• Title/Summary/Keyword: 오토클레이브

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Engineering Performance of Extruded Fly Ash Cement Panel with Bottom Ash (잔골재로서의 바텀애시를 사용한 플라이애시 시멘트 압출경화체의 공학적 특성)

  • Lee, Myeong-Jin;Kim, Jin-Man;Han, Dong-Yeop;Choi, Duck-Jin;Lee, Keun-Woo
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.3 no.3
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    • pp.252-260
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    • 2015
  • The aim of this research is providing the fundamental data for treating and recycling the byproducts by using the wet processed bottom ash as a fine aggregate replacement for cement-based extruded panel. Although the cement-based extruded panel was used mainly as a cladding component with its high strength and outstanding durability, it was hardly spread because of low economic feasibility due to the high cost of additives or fibers which were used to achieve 14 MPa of flexural strength as a cladding material. As a solution of this drawback, by the previous research, it was possible to replace cement by fly ash up to 80 % by decreasing quality criteria with restricting the application to indoor purpose. In this research, based on the previous research, by using the bottom ash as a replacement of fly ash, improvement of shape retention performance is tried. As a result of the experiment on evaluating the optimum content and PSD of bottom ash, as the fineness modulus and content of bottom ash was increased, the extruding performance was decreased and penetration resistance was increased. Additionally, the optimum content and the maximum particle size was found as 20 %, and 0.3 mm, respectively.

Optimum Mix of Extrusion panel Using Low Energy Curing Admixture (LA) based on Ground Granulated Blast-Furnace Slag and Ladle Furnace Slag (고로슬래그와 환원슬래그를 기반으로 한 저에너지양생용 결합재를 사용한 압출성형패널의 최적배합)

  • Kim, Ha-Seog;Baek, Dae-Hyun;Lee, Sea-Hyun
    • Resources Recycling
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    • v.24 no.2
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    • pp.13-22
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    • 2015
  • $CO_2$ emitted from building materials and construction materials industry reaches about 67 million tons, which occupy about 30 % of $CO_2$ emitted from the construction field. Controls on the use of consumed fossil fuels and reduction of emission gases are essential for the reduction of $CO_2$ in the construction area as we reduce the second and third curing to emit $CO_2$ in the construction materials industry. Accordingly, this study applied the low energy curing admixture (hereinafter "LA") to the extruded panels to observe the physical properties, depending on the mixing amount of fiber, type of fiber and mixing ratio of fiber. The type of fiber did not appear to be a main factor to affect strength, while the LA mixing ratio and mixing amount of fiber appeared to be major factors to affect strength. Especially, the highest strength was developed when the LA mixing ratio was 40%, whereas the test object with the mixing ratio of 50% resulted in the decrease of strength. In addition, it appeared that the mixing ratio of fiber greatly affected flexural strength and strength increased as the mixing ratio increased.

Pre-treatment condition and Curing method for Fabrication of Al 7075/CFRP Laminates (Al 7075/CFRP 적층 복합재료 제조를 위한 전처리 조건과 경화방법 연구)

  • 이제헌;김영환
    • Composites Research
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    • v.13 no.4
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    • pp.42-53
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    • 2000
  • A study has been made to establish an optimum condition in the surface treatment and curing method that is important for the fabrication of Al 7075/CFRP laminates. PAA(Phosphoric Acid Anodizing) provided a good adhesive strength and FPL(Sulfuric / Sodium Dichromate Acid Etching) had a similar adhesive strength with PAA. On the other hand, the poor adhesive strength was shown on vapor degrease and CAA(Chromic Acid Anodizing). By using the atomic force microscope(AFM), it was found that the PAA oxide surface obviously had a greater degree of microroughness as compared to vapor degrease, CAA and FPL treated surfaces. These results support the concept of a mechanical interlocking of the adhesive with-in the oxide pores as the predominant adhesion mechanism. In curing methods, the adhesive strength of co-curing method was higher than that of secondary curing method. With respect to stability of specimen shape, the secondary curing method was better than co-curing method. DMA(Dynamic Mechanical Analysis) test revealed $T_g$ in curing times over 60 min is nearly same, so it is estimated they will have similar degree of curing and joint durability in using FM300M adhesive film.

