• Title/Summary/Keyword: 열분석적 특성

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The study of optimal reduced-graphene oxide line patterning by using femtosecond laser pulse (펨토초 레이저 펄스를 이용한 환원된 그래핀의 최소 선폭 패턴 구현에 관한 연구)

  • Jeong, Tae-In;Kim, Seung-Chul
    • Journal of the Korea Convergence Society
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    • v.11 no.7
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    • pp.157-162
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    • 2020
  • In recent years, laser induced graphene process have been intensively studied for eco-friendly electronic device such as flexible electronics or thin film based energy storage devices because of its simple and effective process. In order to increase the performance and efficiency of an electronic device using such a graphene patterned structure, it is essential to study an optimized laser patterning condition as small as possible linewidth while maintaining the graphene-specific 2-dimensional characteristics. In this study, we analyzed to find the optimal line pattern by using a Ti:sapphire femtosecond laser based photo-thermal reduction process. we tuned intensity and scanning speed of laser spot for generating effective graphene characteristic and minimum thermal effect. As a result, we demonstrated the reduced graphene pattern of 30㎛ in linewidth by using a focused laser beam of 18㎛ in diameter.

Feasibility Study on the Fire Scenario Design of a Couch Burning through a Fire Spread Model (화염 전파모델을 이용한 소파화재 설계화원구성의 적용성 연구)

  • Kim, Sung-Chan
    • Fire Science and Engineering
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    • v.30 no.6
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    • pp.37-42
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    • 2016
  • The present study has been performed to examine the feasibility of a flame spread model on the design fire scenario for fire risk analysis. Thermo-Gravimetric analysis and sample burning test were conducted to obtain the material properties of a single couch covered with synthetic leather material and a series of FDS calculations applying with the measured material properties were performed for different grid sizes. The overall fire growth characteristics predicted by the fire model were quite different from the results of a real scale fire test and the initial peak value of the HRR and total released energy showed the results within a 30% discrepancy for the computational grids used in the present study. The current model has some limitations in predicting the fire growth characteristics, such as fire growth rate and the time to the maximum HRR. This study shows that the fire model may be applicable to creating the design fire scenario through continuous model improvement and detailed material properties.

A study on the optimization of manufacturing processes of double wall bellows for dual fuel engine II - Optimization of welding process - (Dual Fuel 엔진용 이중관 벨로우즈 제작 공정의 최적화에 관한 연구 II - 용접공정의 최적화 -)

  • Kim, Pyung-Su;Kim, Jong-Do;Song, Moo-Keun
    • Journal of Advanced Marine Engineering and Technology
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    • v.40 no.6
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    • pp.504-509
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    • 2016
  • Production processes of double wall bellows can be roughly categorized into two steps. In the first step, inner and outer bellows are made of STS316L in austenite stainless steel due to their excellent formability and corrosion resistance. In the second step, the double wall bellows are manufactured using the welding method with both the inner and outer bellows. The microstructure and defects of each weldment are observed to ensure the reliability of bellows since weldment is a highly vulnerable part, which can crack and fracture when bellows are formed or used. In this study, optimum welding conditions were derived from the analysis of microstructure and inspection of weldment of bellows that were produced using various welding procedure. Moreover, the mechanical properties were evaluated through hardness measurement of substrate, weldment and the heat-affected zone.

Comparison of Chemicophysics Properties of the Detonation Monocrystalline and Synthetic Polycrystalline Nanodiamond (폭발 단결정과 합성 다결정 나노다이아몬드의 물리화학적 특성 비교)

  • Kang, Soon-Kook;Chung, Myung-Kiu
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.12 no.10
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    • pp.4689-4695
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    • 2011
  • Nanodiamond is a relatively new nanomaterial with broad prospects for application. In this paper, a variety of methods were used to analyze comprehensively chemicophysics properties of the detonation monocrystalline and synthetic polycrystalline nanodiamond, XRD spectroscopy, EDS, HRTEM, FTIR, Raman spectroscopy, TGA-DTA and BET. The results show that the monocryctalline detonation nanodiamond particles are spherical or elliptical shape of 4nm ~ 6nm grain size and the polycryctalline synthetic nanodiamond particles are angular shape of 80nm ~ 120nm grain size. The surface of the monocrystalline and polycrystalline nanodiamond contain hydroxy, carbonyl, carboxyl, ether-based resin, and other functional groups. The phase transition temperature of the monocrystalline detonation nanodiamond in the $N_2$ is about $650^{\circ}C$.

