• Title/Summary/Keyword: ASTM method

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Properties Characterization of the Hydrophilic Inorganic Film as Function of Coating Thickness (코팅 두께에 따른 친수성 무기 필름의 특성 분석)

  • Joung, Yeunho;Choi, Won Seok;Shin, Yongtak;Lee, Minji;Kim, Heekon
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.26 no.6
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    • pp.425-428
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    • 2013
  • In this paper, we present a novel hydrophilic coating material (Wellture Finetech, Korea) which can be utilized as a coating layer for anti-contamination for electrical and electronic system. The coating material was deposited on 4 inch silicon wafer with several different film thickness. The film thickness was controlled by spin coating speed. After curing of the film, we have scratched by permanent marker to check self-cleaning property of the film. Also we have executed several mechanical tests of the films. As the spin coating speed is increased, the film thickness was thinned from 230 nm to 125 nm. Contact angle of the film was lowered from $30^{\circ}$ to $12^{\circ}$ as the spin coating speed is increased from 700 to 2,500 rpm. On permanent marker scratched film surface coated at 1,000 rpm, we have poured regular city water to investigate self cleaning property of the film. The scratches were gradually separated from the film surface due to super-hydrophilicity of the film. Hardness of spin coated film was 9H measured by ASTM D3363 method. and adhesion of all film was 5B tested by ASTM D3359 method. Also, to get exact hardness value of the film, we have utilized a nano-indenter. As spin speed is increased, the hardness of film was increased from 3 GPa to 5 GPa.

Characteristic Analysis of Functional Nano-coating Films Synthesized according to the Annealing Ambient and Fabrication of Anti-pollution PV Module (기능성 나노코팅 박막의 열처리 분위기에 따른 특성분석 및 오염방지 태양광 모듈제작)

  • Kang, Hyunil;Shin, Seung Kwon;Kim, Hyungchul;Lim, Yonnsik;Yoo, Youngsik;Joung, Yeun-Ho;Kim, Junghyun;Choi, Won Seok
    • The Transactions of the Korean Institute of Electrical Engineers P
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    • v.64 no.3
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    • pp.182-186
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    • 2015
  • We investigated that effects of annealing ambient on the characteristics of functional nano thin film synthesized on glass substrate. The functional nano thin films were annealed by using rapid thermal annealing (RTA) equipment in vacuum, oxygen and nitrogen ambient, respectively. The hardness of the functional nano thin films were measured by a standard hardness testing method (ASTM D3363) such as a H-9H, F, HB and B-6B pencil (Mitsubishi, Japan). Also, the adhesion of the functional nano thin films were measured by a standard adhesion testing method (ASTM D3359) using scotch tape (3M, Korea). The contact angle of the functional nano thin films was measured by a contact angle analyzer (Phoenix 300 Touch, S.E.O.). The optical property of functional nano thin films was measured via UV-visible spectroscopy (S-3100, Scinco).

Development and Calibration of a Plate Type Eddy Current Standard (평판형 와전류 표준 시험편의 개발 및 교정)

  • Kim, Young-Joo;Kim, Young-Gil;Ahn, Bong-Young;Yoon, Dong-Jin
    • Journal of the Korean Society for Nondestructive Testing
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    • v.27 no.5
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    • pp.393-397
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    • 2007
  • Eddy current standard including an artificial slot for the calibration of absolute type surface probe was fabricated. Developed eddy current standard has the electric conductivity and dimensions, and contains artificial slot as established in ASTM E 1629. The width and depth of artificial slot are 0.1 mm and 0.5 mm respectively. This slot was only possible to measure the depth on the two side edges, and impossible for the middle part with general measurement tools. The ultrasonic test method was applied for measuring depth of the middle part of the artificial slot in the standard. Using this method the dimension could be measured successfully with uncertainty about $15\;{\mu}m$. Calibration of eddy current standard for the absolute probe can be performed by this technique.

