• Title/Summary/Keyword: Accelerated Deterioration Test

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The effect of glazing and aging on the surface properties of CAD/CAM resin blocks

  • Tekce, Neslihan;Fidan, Sinan;Tuncer, Safa;Kara, Dilan;Demirci, Mustafa
    • The Journal of Advanced Prosthodontics
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    • v.10 no.1
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    • pp.50-57
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    • 2018
  • PURPOSE. To investigate the effect of accelerated aging on surface properties of glazed CAD/CAM resin blocks using a 2D surface profilometer and a 3D non-contact optical profilometer. MATERIALS AND METHODS. Three types of CAD/CAM resin restorative materials, LAVA Ultimate (3M ESPE, St Paul, MN, USA), VITA Enamic (Vita Zahnfabrik H. Rauter, Bad $S\ddot{a}ckingen$, Germany), and Cerasmart (GC Corparation, Tokyo, Japan) were used for this study. CAD/CAM blocks were cut in 3-mm thickness slabs and divided into three groups; Group 1: control group (specimens polished with 600 grit SCI paper); Group 2: specimens sandblasted, silanized, and glazed with Optiglaze Color (GC); Group 3: glazed specimens subjected to 5000 thermocycles (n=15). The surface roughness ($R_a$ and $R_z$) was evaluated using a profilometer and a 3D scanning instrument. Data were analyzed using two-way ANOVA and Tukey's post- hoc test (P<.05). RESULTS. LAVA, VITA, and Cerasmart exhibited statistically similar $R_a$ and $R_z$ values for each group (P>.05). For VITA and Cerasmart, the specimens in Group 1 exhibited significantly higher $R_a$ values than Group 2 (P<.05). Group 1 ($0.502R_a$), Group 2 ($0.384R_a$), and Group 3 ($0.431R_a$) exhibited statistically similar $R_a$ values for LAVA (P=.062). After 5000 thermocycles, surface roughness values did not change significantly for glazed LAVA, VITA, and Cerasmart (P>.05). CONCLUSION. Glaze material Optiglaze Color makes CAD/CAM resin surfaces smooth and glazed CAD/CAM surfaces seem resistant to deterioration under 5000 thermocycles.

A Study of Weathering Characteristics of Cretaceous Granite in Kimhae Area due to Artificial Weathering Processes (인공풍화과정에 의한 김해지역 백악기 화강암의 풍화특성에 관한 연구)

  • Um, Jeong-Gi
    • Tunnel and Underground Space
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    • v.22 no.1
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    • pp.32-42
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    • 2012
  • It is very difficult to capture the weathering characteristics of rock because of limitation caused by time and space. A new scheme of experiment that includes physical and chemical weathering processes was implemented on Cretaceous granitic rock samples from Kimhae area to investigate the variations of geomechanical properties of deteriorated rocks due to artificial weathering processes. The seismic velocity was found to decrease with increasing artificial weathering cycle. Effective porosity and absorption tend to increase with artificial weathering processes. The amount of deterioration of rock samples depend on pre-test degree of weathering. Effective porosity, absorption and seismic velocity can be used as the measure of weathering characteristics of granite in the study area. Weathering is accelerated by combined effect of physical and chemical weathering processes. The new experimental methodology conducted in this study has strong capability to analyze the weathering characteristics of rocks.

Effects of Thermal Aging of Natural Rubber Bearing on Seismic Performance of Bridges (천연고무받침의 열 노화가 교량 내진성능에 미치는 영향)

  • Oh, Ju;Jung, Hie-Young
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.33 no.3
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    • pp.855-864
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    • 2013
  • The dynamic characteristics of natural rubber bearings, which are used as isolator, are dependent on the main rubber's dynamic behaviors and nonlinear properties. Rubber materials tend to undergo an aging process under the influence of mechanical or environmental factors, so they inevitably end up facing damage. A main cause of aging like this is known to be oxidization, which occurs through the heat of reaction at high temperatures. Accordingly, in this study an accelerated thermal aging test was carried out in order to compare the characteristic values of the bearings before and after thermal aging occurs. As a result of this experiment, it was found that a thermal aging phenomenon could have some effects on shear stiffness, energy absorption, and equivalent damping coefficients of the bearings. Furthermore, a deterioration in the dynamic properties of the natural rubber bearings caused by the thermal aging was applied to an actual bridge and then the effects of such thermal aging on the seismic performance of the bridge were also compared and analyzed based on numerical analysis. As a result of this analysis, it was found that the changes in the basic properties of the natural rubber bearings caused by the thermal aging bring only a minor effect on the seismic performance of bridges.

