• The Journal of Korean Institute of Communications and Information Sciences
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• v.37 no.5C
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• pp.429-436
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• 2012

In this paper, an RFID system for the automatic preparation system of positron emission tomography (PET) radiopharmaceuticals is developed. Since the preparation system uses radioactive isotope, the preparation system is generally placed in lead-shielded hot-cell. Disposable cassettes including tubes and valves are used in the preparation system, since they are easily contaminated by radioactivity during preparation of radiopharmaceuticals. Currently, a system for preventing re-use of the cassette and managing the information about the preparation precess and result independently from the PC which control the preparation system is highly required for preventing danger from the radiation accident. Since RFID can store and re-write relatively large amount of information, it is suitable for the purpose. However, it is hard to read multiple cassettes' information using antennas installed on the metallic surfaces with current RFID systems. For the problem, we improve RFID system in two directions. First, the interface of the RFID reader is changed then it is possible that multiple readers can be daisy-chained. Also, antenna is tuned while inserting in a metallic coated antenna case, then the effect from the metallic surface of the preparation system is minimized. The test result using the developed system shows that the developed RFID system can read multiple tags using the antennas which are attached on the metallic surface.

• Applied Chemistry for Engineering
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• v.33 no.5
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• pp.459-465
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• 2022

A pitch coating method was proposed for the purpose of improving the electrochemical properties of natural graphite. The synthesis conditions of pitch coating were optimized via measuring electrochemical properties of pitch-coated graphite anodes. As the synthesis temperature increased, the thermal stability was improved in addition to an increase in the softening point and residual carbon weight. However, the synthesis temperature of 430 ℃ resulted in the synthesis of a large amount of NI (NMP Insoluble) due to excessive condensation reaction. As the surface uniformity and coating thickness increased due to high thermal stability, the initial coulombic efficiency and rate capability of the pitch-coated graphite were improved. However, the graphite coated with the pitch containing excessive NI showed lower electrochemical properties than the uncoated graphite. NI had low dispersibility and formed spheres after heat treatment, so it formed the heterogeneous and thicker SEI layer. The optimum conditions for forming a uniform surface and an appropriate coating layer were investigated.

• Journal of the Korean Electrochemical Society
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• v.25 no.3
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• pp.95-104
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• 2022

The development of non-flammable all-solid-state batteries (ASSLBs) has become a hot topic due to the known drawbacks of commercial lithium-ion batteries. As the possibility of applying sulfide solid electrolytes (SSEs) for electric vehicle batteries increases, efforts for the low-cost mass-production are actively underway. Until now, most studies have used high-energy mechanical milling, which is easy to control composition and impurities and can reduce the process time. Through this, various SSEs that exceed the Li⁺ conductivity of liquid electrolytes have been reported, and expectations for the realization of ASSLBs are growing. However, the high-energy mechanical milling method has disadvantages in obtaining the same physical properties when mass-produced, and in controlling the particle size or shape, so that physical properties deteriorate during the full process. On the other hand, wet chemical synthesis technology, which has advantages in mass production and low price, is still in the initial exploration stage. In this technology, SSEs are mainly manufactured through producing a particle-type, solution-type, or mixed-type precursor, but a clear understanding of the reaction mechanism hasn't been made yet. In this review, wet chemical synthesis technologies for SSEs are summarized regarding the reaction mechanism between the raw materials in the solvent.

• The Proceedings of the Korean Institute of Illuminating and Electrical Installation Engineers
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• v.7 no.3
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• pp.27-33
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• 1993

This paper presents the &tal controller for driving high frequency voltage fed PWM inverter that carrier frequency is over 2OkHz.We analyzed the conventional PWM to select a proper PWM pattern. as the result, obtained PWM pattern of the controller in which asynchronus staircase sinusoidal waveform is used as reference signal, and variable carrier ratio method was used for PWM control. The PWM controller is designed by fully digital method. Especially, Thk proposed controller is consisted of 8 bit one-chip microprocessor and digital logic. the former is for arithmetic and data processing, and the latter is for PWM pattern synthesis. Therefore, The responsibility and controllability is improved. Also, Data processing capability is improved using proper program to output modulation index with 9 bits. Circuits configuration of digital controller are made up of one chip 8051 and EPLD, and its controllability is tested by operating voltage fed inverter. Harmonics and current waveform is evaluated and analyzed for the voltage fed inverter system.

• Journal of the Korean Institute of Intelligent Systems
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• v.15 no.5
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• pp.527-532
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• 2005

In this paper, we proposed an adaptive fuzzy sliding control for unknown nonlinear systems using estimation of bounds for approximation errors. Unknown nonlinearity of a system is approximated by the fuzzy logic system with a set of IF-THEN rules whose consequence parameters are adjusted on-line according to adaptive algorithms for the purpose of controlling the output of the nonlinear system to track a desired output. Also, using assumption that the approximation errors satisfy certain bounding conditions, we proposed the estimation algorithms of approximation errors by Lyapunov synthesis methods. The overall control system guarantees that the tracking error asymptotically converges to zero and that all signals involved in controller are uniformly bounded. The good performance of the proposed adaptive fuzzy sliding mode controller is verified through computer simulations on an inverted pendulum system.

