• Title/Summary/Keyword: 합성율

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Physiological Activities of Hot Water Extract from Ailanthus altissima (가죽나무(Ailanthus altissima) 열수 추출물의 생리활성)

  • Lee, Yang-Suk
    • Food Science and Preservation
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    • v.14 no.2
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    • pp.170-176
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    • 2007
  • In this study, extract of Ailanthus altissimawere prepared using hot water under high pressure. The extract were examined for election donating ability (EDA), superoxide dismuase (SOD)-like activity, nitrite scavenging ability (NSA), xanthine oxidase inhibition levels, and tyrosinase inhibition ability. The EDA, using the 1,1-diphenyl-2-picrylhydrazyl method of root extract was 91.25% at 1.0mg/mL. The SOD-like activity of leaf extract was highest at 49.07% and the NSA was 93.33% at pH 1.2, and 85.40% at pH 3.0. The xanthine oxidase inhibitory levels of extracts of A. altissima roots, stems, and leaves were 92.09 97.44% when the extract were tested at 2.0mg/mL. The highest tyrosinase inhibition levels obtained from loot extract were 67.38% at 2.0mg/mL and 63.97% at 0.1mg/mL.

Synthesis and Electrochemical Properties of Porous Li4Ti5O12 Anode Materials (기공구조로 제조된 Li4Ti5O12 음극활물질의 전기화학적 특성)

  • Seo, Jin-Seong;Na, Byung-Ki
    • Korean Chemical Engineering Research
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    • v.57 no.6
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    • pp.861-867
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    • 2019
  • $Li_4Ti_5O_{12}$ is a promising next-generation anode material for lithium-ion batteries due to excellent cycle life, low irreversible capacity, and little volume expansion during charge-discharge process. However, it has poor charge capacity at high current density due to its low electrical conductivity. To improve this weakness, porous $Li_4Ti_5O_{12}$ was synthesized by sol-gel method with P123 as chelating agent. The physical characteristics of as-prepared sample was investigated by XRD, SEM, and BET analysis, and electrochemical properties were characterized by cycle performance test, cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS). $Li_4Ti_5O_{12}$ synthesized by 0.01mol ratio of P123/Ti showed most unified particle size, high specific surface area, and relatively high porosity. EIS analysis showed that depressed semicircle size was remarkably reduced, which suggested resistance value in electrode was decreased. Capacity in rate performance showed 178 mAh/g at 0.2C, 170 mAh/g at 0.5C, 110 mA/h at 5C, and 90 mAh/g at 10C. Capacity retention also showed 99% after rate performance.

Long-range multiple-input-multiple-output underwater communication in deep water (심해에서의 장거리 다중입출력 수중통신)

  • Kim, Donghyeon;Kim, Daehwan;Kim, J.S.;Hahn, Joo Young
    • The Journal of the Acoustical Society of Korea
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    • v.40 no.5
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    • pp.417-427
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    • 2021
  • Long-range communication in deep waters must overcome the low data rate due to limited bandwidth. This paper presents the performance of Multiple-Input-Multiple-Output (MIMO) system to increase the data rate. In MIMO system, communication performance is degraded by crosstalk between users and an adaptive passive Time Reversal Processing (TRP) is widely used to eliminate this. In October 2018, long-range underwater acoustic communication experiment was conducted in deep water (1,000 m ~) off the east of Pohang, South Korea. During the experiment, a vertical line array was utilized and communication signals modulated by binary phase shift keying and quadrature phase shift keying with a symbol rate of 512 sps were transmitted. To generate MIMO communication signals, received signals from ranges of 26 km and 30 km is synthesized. Compared to the conventional passive TRP, the adaptive passive TRP eliminates the crosstalk between users and achieves error-free performance with an increase of output signal-to-noise ratio. Therefore, two users separated by 4 km in range achieves an aggregate data rate of 1,024 symbols/s.

Extraction of Total Flavonoids from Lemongrass Using Microwave Energy: Optimization Using CCD-RSM (마이크로웨이브 에너지를 이용한 레몬그라스로부터 플라보노이드 성분의 추출: CCD-RSM을 이용한 최적화)

  • Yoo, Bong-Ho;Jang, Hyun Sick;Lee, Seung Bum
    • Applied Chemistry for Engineering
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    • v.32 no.2
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    • pp.168-173
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    • 2021
  • In this study, we measured total flavonoids after extracting the total flavonoids from lemongrass which is known to have a high content of antioxidant ingredients when using microwave energy. Also, optimal extraction conditions of active ingredients using central composite design-response surface methodology (CCD-RSM) were presented. Both ultrapure water and alcohol were used as extraction solvents and the volume ratio of ethanol/ultrapure water, microwave irradiation time, and microwave irradiation power were set as independence variables. And the extraction yield and total flavonoids were measured. The optimal extraction conditions using CCD-RSM were the volume ratio of ethanol/ultrapure water = 56.3 vol.%, the microwave irradiation time = 6.1 min, and the microwave irradiation power = 574.6 W. We could also obtain expected results of yield = 17.2 wt.% and total flavonoids = 44.7 ㎍ QE/mL dw under the optimum conditions. The comprehensive satisfaction degree of this formula was 0.8562. The P-value was calculated for the yield of 0.037 and the total flavonoids content of 0.002. The average error from actual experiments established for the verification of conclusions was lower than 2.5%. Therefore, a high favorable level could be obtained when the CCD-RSM was applied to the optimization of extraction process.

