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Sintering and Microstructure of PZT Ceramics Prepared from Nanoparticles by Sol-Gel Process (나노 입자를 이용한 PZT 압전 세라믹스의 소결 및 미세구조)

  • Park Yong-Kap
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.6 no.6
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    • pp.457-460
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    • 2005
  • Nano-sized titanium oxide and zirconium oxide powders were synthesized by hydrolysis of titanium isopropoxide $[Ti(OC_3H7)_4]$ and zirconium tetrachloride ($ZrC1_4$) via a sol-gel technique. Lead titanate powders were prepared by mixing $TiO_2$ precursors with PbO slurry made with dilute $NH_4OH$. Lead zirconate titanate powders were, then, synthesized by mixing $PbTiO_3$ with $ZrO_2$ powders. The goal of this research was to obtain the $PbZrTiO_3(PZT)$ powders and sintering these powders at low temperature. The $PbTiO_3$ and PZT powders after firing were analyzed by X-ray diffraction(XRD) and transmission electron microscopy(TEM) was utilized to observe the shape and size of the synthesized nano-particles. In the XRD pattern, the well-crystallized PZT phase could be obtained in consequence of firing at $900^{\circ}C$. SEM micrographs also showed that grains of PZT were relatively well grown with the size of the range of $2{\~}4{\mu}m$. The densified perovskite structure of $PbZrTiO_3$ could be obtained by sintering at temperature as low as $900^{\circ}C$. Characterization of the samples showed improved piezoelectric properties.

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Egg Development and Morphology of Larvae of South Sea Devil Stinger Inimicus japonicus (Cuvier et Valenciennes) Reared in the Aquarium (수조(水槽)에서 사육(飼育)한 남해산(南海産) 쑤기미, Inimicus japonicus의 난발생(卵發生)과 부화자어(孵化仔魚)의 형태(形態))

  • Myoung, Jeong-Goo;Kim, Jong-Man;Kim, Yong-Uk
    • Korean Journal of Ichthyology
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    • v.1 no.1_2
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    • pp.1-8
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    • 1989
  • In August, 1988, matured adults of devil stinger were collected from Jinhae Bay and Jaran Bay, Kyongsangnam-do, Korea and kept in the aquarium (1 ton) for spawning. The egg development was observed with the eggs laid in the aquarium of adult fish. The diameters of eggs ranged from 1.2 to 1.3 mm (n=6), and no oil globules were found in the eggs. The hatching took place from 26 to 29 hours after eight cells stage at the water temperature of $24.9-26.5^{\circ}C$. The newly hatched larvae were 2.47~3.10 mm in total length with xanthophore on the body and yolk sac. Myomere number was 13+16-17=29-30. Two days after hatching, larvae were 3.61-4.16 mm in total length, and 3 to 4 large spots of melanophore appeared on the large pectoral fin. Three days after hatching, larvae were 3.97-4.29 mm in total length, and the larvae absorved the yolk material completely to become post larvae with 4-5 rays of the pectoral fin. Six days after hatching, larvae attained 4.07-5.46 mm in total length, and 11 rays and 8-9 spots of melanophore were developed on the pectoral fin.

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Intraspecific Androgenesis in Mud Loach (Misgurnus mizolepis): II. Diploid Restoration and Viability Assessment (미꾸라지(Misgurnus mizolepis)의 웅성발생성 처녀생식: II. 웅성발생성 이배체 유도 및 생존능력 평가)