• Journal of the Korean Geotechnical Society
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• v.19 no.5
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• pp.291-299
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• 2003

The effect of temperature and soil confining stress on geosyntheic creep behaviour was studied by performing the temperature dependent confined creep tests for HDPE geogrid and geomembrane specimen. The visco-elastic creep coefficients of the geosynthetics were evaluated by the test results and it was proposed that the simple expressions for the instantaneous and limit creep strain of geosynthetics was considered as a function of temperature and confining stress on geosynthetics. Based on the time-temperature superposition principle, a master curve has been drawn for extrapolating tensile creep strains to longer time intervals(1$\times$10 $^7$min.∼1$\times$10$^{10}$min.). By using this master curves, the shift factors which can be used in establishing master curve considering confining stress on geosynthetics were carried out. Each tests was performed during 8,000∼12,000 min., with temperature ranging between 5$^{\circ}C$ and 4$0^{\circ}C$ and with confining stress ranging between 0 t/$m^2$ and 9 t/$m^2$.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.16 no.11
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• pp.7838-7843
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• 2015

In this study, metformin hydrochloride for first choice of type 2 diabetes patient is administered relatively high dose, 1000 to 2000 mg orally once a day, and had very high water solubility, so it make difficult to swallow tablet to requires high amount of sustained release agent. To overcome these challenges, we used novel metformin salts had relatively low water solubility to minimize sustaining excipient for small size of dosage form. six novel metformin salts were synthesized by making metformin free form under reaction with NaOH and adding acid salts. we confirmed metformin stearate had the lowest water solubility and showed half drug release in dissolution study at 12hour. In conclusion, novel metformin salts had low water solubility can be used to reduce the size of sustained metformin tablet for improving patient compliance.

• Korean Chemical Engineering Research
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• v.50 no.4
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• pp.729-732
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• 2012

Herein we report the in-situ synthesis and direct decoration of chalcogenide naoparticles (NPs) onto multiwalled carbon nanotubes (MWCNTs) through an ionic liquid-assisted sonochemical method (ILASM). The as-obtained MWCNT/$BMimBF_4$/CdTe, MWCNT/$BMimBF_4$/ZnTe and MWCNT/$BMimBF_4$/ZnSe nanocomposites were characterized by TEM images and EDS spectra. In particular, the morphologies of nanocomposites such as bump-like, rough, and smooth core-shell structures were strongly influenced by the type of precursors and the interactions with MWCNT. This synthetic strategy opens a new way to directly synthesize and deposit semiconducting NPs (s-NPs) onto CNTs, which consist of binary components obtained from two precursors with different reaction rates.

• The Journal of Korean Institute of Electromagnetic Engineering and Science
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• v.19 no.5
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• pp.533-540
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• 2008

In the sum and difference pattern synthesis problem of the equi-spaced monopulse tracking linear array antennas, an efficient numerical approach to deriving the relative excitation current weights of antenna elements is presented for the desired patterns. This method is based on the optimum perturbation of null points which are inherent to the Schelkunoffs polynomial representing the pattern array factor. Accordingly, opposite to the conventional method in which the excitation weights are directly optimized, this method is advantageous in that the patterns with the desired individual sidelobe levels(SLLs) and the corresponding excitation weights are easily synthesized by the control of null points. Furthermore, it is showed that two types of difference patterns can be synthesized as imposing the different initial values of null points in the optimization process. The proposed method is numerically validated by synthesizing the patterns with the arbitrary SLLs and substituting the extracted results into the array factor equation.

• Journal of the Korean Ceramic Society
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• v.34 no.10
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• pp.1083-1091
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• 1997

As one of the chemical powder fabrication methods, the powder preparation method by using oxalate has the following advantages; (1) easy to control the chemical stoichiometry, (2) easy to fabricate homogeneous and fine particles, and (3) easy to be thermaly decomposed at low temperature. In the present study, the initial morphology and size distribution of the powder were controlled and the homogeniaty was improved. By carefully controlling the pH with NH4OH, the Bi(Pb)-Sr-Ca-Cu-O superconducting powders were prepared and investigated for their properties. The microstructures and the superconducting properties of the pelletized samples were investigated. Also, the microstructures and electrical properties of the samples prepared by tape casting method were investigated. The fabricated powders were spherical with less than 400 nm, but most of them were agglomerated to be 1~3 ${\mu}{\textrm}{m}$ in size. The critical temperature of the pelletized sample annealed at 84$0^{\circ}C$ for 72 hours in air was 110K. And the critical currents of annealed samples in air prepared by tape casting process for 24 hours and 72 hours were 0.6 A (Jc=600A/$\textrm{cm}^2$) and 1.9A (Jc=1, 900A/$\textrm{cm}^2$) respectively.