Non Destructive Technique for Steel Corrosion Detection Using Heat Induction and IR Thermography (열유도 장치와 적외선 열화상을 이용한 철근부식탐지 비파괴 평가기법)

  • Kwon, Seung Jun;Park, Sang Soon
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.16 no.2
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    • pp.40-48
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    • 2012
  • Steel corrosion in concrete is a main cause of deterioration and early failure of concrete structures. A novel integration of electromagnetic heat induction and infrared (IR) thermography is proposed for nondestructive detection of steel corrosion in concrete, by taking advantage of the difference in thermal characteristics of corroded and non-corroded steel. This paper focuses on experimental investigation of the concept. An inductive heater is developed to remotely heat the embedded steel from concrete surface, which is integrated with an IR camera. Concrete samples with different cover depths are prepared. Each sample is embedded with a single rebar in the middle, resulting an identical cover depth from the front and the back surfaces, which enable heat induction from one surface and IR imaging from the other simultaneously. The impressed current (IC) method is adopted to induce accelerated corrosion on the rebar. IR video images are recorded during the entire heating and cooling periods. The test results demonstrate a clear difference in thermal characteristics between corroded and non-corroded samples. The corroded sample shows higher rates of heating and cooling than those of the non-corroded sample. This study demonstrates a potential for nondestructive detection of rebar corrosion in concrete.

Durability Evaluation of Cathode Open-type Proton Exchange Membrane Fuel Cells Stacks (Cathode 개방형 고분자연료전지 스택 내구성 평가)

  • Yoo, Donggeun;Kim, Hyeonsuck;Oh, Sohyeong;Park, Kwon-Pil
    • Korean Chemical Engineering Research
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    • v.60 no.1
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    • pp.12-19
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    • 2022
  • Cathode open-type PEMFC (Proton Exchange Membrane Fuel Cells) stacks, which are widely used in small transport-type PEMFC, have a problem with poor durability. Through the accelerated durability test of the 13-cell PEMFC stack, we tried to find the cause of the degradation of the stack and to contribute to the improvement of the durability of the cathode open stack. A hydrogen/air boundary is formed during start-up/shut-down (SU/SD) due to the structural problem of the cathode open stack in which the cathode is open to the atmosphere and it is difficult to maintain airtightness, thereby deteriorating the cathode. In this study, it was possible to evaluate the durability in a relatively short time by reducing the 54% of the initial performance by repeating SU/SD 1,800 times on the cathode open stack. After dismantling the stack, each cell was divided into two and the performance was analyzed. Overall, the anode outlet MEA, which facilitates air inflow, showed more severe electrode deterioration than the inlet MEA, confirming that the hydrogen/air boundary formation during SU/SD is the main cause of degradation.

An Experimental Study on the Resistance to Penetration of Harmful Ions in Surface Coatings Material Containing Organic Corrosion inhibitor (유기계 방청제를 혼입한 표면피복재의 유해이온 침투저항에 관한 실험적 연구)

  • Ryu, Hwa-Sung;Shin, Sang-Heon;Lee, Han-Seung
    • Journal of the Korea Institute of Building Construction
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    • v.17 no.2
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    • pp.157-166
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    • 2017
  • In general, carbonation and chlorine ions are the most harmful causes of deterioration of concrete structures. Recently, a method has been developed to control the corrosion of rebar in concrete containing chloride by impregnating a Surface coating material with a inhibitor. In this study, accelerated carbonation and differential thermogravimetric analysis (TG-DTA) and CASS tests were carried out to evaluate the characteristics of Surface coatings containing Organic Corrosion inhibitors which are excellent in corrosion inhibition and fix degradation causes $CO_2$ and $Cl^-$. As a result of the experiment, TG-DTA analysis and accelerated carbonation showed that $CO_2$ was directly reacted with amine derivative in concrete by the incorporation of Organic Corrosion inhibitor. In other words, $CO_2$ was immobilized and carbonation inhibition effect was confirmed. In addition, in the CASS test, the specimen coated with the Surface coating material containing the Organic Corrosion inhibitor with $Cl^-$ fixing property showed no corrosion until the 28th day and had excellent performance in preventing corrosion of a rebar by the chloride ion.

Dehydration of Foamed Fish(Sardine)-Starch Paste by Microwave Heating 2. Quality Stability and Shelf-life of the Product (어육(정어러) 발포건조제품가공에 관한 연구 2. 제품저장중의 품질변화와 저장기간)

  • LEE Kang-Ho;LEE Byeong-Ho;SONG Dong-Suck;You Byeong-Jin;LEE Byeong-Ho;SUH Jae-Soo;JEA YOi-Guan;RYU Hong-Soo
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.15 no.4
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    • pp.291-297
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    • 1982
  • In this part of the studies on dielectric dehydration of foamed fish-starch paste, qualify stability and shelf-life of the product of which the preparation formula and processing conditions were described in previous report (Lee et al, 1982) were determined by means of accelerated reaction test. The product was stored for 50 days under the conditions of temperatures at 35, 45, and $55^{\circ}C$ in steady state and various water activities of 0.44, 0.52, 0.65, and 0.75, respectively. The loss of available lysine, extent of TBA value, and development of browning during the storage were measured and reaction kinetically analysed to assess quality stability and shelf-life of the product for the storage at room temperature of $25^{\circ}C$. Extent of browning was accelerated with the increase of water activity and temperature marking the time to reach a limit of color and flavor deterioration, or to reach brown color density of 0.17 O.D./g at 420 nm, 106 days at aw=0.44, $35^{\circ}C$, and 41 days at aw=0,65, $55^{\circ}C$, These reaction rates resulted in a prediction of shelf-life, 130 to 110 days in the storage at aw=0.44 to 0.75, $25^{\circ}C$. The quality limit assessed by TBA values and sensory evaluation of rancidity was 87 days at aw=0.44, $35^{\circ}C$, and 30 days at aw=0.75, $55^{\circ}C$ which gave a predicted shelf-life, 128 to 113 days . at aw=0.44 to 0.75, $25^{\circ}C$ storage.

