄 나노분말의 부착과 이를 활용한 초소수성 표면 제작 (Deposition of aluminum nitride nanopowders and fabrication of superhydrophobic surfaces )

  • 이광석;최헌주;조한동
    • 한국표면공학회지
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    • 제57권1호
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    • pp.49-56
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    • 2024
  • Superhydrophobic surfaces have been expected to be able to provide considerable performance improvements and introduce innovative functions across diverse industries. However, representative methods for fabricating superhydrophobic surfaces include etching the substrate or attaching nanosized particles, but they have been limited by problems such as applicability to only a few materials or low adhesion between particles and substrates, resulting in a short lifetime of superhydrophobic properties. In this work, we report a novel coating technique that can achieve superhydrophobicity by electrophoretic deposition of aluminum nitride (AlN) nanopowders and their self-bonding to form a surface structure without the use of binder resins through a hydrolysis reaction. Furthermore, by using a water-soluble adhesive as a temporary shield for the electrophoretic deposited AlN powders, hierarchical aluminum hydroxide structures can be strongly adhered to a variety of electrically conductive substrates. This binder-free technique for creating hierarchical structures that exhibit strong adhesion to a variety of substrates significantly expands the practical applicability of superhydrophobic surfaces.

철강(鐵鋼) 및 알루미늄재료(材料)의 기계적(機械的) 성능(性能)에 미치는 TMT(thermomechanical treatment)의 영향 (The Effect of TMT on Mechanical Properties of Steel & Aluminum Alloy)

  • 소명기
    • 산업기술연구
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    • 제1권
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    • pp.53-60
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    • 1981
  • A study has been performed on the effect of TMT(thermomechanical treatment) on the mechanical properties of steel and aluminum alloys. Improvement of the mechanical properties on steel by HTMT is due to refinement of prior austenite grain size, martensite lath size and the distribution of fine carbide precipitates and on aluminum alloy by ITMT is due to grain size refinement, homogeneous distribution of small second phase particles and retardation of the recrystallization.

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Template-free Synthesis and Characterization of Spherical Y3Al5O12:Ce3+ (YAG:Ce) Nanoparticles

  • Kim, Taekeun;Lee, Jin-Kyu
    • Bulletin of the Korean Chemical Society
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    • 제35권10호
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    • pp.2917-2921
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    • 2014
  • Cerium-activated yttrium aluminate ($Y_3Al_5O_{12}:Ce^{3+}$) exhibiting a garnet structure has been widely utilized in the production of light emitting diodes (LEDs) as a yellow emitting phosphor. The commercialized yttrium aluminum garnet (YAG) phosphor is typically synthesized by a solid-state reaction, which produces irregular shape particles with a size of several tens of micrometers by using the top-down method. To control the shape and size of particles, which had been the primary disadvantage of top-down synthetic methods, we synthesized YAG:Ce nanoparticles with a diameter of 500 nm using a coprecipitation method under the atmospheric pressure without the use of template or special equipment. The precursor particles were formed by refluxing an aqueous solution of the nitrate salts of Y, Al, and Ce, urea, and polyvinylpyrrolidone (55 K) at $100^{\circ}C$ for 12 h. YAG:Ce nanoparticles were formed by the calcination of precursor particles at $1100^{\circ}C$ for 10 h under atmospheric conditions. The phase identification, microstructure, and photoluminescent properties of the products were evaluated by X-ray powder diffraction, scanning electron microscopy, absorption spectrum and photoluminescence analyses.

분말피복압연법에 의해 제조된 (SiC)p/Al 복합재료의 미세조직 및 기계적 성질 (Microstructure and Mechanical Properties of (SiC)p/Al Composite Fabricated by a Powder-in Sheath Rolling Method)

  • 이성희;이충효
    • 한국분말재료학회지
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    • 제11권3호
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    • pp.259-264
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    • 2004
  • Aluminum based metal matrix composite reinforced with SiC particles was fabricated by the powder-in sheath rolling method. A stainless steel tube with outer diameter of 12 mm and wall thickness of 1mm was used as a sheath. Mixture of aluminum powder and SiC particles of which volume content was varied from 5 to 20vol.% was filled in the tube by tap filling and then rolled to 75% reduction at ambient temperature. The rolled specimen was sintered at 56$0^{\circ}C$ for 0.5hr. The tensile strength of the (SiC)$_{p}$/Al composite increased with the volume content of SiC particles, and at 20vol.% it reached a maximum of 100㎫ which is 1.6 times higher than unreinforced material. The elongation decreased with the volume content of $Al_{2}$O$_{3}$ particles. The mechanical properties of the (SiC)$_{p}$/Al composite fabricated by the powder-in sheath rolling is compared with that of (Al$_{2}$O$_{3}$)$_{p}$/Al composite by the same process.ess.