Applicability Evaluation of Spatio-Temporal Data Fusion Using Fine-scale Optical Satellite Image: A Study on Fusion of KOMPSAT-3A and Sentinel-2 Satellite Images (고해상도 광학 위성영상을 이용한 시공간 자료 융합의 적용성 평가: KOMPSAT-3A 및 Sentinel-2 위성영상의 융합 연구)

  • Kim, Yeseul;Lee, Kwang-Jae;Lee, Sun-Gu
    • Korean Journal of Remote Sensing
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    • v.37 no.6_3
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    • pp.1931-1942
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    • 2021
  • As the utility of an optical satellite image with a high spatial resolution (i.e., fine-scale) has been emphasized, recently, various studies of the land surface monitoring using those have been widely carried out. However, the usefulness of fine-scale satellite images is limited because those are acquired at a low temporal resolution. To compensate for this limitation, the spatiotemporal data fusion can be applied to generate a synthetic image with a high spatio-temporal resolution by fusing multiple satellite images with different spatial and temporal resolutions. Since the spatio-temporal data fusion models have been developed for mid or low spatial resolution satellite images in the previous studies, it is necessary to evaluate the applicability of the developed models to the satellite images with a high spatial resolution. For this, this study evaluated the applicability of the developed spatio-temporal fusion models for KOMPSAT-3A and Sentinel-2 images. Here, an Enhanced Spatial and Temporal Adaptive Fusion Model (ESTARFM) and Spatial Time-series Geostatistical Deconvolution/Fusion Model (STGDFM), which use the different information for prediction, were applied. As a result of this study, it was found that the prediction performance of STGDFM, which combines temporally continuous reflectance values, was better than that of ESTARFM. Particularly, the prediction performance of STGDFM was significantly improved when it is difficult to simultaneously acquire KOMPSAT and Sentinel-2 images at a same date due to the low temporal resolution of KOMPSAT images. From the results of this study, it was confirmed that STGDFM, which has relatively better prediction performance by combining continuous temporal information, can compensate for the limitation to the low revisit time of fine-scale satellite images.

Heat Risk Assessment of Wood Coated with Silicone Compounds (실리콘 화합물로 도포된 목재의 열위험성 평가)

  • Jin, Eui;Chung, Yeong-Jin
    • Fire Science and Engineering
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    • v.33 no.2
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    • pp.9-19
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    • 2019
  • Experiments on the combustion characteristics of untreated wood specimens and those treated with four types of silicone compounds were carried out using a cone calorimeter according to the ISO 5660-1 standard. 3-Aminopropyltrimethoxysilane (APTMS), 3-(2-aminoethylamino) propylmethyldimethoxysilane (AEAPMDMS), and 3-(2-aminoethylamino) propyltrimethoxysilane (AEAPTMS) were used as the silane compounds. The flame retardants were synthesized with sodium silicate and amino silane compounds. The measured time to ignition after combustion at an external heat flux of $50kW/m^2$ was 9 s to 11 s. Time to ignition was marked with a delayed value in the 3 s to 5 s range. The peak heat release rate ($HRR_{peak}$) was reduced by 5 to 20% compared with the uncoated specimen, and AEAPMDMS showed the highest initial fire risk. The total heat release (THR) was decreased by 1 to 22%. Compared to the untreated specimen, the fire performance index (FPI) of the specimens coated with silicone sol compounds increased by 1.5 to 2.2 fold. The fire growth index (FGI) of the AEAPMDMS specimen was increased by 30% and the others were decreased by 93 to 94%. Therefore, the fire risk of wood coated with silicone compounds was improved in terms of the heat risk properties.