Effect of sewage flow on treatment efficiency of small scale wastewater treatment plant in rural community (농촌 지역에서 유입 유량이 소규모 하수처리장 처리 효율에 미치는 영향)

  • Im, Jiyeol;Gil, Kyungik
    • Journal of Wetlands Research
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    • v.18 no.3
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    • pp.267-274
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    • 2016
  • Sewerage supply in rural community is the important for water quality protection of water system such as river, lake and wetland. And characteristic of small scale wastewater system that have wide range of inflow and concentration in sewage should be considered for stable operation of small scale wastewater treatment plant. In this research, characteristics of flow ratio (flow / designed flow), effect on treatment efficiency of small scale wastewater treatment plant and assessment of optimal flow ratio were conducted through analysis on operation result of 18 small scale wastewater treatment plant in Bong-hwa gun. As a result, flow ratio shows the higher value during summer. However pollutants concentration in sewage was shown the higher concentration during autumn and winter. Treatment of small scale wastewater treatment plant is increased when flow ratio increased, and nutrient treatment efficiency is more sensitive to change of flow ratio than organic compound and suspended solids. According to this research result, it need to be maintained flow ratio 0.8 over value for stable treatment efficiency of small scale wastewater treatment plant.

Fabrication and Characterization of Macro/Mesoporous SiC Ceramics from SiO2 Templates (실리카 주형을 이용한 메크로/메조다공성 탄화규소 세라믹의 제조와 비교특성)

  • ;Hao Wang
    • Journal of the Korean Ceramic Society
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    • v.41 no.7
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    • pp.528-533
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    • 2004
  • Macroporous SiC with pore size 84∼658 nm and mesoporous SiC with pore size 15∼65 nm were respectively prepared by infiltrating low viscosity preceramic polymer solutions into the various sacrificial templates obtained by natural sedimentation or centrifuge of 20∼700 nm silica sol, which were subsequently etched off with HF after pyrolysis at 1000∼140$0^{\circ}C$ in an argon atmosphere. Three-dimensionally long range ordered macroporous SiC ceramics derived from polymethylsilane (PMS) showed surface area 584.64$m^2$g$^{-1}$ when prepared with 112nm silica sol and at 140$0^{\circ}C$, whereas mesoporous SiC from polycarbosilane (PCS) exhibited the highest surface area 619.4 $m^2$g$^{-1}$ with random pore array when prepared with 20-30 nm silica sol and at 100$0^{\circ}C$. Finally, tile pore characteristics of porous SiC on the types of silica sol, polymers and pyrolytic conditions were interpreted with the analytical results of SEM, TEM, and BET instruments.

Graft Copolymerization of Acrylic Monomer Containing Aromatic Carboxylic Acid Group onto EPDM and Their Mechanical Properties (EPDM에 방향족 카르복시산을 함유하는 아크릴 단량체의 그라프트 공중합과 기계적 특성)

  • Park, Hyun-Ju;Park, Jong-Hyuk;Bae, Jong-Woo;Kim, Gu-Ni;Oh, Sang-Taek
    • Elastomers and Composites
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    • v.47 no.3
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    • pp.216-222
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    • 2012
  • In this study, p-acryloyloxybenzoic acid(ABA) was synthesized with p-hydroxybenzoic acid(HBA) and acryloyl chloride(AC). The synthesized ABA monomer was grafted onto ethylene-propylene-diene rubber(EPDM) in toluene using benzoyl peroxide(BPO) as an initiator. The structures of ABA and EPDM-g-ABA were characterized by FT-IR, $^1H$-NMR, and $^{13}C$-NMR spectrometer. The graft ratio of EPDM-g-ABA increased with increasing the concentration of the initiator and the monomer. Mechanical properties such as tensile strength and compression set of the EPDM-g-ABA were improved with increasing the graft ratio. The $T_g$ and initial decomposition temperature were also increased with increasing the graft ratio.