Antifoaming Properties for Aliphatic Antifoamer Formula (지방족 소포제 조성물의 소포특성)

  • Jeong, Noh-Hee;Park, Gor-Soon;Park, Joon-Suk;Nam, Ki-Dae
    • Journal of the Korean Applied Science and Technology
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    • v.16 no.2
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    • pp.147-153
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    • 1999
  • As main components of antifoamers, we were used fatty alcohols, fatty acid and fatty acid esters. Then the antifoaming properties on the particle size distribution, temperature and concentration for antifoamers was measured by Air Injection Method of ASTM under 1L/min air flow rate condition, and was measured surface tensions and emulsifying power of antifoamers. The antifoaming properties on the particle size distribution of antifoamers showed excellent antifoaming properties in the range of emulsion particle size from 5.5 to 6.8${\mu}m$. Surface tensions on the $10^{-2}$wt% aqueous solution of antifoamers was $33{\sim}34$ mN/m. And emulsifying power of fatty alcohol antifoamers showed good.

Evaluation of Adhesion and Electrical Properties of CNT/PU Topcoat with Different CNT Weight Fraction for Aircraft (탄소나노튜브의 함량에 따른 항공기용 탄소나노튜브/폴리우레탄 탑코트의 접착 및 전기적 특성 평가)

  • Kim, Jong-Hyun;Shin, Pyeong-Su;Kim, So-Yeon;Park, Joung-Man
    • Composites Research
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    • v.33 no.1
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    • pp.1-6
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    • 2020
  • Dispersion and electrical resistance (ER) properties of polyurethane (PU) type topcoat were evaluated using carbon nanotube (CNT) with different CNT weight fraction. CNT was dispersed in PU type topcoat using ultra sonication dispersion method. CNT/PU topcoat was coated on carbon fiber reinforced epoxy composite (CFRC) surface using gravity feed spraying method. Static contact angles of CFRC and CNT/PU topcoat were performed using 4 types of solvents to calculate the work of adhesion between CNT/PU topcoat and CFRC surface. Surface resistance of CNT added PU topcoat was measured to determine CNT dispersion. Adhesion property between CNT/PU topcoat and CFRC was determined via cross hatch cutting test based on ASTM D3359. The optimized condition of CNT weight fraction was found.

Fatigue Crack Growth Behavior of Powder Metallurgical Nickel-based Superalloy using DCPD Method at Elevated Temperature (DCPD법을 이용한 분말야금 니켈기 초내열합금의 고온 피로균열진전거동)

  • Na, Seonghyeon;Oh, Kwangkeun;Kim, Hongkyu;Kim, Donghoon;Kim, Jaehoon
    • Journal of the Korean Society of Propulsion Engineers
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    • v.20 no.2
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    • pp.11-17
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    • 2016
  • Powder metallurgy nickel based superalloy has been used in a high temperature part of turbine engine for airplane. The fatigue crack growth behavior was investigated using CT specimens for the materials at room temperature(R.T.), $600^{\circ}C$ and $700^{\circ}C$. The direct current potential drop(DCPD) method suggested by ASTM E647 was used to measure the crack length during fatigue crack growth at various stress ratios. The fatigue crack growth rate at R=0.5 was faster than that at R=0.1 for all temperature conditions and increased with the increase of stress ratio and temperature. Fractography was conducted for analysis of fracture mechanism.

Design for Improving the Loss Factor of Composite with Sandwich Structure (샌드위치 구조를 가지는 복합재의 손실계수 향상을 위한 설계)

  • Lee, C. M.;Jeon, G.S.;Kang, D.S.;Kim, B.J.;Kim, J.H.;Kang, M.H.;Seo, Y.S.
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.26 no.3
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    • pp.235-241
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    • 2016
  • Underwater weapon system is required to structurally strong material, since as it is directly exposed to external shock. It should also be using the lightweight material in order to take advantage of buoyancy. Composite materials meet these requirements simultaneously. Particularly in the case of submarine, composite materials are widely used. It is important to have a high strength enough to be able to withstand external shock, but it is also important to attenuate it. In a method for the shock damping, viscoelastic damping materials are inserted between the high strength composite material as a sandwich structure. Shock attenuation can be evaluated in the loss factor. In ASTM(American Society of Testing Materials), evaluation method of the loss factor of cantilever specimens is specified. In this paper, mode tests of the cantilever are performed by the ASTM standard, in order to calculate the loss factor of the viscoelastic damping material by the specified expression. Further, for verifying of the calculated loss factor, mode test of compound beams is carried out. In addition, the characteristics of the material were analyzed the effect on the loss factor.