Electrochemical Performance of Pitch coated Nano Silicon Sheets / Graphite Composite as Anode Material (피치로 코팅된 Nano Silicon Sheets/Graphite 음극복합소재의 전기화학적 특성)

  • Lee, Tae Heon;Lee, Jong Dae
    • Korean Chemical Engineering Research
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    • v.59 no.4
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    • pp.487-492
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    • 2021
  • In this study, the electrochemical properties of pitch coated silicon sheets/graphite anode materials were investigated. Using NaCl as a template, silicon sheets were prepared through the stöber method and the magnesiothermic reduction methode. In order to synthesize the anode composite, the silicon sheets and graphite were combined with SDBS. The pitch coated silicon sheets/graphite was synthesized using THF as a solvent for the anode material composite. The physical properties of the prepared anode composites were analysed by XRD, SEM, EDS and TGA. The electrochemical performances of the prepared anode composites were performed by the current charge/discharge, rate performance, cyclic voltammetry and EIS tests in the electrolyte LiPF6 dissolved solvents (EC:DMC:EMC=1:1:1 vol%). As the silicon composition of silicon sheets/graphite composite material increased, the discharge capacity also increased, but the cycle stability tended to decrease. The anode material of pitch coated silicon sheets/graphite composite (silicon sheets:graphite=3:7 weight ratio) showed the initial discharge capacity of 1228.8 mAh/g and the capacity retention ratio of 77% after 50 cycles. From these results, it was found that the cycle stability of pitch coated silicon sheets/graphite was improved.

Development of antimicrobial edible films and coatings: a review (항균 가식성 필름/코팅 개발 현황)

  • Kim, Su Yeon;Min, Sea C.
    • Food Science and Industry
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    • v.50 no.2
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    • pp.37-51
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    • 2017
  • Food packaging strategies have steadily improved with increasing demand for improved food safety, convenience, and shelf life. The development of edible film has been hailed as a technology substituting packaging using synthetic plastics. There has been a surge for research to develop antimicrobial edible films and coatings that can increase microbiological safety while preserving foods. This review addresses recent results that are useful in advancing and extending research into antimicrobial edible films. In this review, we suggest the trend of the development of antimicrobial edible film/coatings by outlining edible film materials, antimicrobial substances, antimicrobial and physical properties of the films, commercial antimicrobial edible films, and methods to statistically predict the efficacy of antimicrobial edible film/coatings, reported in recent studies.

Implementation of RSA modular exponentiator using Division Chain (나눗셈 체인을 이용한 RSA 모듈로 멱승기의 구현)

  • 김성두;정용진
    • Journal of the Korea Institute of Information Security & Cryptology
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    • v.12 no.2
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    • pp.21-34
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    • 2002
  • In this paper we propos a new hardware architecture of modular exponentiation using a division chain method which has been proposed in (2). Modular exponentiation using the division chain is performed by receding an exponent E as a mixed form of multiplication and addition with divisors d=2 or $d=2^I +1$ and respective remainders r. This calculates the modular exponentiation in about $1.4log_2$E multiplications on average which is much less iterations than $2log_2$E of conventional Binary Method. We designed a linear systolic array multiplier with pipelining and used a horizontal projection on its data dependence graph. So, for k-bit key, two k-bit data frames can be inputted simultaneously and two modular multipliers, each consisting of k/2+3 PE(Processing Element)s, can operate in parallel to accomplish 100% throughput. We propose a new encoding scheme to represent divisors and remainders of the division chain to keep regularity of the data path. When it is synthesized to ASIC using Samsung 0.5 um CMOS standard cell library, the critical path delay is 4.24ns, and resulting performance is estimated to be abort 140 Kbps for a 1024-bit data frame at 200Mhz clock In decryption process, the speed can be enhanced to 560kbps by using CRT(Chinese Remainder Theorem). Futhermore, to satisfy real time requirements we can choose small public exponent E, such as 3,17 or $2^{16} +1$, in encryption and verification process. in which case the performance can reach 7.3Mbps.

Synthesis and Electrochemical Properties of Zn and Al added LiNi0.85Co0.15O2 Cathode Materials (Zn와 Al을 첨가한 LiNi0.85Co0.15O2 양극활물질의 제조 및 전기화학적 특성평가)

  • Kim, Su-Jin;Seo, Jin-Seong;Na, Byung-Ki
    • Korean Chemical Engineering Research
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    • v.59 no.1
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    • pp.42-48
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    • 2021
  • Zn and Al added LiNi0.85Co0.15O2 cathode materials were synthesized to improve electrochemical properties and thermal stability using a solid-state route. Crystal structure, particle size and surface shape of the synthesized cathode materials was measured using XRD (X-ray diffraction) and SEM (scanning electron microscopy). CV (cyclic voltammetry), first charge-discharge profiles, rate capability, and cycle life were measured using battery cycler (Maccor, series 4000). Strong binding energy of Al-O bond enhanced structure stability of cathode material. Electrochemical properties were improved by preventing cation mixing between Li+ and Ni2+. Large ion radius of Zn+ increased lattice parameter of NC cathode material, which meant unit-cell volume was expanded. NCZA25 showed 80% of capacity retention at 0.5 C-rate during 100 cycles, which was 12% higher than that of NC cathode. The discharge capacity of NCZA25 showed 104 mAh/g at 5 C-rate. NCZA25 achieved 36 mAh/g more capacity than that of NC cathod. NCZA25 cathode material showed excellent rate capability and cycling performance.