A Study on the Forecast of Sales of High Level Convenience Store Products Using System Dynamics - Focused on the Icecup and Cigarette (시스템 다이내믹스를 활용한 편의점 상위상품 매출예측에 관한 연구 - 아이스컵 및 담배를 중심으로)

  • Kim, Dong-Myung;Park, Sung-Hoon;Yeo, Gi-Tae
    • Journal of Digital Convergence
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    • v.18 no.8
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    • pp.169-177
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    • 2020
  • The purpose of this study is to forecast the sales of convenience store flagship products with nonlinear characteristics and time series characteristics. According to the results, the sales of 'Ice Cup' began to increase from March, reached the highest value in summer, especially July and August, and then decreased, revealing a seasonal pattern. Cigarettes showed a seasonal pattern of higher sales in summer and lower sales in winter and was predicted to decrease in sales in the future. This study provides an academic implication in that it focused on the top-selling products that affected an increase in financial performance in a specific convenience store, a method that has been hardly adopted by the existing studies.

Effect of Surface Film on Void Behavior in Composite Integrated Structure (표면접착필름이 복합재 일체형 구조물에서의 기공 거동에 미치는 영향)

  • Park, Dong-Cheol;Kim, Yun-Hae
    • Composites Research
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    • v.33 no.3
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    • pp.147-152
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    • 2020
  • In this study, void behavior of composite laminate by local internal pressure gradient due to structural geometry and surface film application condition was experimentally evaluated through fabrication of spar/skin integrated structure specimens. Viscosity comparison and thermal analysis for both carbon fiber prepreg and surface film were conducted and cure characteristic and rate difference were analyzed. 2 types of spar/skin integrated structural specimens were prepared based on different application condition of surface film. Subsequently, those specimens were evaluated through visual surface inspection, non-destructive and destructive inspection. In a specimen #1 with full application of surface film, low pressurized area of composite laminate created by pressure gradient of structural geometry had voids. It exhibited that voids could not be evacuated and were locked in cured laminate by the influence of pre-cured surface film with relatively faster cure rate. In a specimen #2 without surface film, it revealed that all internal voids disappeared in the cured laminate. Therefore, it is verified that surface film acts as barrier film preventing void movement and evacuation during autoclave cure.

Fabrication of $CaSO_4:Eu$ TLD and Its Physical Characteristics ($CaSO_4:Eu$ TLD의 제작과 물리적 특성)

  • Kim, Do-Sung;Park, Myeong-Hwan
    • Journal of Sensor Science and Technology
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    • v.8 no.5
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    • pp.388-393
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    • 1999
  • In this study, the $CaSO_4:Eu$ TLDs are fabricated and their trap parameters are determined. The optimum concentration of Eu for fabrication of the $CaSO_4:Eu$ TLD is 0.5 mol% and optimum temperature is $600^{\circ}C$ for 2 hours sintering in air. The glow curve of $CaSO_4:Eu$ consists of two glow peaks and these peaks are isolated by thermal bleaching method. Trap parameters of two glow peaks are measured using the initial rise, the peak shape, the heating rate and the least square curve fitting methods. The activation energies of the glow peak I and II are 1.00 eV and 1.09 eV, and the frequency factors are $7.04{\times}10^{11}\;s^{-1}$ and $5.12{\times}10^{11}\;s^{-1}$ and the kinetic orders are 1.11 and 1.33, respectively.

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