Determination of Permissible Shear Stresses on Vegetation Mats by Soil Loss Evaluation (토양 손실 평가에 의한 식생매트의 허용 소류력 결정)

  • Lee, Du Han;Rhee, Dong Sop;Kim, Myounghwan
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.14 no.11
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    • pp.5956-5963
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    • 2013
  • By the activation of environment-friendly river works, application of vegetation mats is increasing, however, evaluation techniques for hydraulic stability of vegetation mats are not presented. This study is conducted to develop the objective test method for vegetation mats. Two kind of vegetation mats are tested by the real scale experiments, and hydraulic quantities are measured and analyzed to evaluate acting shear stresses. To evaluate soil loss, Terrestrial 3D LiDAR measurement is conducted and soil loss index are calculated from changes of bed elevation. Quantified evaluation for permissible shear stresses is conducted by graphical method for acting shear stresses and soil loss index. By the results of precision survey, changes of sub soil are limited to local range in stable cases and relatively large changes of sub soil which is similar to natural river bed are detected in unstable cases. From the study, evaluation of permissible shear stresses by ASTM D 6040 is avaliable in the failure mechanism and failure criteria by soil loss index.

Approximate Solution for Constant Velocity of Archimedean Spiral for Abrasion Testing of Rock Cutting Tools (암석공구 마모시험을 위한 아르키메데스 나선의 등속도 운동 근사해 조사)

  • Kang, Hoon;Kim, Dae-ji;Song, Changheon;Oh, Joo-Young;Cho, Jung-Woo
    • Tunnel and Underground Space
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    • v.30 no.3
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    • pp.181-192
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    • 2020
  • Pin-on-disk test is a suggested abrasion testing method by ASTM (American Society for Testing and Materials). This briefly illustrated the Archimedean spiral motion of a pin type specimen on a disk. To apply this method to rock cutting tools, a constant linear velocity (CLV) is precisely maintained during the test. We defined the two velocity vectors (RPM and horizontal speed) which connected to the resultatnt velocity. We derived a differential equations for the two parameters under CLV condition. It was difficult to find a exact solution. Previous literatures had been reviewed, and an approximate solution was investigated. We mathematically simulated the result for a certain parameter, and examine the accuracy of the solution.

Evaluation of Corrosion Behavior of Railway Axle Material (RSA1) in Seawater (해수환경에서의 차축소재(RSA1) 부식특성 평가)

  • Choi, Dooho;Seo, Sung-il
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.16 no.8
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    • pp.5039-5044
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    • 2015
  • In this study, we evaluated corrosion behavior of a common rolling stock axle material, RSA1, in seawater. 3-electrode electrochemical cell experiment was conducted using artificial sea water, fabricated according to ASTM-D1141 set by American Society for Testing and Materials, where the corrosion current density and corrosion rate were determined to be $18.3{\mu}A/cm2$ and 0.217 mm/yr, respectively, by employing potentiodynamic test method and impedance spectroscopy method. Considering the fact that life time of railway car is ~25 years, the expected corrosion layer depth is 5mm. Constant-current corrosion test was conducted to accelerate the corrosion process, to reach corrosion periods of 1,3 and 4 years based on Faraday's law, followed by tension tests where the reduced specimen gauge cross-section was re-measured for stress calculation. While no apparent corrosion-related changes in mechanical properties were observed in the elastic regime, the reduction in ductility of the material was found to be increased as the corrosion period increased. The results of this study are expected to be basic corrosion data for the design of rolling stock axles, which will be operated in the sea water environment.