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Physical and Chemical Properties of Waste Concrete Powders Originated from the Recycling Process of Waste Concrete (폐콘크리트의 재활용 공정에서 발생되는 폐콘크리트 미립분의 물리.화학적 특성)

  • Kim, Jin Man;Kang, Cheol;Kim, Ha Suk
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.4 no.2
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    • pp.82-89
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    • 2009
  • According to the great city development and the rapid growth of redevelopment project, waste concrete emission has been increased. Waste concrete powder is one of the by-product originated from the recycling of the waste concrete. The more making high quality recycled aggregate to use aggregate for concrete, the more waste concrete powder is producted relatively. Therefore, to realize the total recycling of waste concrete, development of recycling technology for waste concrete powder need very much. This technical note present the discharged process and the various properties of waste concrete powder. As the results, on the average, the maximum particle-size of waste concrete powder is less than $600{\mu}m$, and oven-dry density is less than $2.5g/cm^3$. And waste concrete powder contains more than 50% of $SiO_2$, 30% of CaO and 10% of $Al_2O_3$. Thus qualities of waste concrete powder is lower than those of high quality raw material for concrete. However, if it is processed by grading to the purpose, it will be used as resource of raw materials for construction field.

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Effect of limestone addition on mechanical properties of ceramic tiles with fly ash (플라이애시가 첨가된 도자타일 성능에 석회석 함량이 미치는 효과)

  • Lee, Jin-Wook;Han, Kyu-Sung;Hwang, Kwang-Taek;Kim, Jin-Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.28 no.6
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    • pp.256-262
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    • 2018
  • A great amount of fly ash, which is a waste from a thermal power plant, has not been appropriately recycled until now. Landfill of flay ash causes environmental pollution and enormous economic costs. In this study, manufacturing of architectural ceramic tile was investigated replacing fly ash with clay raw material. The properties of porcelain tile was analyzed after manufacturing porcelain tile with mineral based glaze and fast firing process. In particular, the effect of the fly ash addition on the properties of ceramic tile was investigated by increasing the amount of limestone addition. Porcelain tile with fly ash showed excellent bending strength, water absorption, warping and abrasion resistance. However, a significant decrease in durability was observed through the autoclave test. Addition of limestone increased the water absorption, twisting and hydration expansion of the ceramic tile, but it was confirmed that the durability of the ceramic tile with fly ash was greatly improved. In conclusion, recycled architectural ceramic tiles, which can meet domestic construction standards, could be manufactured with the addition of fly ash and limestone.

A Study on the Fatigue Strength of the 3-D Reinforced Composite Joints (3-차원 보강 복합재 체결부의 피로강도 특성 연구)

  • Kim, Ji-Wan;An, Woo-Jin;Seo, Kyeong-Ho;Choi, Jin-Ho
    • Composites Research
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    • v.35 no.5
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    • pp.322-327
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    • 2022
  • Composite lap joints have been extensively used due to their excellent properties and the demand for light structures. However, due to the weak mechanical properties in the thickness direction, the lap joint is easily fractured. various reinforcement methods that delay fracture by dispersing stress concentration have been applied to overcome this problem, such as z-pinning and conventional stitching. The Z-pinning is reinforcement method by inserting metal or carbon pin in the thickness direction of prepreg, and the conventional stitching process is a method of reinforcing the mechanical properties in the thickness direction by intersecting the upper and lower fibers on the preform. I-fiber stitching method is a promising technology that combines the advantages of both z-pinning and the conventional stitching. In this paper, the static and fatigue strengths of the single-lap joints reinforced by the I-fiber stitching process were evaluated. The single-lap joints were fabricated by a co-curing method using an autoclave vacuum bag process and I-fiber reinforcing effects were evaluated according to adherend thickness and stitching angle. From the experiments, the thinner the composite joint specimen, the higher the I-fiber reinforcement effect, and Ifiber stitched single lap joints showed a 52% improvement in failure strength and 118% improvement in fatigue strength.

Test Evaluation of a Linerless Composite Propellant Tank Using the Composite Collapsible Mandrel (복합재 분리형 맨드릴을 이용한 라이너 없는 복합재 추진제 탱크에 대한 시험 평가)