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Evaluation of Time-Dependent Chloride Resistance in HPC Containing Fly Ash Cured for 1 Year (1년 양생 조건의 Fly Ash를 혼입한 고성능 콘크리트의 시간의존적 염해저항성 평가)

  • Yoon, Yong-Sik;Kwon, Seung-Jun
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.22 no.4
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    • pp.52-59
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    • 2018
  • To control chloride attacks which is a representative deterioration in RC(Reinforced Concrete) structures, many studies have been conducted. Above all, a method using mineral admixture was known to be effective for corrosion protection. In this study, durability test about chloride attacks was carried out for concrete specimens containing FA(Fly Ash)-representative concrete mineral admixture and OPC concrete specimens considering 3 different levels of W/B(Water to Binder). Accelerated chloride diffusion coefficient tests referred to Tang's method, total passed charge tests referred to ASTM C 1202, and compressive strength tests based on KS F 2405 were performed at each target age day. Also, based on previous studies of 28 days, time-parameter which is a key parameter for diffusion behavior is evaluated and its relations with compressive strength at the age of 365 days is evaluated. After the age of 49 days, chloride resistance of FA concrete is much improved than that of OPC concrete, which arose out of stable hydrates due to pozzolan reaction of fly ash. Time-parameter of FA concrete is evaluated to be about 1.5 times larger than that of OPC concrete. Also, time-parameter of FA concrete has a linearly decreasing relation while that of OPC concrete has a linearly increasing relation with compressive strength development.

Revision of Repair Materials Performance Requirement for Concrete Structures (콘크리트 구조물 단면복구공사 보수재료 품질기준개선)

  • Lee, Il Keun;Kim, Ki Hwan;Kim, Hong Sam;Yun, Sung Hwan;Kim, Woo Seok
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.43 no.1
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    • pp.9-20
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    • 2023
  • For highway concrete structures, the deterioration of the structure is accelerated due to the increase in the use of deicing materials, and sectional repair work is being frequently carried out to restore performance. However, after the repair work, re-damage such as cracks, delamination, and poor bond performance is exhibited in the repaired sectional area. In this study, overseas repair material requirements were first analyzed, and present domestic requirements were improved repair material performance through field surveys of common concrete structures, laboratory experiments, and test construction on a disused concrete bridge. In addition, performancebased quality requirements were presented so that all materials that meet the required performance can be applied, and different test methods for each material were unified into concrete test methods for consistent test results analysis. The considered performance requirements were compression strength, bending strength, and bond strength for structural properties, and length change rate, crack resistance, thermal expansion coefficient, and elasticity coefficient were for dimensional behavior. For resistance to chloride penetration resistance and freeze-thaw resistance were presented as durability. The proposed requirements for concrete repair materials are expected to contribute to the improvement of the quality of concrete sectional repair work in Korea.

Dry-heat Treatment Effect for Seed Longevity Prediction in Rice Germplasm (벼 유전자원의 저장수명 예측을 위한 건열처리 효과)

  • Na, Young-Wang;Baek, Hyung-Jin;Choi, Yu-Mi;Lee, Sok-Young;Lee, Jung-Ro;Chung, Jong-Wook;Park, Yong-Jin;Kim, Seok-Hyeon
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.59 no.3
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    • pp.230-238
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    • 2014
  • The purpose of this study was to develop the cost-effective and efficiency seed longevity prediction method of rice (Oryza sativa L.) germplasm for viability monitoring. To find an optimum predicting method for rice seed longevity at genebank, an accelerated ageing (AA) test, a controlled deterioration (CD) test and a dry-heat treatment (DHT) were conducted to the four groups of rice germplasm based on ecotype, such as Indica, Japonica, Javanica and Tongil type. Among the three artificial aging treatments, the dry-heat treatment of 36 hours at $90^{\circ}C$ is suggested as a routine predictive test method of rice germplasm longevity at a genebank. The distribution of germination rate on 3,066 accessions which conserved 26.5 years at $4^{\circ}C$ showed similar trend with the result of distribution by dry-heat treatment at $90^{\circ}C$ on 36 hours using 106 accessions of rice selected samples which composed four ecotype groups. The results show that the dry-heat treatment affect not only predicting the rice seed longevity but also determining effective interval for monitoring germination of rice germplasm in genebanks.