  • Seung Yun Rhee;Kwangsoo Kim;Young-Ha Yoon;Moo-Keun Yi;Hee Chul Kim
    • Composites Research
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    • v.36 no.2
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    • pp.132-139
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    • 2023
  • A linerless composite propellant tank was designed and manufactured by using the carbon fiber-reinforced composite materials which have superior strength-to-weight ratio in order to reduce weight of the tank. In this research, we designed a sub-scale composite propellant tank with a diameter of 800 mm to withstand an MEOP of 1.7 MPa. We manufactured the boss of the tank by using the same composite materials to reduce the thermal expansion difference between the boss and the secondary-bonded composite layers of the barrel in the cryogenic environment. We used the collapsible mandrel to manufacture the tank without any liner. The mandrel was made from epoxy-based composite tooling prepregs to reduce weight of the mandrel. We manufactured the test tanks by laying up the carbon fiber fabric prepregs manually on the mandrel and then applying the autoclave cure process. We performed a proof test, a helium tightness test, a repeated pressurization test, and a burst test in room temperature. The test results demonstrate that the proposed design and manufacture process satisfies all strength requirements as well as an anti-leakage requirement.

Annealing Effects on Properties of ZnO Nanorods Grown by Hydrothermal Method (수열합성법으로 성장된 산화아연 나노막대의 특성 및 열처리 효과)

  • Jeon, Su-Min;Kim, Min-Su;Kim, Ghun-Sik;Cho, Min-Young;Choi, Hyun-Young;Yim, Kwang-Gug;Kim, Hyeoung-Geun;Lee, Dong-Yul;Kim, Jin-Soo;Kim, Jong-Su;Lee, Joo-In;Leem, Jae-Young
    • Journal of the Korean Vacuum Society
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    • v.19 no.4
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    • pp.293-299
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    • 2010
  • Vertically aligned ZnO nanorods on Si (111) substrate were prepared by hydrothermal method. The ZnO nanorods on spin-coated seed layer were synthesized at $140^{\circ}C$ for 6 hours in autoclave and were thermally annealed in argon atmosphere for 20 minutes at temperature of 300, 500, $700^{\circ}C$. The effects of the thermal annealing on the structural and optical properties of the grown on ZnO nanorods were investigated by X-ray diffraction (XRD), field-emission scanning electron microscopy (FE-SEM), photoluminescence (PL). All the ZnO nanorods show a strong ZnO (002) and weak (004) diffraction peak, indicating c-axis preferred orientation. The residual stress of the ZnO nanorods is changed from compressive to tensile by increasing annealing temperature. The hexagonal shaped ZnO nanorods are observed. The PL spectra of the ZnO nanorods show a sharp near-band-edge emission (NBE) at 3.2 eV, which is generated by the free-exciton recombination and a broad deep-level emission (DLE) at about 2.12~1.96 eV, which is caused by the defects in the ZnO nanorods. The intensity of the NBE peak is decreased and the DLE peak is red-shifted due to oxygen-related defects by thermal annealing.

Next Generation Lightweight Structural Composite Materials for Future Mobility Review: Applicability of Self-Reinforced Composites (미래모빌리티를 위한 차세대 경량구조복합재료 검토: 자기강화복합재료의 적용 가능성)

  • Mi Na Kim;Ji-un Jang;Hyeseong Lee;Myung Jun Oh;Seong Yun Kim
    • Composites Research
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    • v.36 no.1
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    • pp.1-15
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    • 2023
  • Demand for energy consumption reduction is increasing according to the development expectations of future mobility. Lightweight structural materials are known as a method to reduce greenhouse gas emissions and improve energy efficiency. In particular, fiber reinforced polymer composite (FRP) is attracting attention as a material that can replace existing metal alloys due to its excellent mechanical properties and light weight. In this paper, industrial applications and research trends of carbon fiber reinforced composites (CFRP, carbon FRP) and self-reinforced composites (SRC) were reviewed based on the reinforcement, polymer matrix, and manufacturing process. In order to overcome the expensive process cost and long manufacturing time of the epoxy resin-based autoclave method, which is mainly used in the aircraft field, mass production of CFRP-applied electric vehicles has been reported using a high-pressure resin transfer molding process including fast-curing epoxy. In addition, thermoplastic resin-based CFRP and interface enhancement methods to solve the recycling issue of carbon fiber composites were reviewed in terms of materials and processes. To form a perfect matrix-reinforcement interface, which is known as the major factor inducing the excellent mechanical properties of FRP, studies on SRC impregnated with the same matrix in polymer fibers have been reported. The physical and mechanical properties of SRC based on various thermoplastic polymers were reviewed in terms of polymer orientation and composite structure. In addition, a copolymer matrix strategy for extending the processing window of highly drawn polypropylene fiber-based SRC was discussed. The application of CFRP and SRC as lightweight structural materials can provide potential options for improving the energy efficiency of future mobility.