  • Nam, Yoon-Kwon;Bang, In-Chul;Noh, Choong-Hwan;Cho, Young-Sun;Kim, Dong-Soo
    • Journal of Aquaculture
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    • v.19 no.4
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    • pp.281-287
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    • 2006
  • Intraspecific diploid androgenesis was achieved in mud loach (Misgurnus mizolepis) by the inhibition of the first mitotic division using combined thermal treatment. A combined thermal treatment (heat shock at $40.5\;^{\circ}C$ for 120 sec followed by cold treatment at $1\;^{\circ}C$ for 45 min) applied to the 1st metaphase of cell division (28 min post insemination at $25\;^{\circ}C$) successfully recovered viable androgenetic diploidy. Mean hatching success of the androgenetic diploid group was 29.6%, and the average yield out of total eggs taken was about 7% assessed at 1 week of age. However, relatively large variations in the yield of diploid androgenesis were observed among different egg batches used as cytoplasmic donors. Successful diploidization was confirmed by flow cytometric analysis, and parthenogenic reproduction in a paternal exclusive manner was verified with transgene dosage. Significant mortality was found in most androgenetic groups especially from hatch to 1 month of age, although such mortality was stabilized later.

Prodution and Properties of the Insoluble Penicillinase from Streptomyces (방선균이 분비하는 불용성 Penicillinase)

  • 이동희;서정훈
    • Microbiology and Biotechnology Letters
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    • v.7 no.3
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    • pp.135-140
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    • 1979
  • A Streptomyces sp. strain AS-727 which was capable of producing penicillinase, was isolated from soil. The enzyme production was affected by the carbon and nitrogen sources added. Among them so far tested, glucose (or maltose) and sodium nitrate increased the enzyme production. And the amount of enzyme prodced reached maximum in 4 days cultivation. The optimla pH and temperature of the penicillinase was between pH 6.0 to 8.0 and 4$0^{\circ}C$ respectively. The stabel pH range of the enzyme was stable at 4$0^{\circ}C$, but it lost about 30% and 40% of the the activity respectively when it was treated at 6$0^{\circ}C$ and 8$0^{\circ}C$ for 60 minutes. The activity of the enzyme was inhibited by Z $n^{++}$, but A $g^{+}$, $Co^{++}$, $_Mn^{++}$, $Ca^{++}$, P $b^{++}$ did not affected enzyme activity. Peculiarly, the enzyme protein precipitated by freezing or addition of ammonium sulfate, urea, sodium chloride and some organic solvents as etanol, methanol, acetone was not dissolved in deionized water or any buffer solution.n.n.ion.n.n.

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대졸자들의 취업 여부에 따른 정신건강의 변화

  • Jang, Jae-Yun;Jang, Eun-Yeong
    • Proceedings of the Korean Association for Survey Research Conference
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    • 2005.12a
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    • pp.91-113
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    • 2005
  • 본 연구는 청년들의 취업 및 실업 경험이 정신건강에 어떠한 영향을 미치는지 종단적으로 알아보는 데 목적이 있다. 구체적으로 대학을 졸업하고 난 이후에 지속적으로 미취업 상태로 남아있는 사람들의 정신건강의 문제 그리고 취업에 성공하는 경험이 정신건강에 미치는 영향을 미치는지 알아보고자 한다. 이를 위해서 국내 대학교 4학년생들을 대상으로 1차 조사를 실시하고 이후 약 6개월 간격으로 2차 조사, 3차 및 4차 조사를 실시하였다. 네 시점에서 모두 응답자들의 취업여부와 정신건강 수준을 측정하였다. 4차 조사까지 모두 응답한 560명 중에서 2차, 3차, 및 4차 시점의 취업여부에 의해서 집단을 다음과 같이 나누었다: 2차, 3차 및 4차 시점 순서대로, 모두 취업 상태인 집단('취업-취업-취업 집단'), 3차 시점에서 취업에 성공한 집단('미취업-취업-취업 집단'), 4차 집단에서 취업에 성공한 집단('미취업-미취업-취업집단') 그리고 모두 미취업 상태인 집단('미취업-미취업-미취업 집단'). 그 결과를 보면, 취업-취업-취업 집단의 경우에는 취업에 성공한 2차 시점에서 정신건강 수준이 상당히 좋아졌다가 3차 및 4차 시점에서 다시 본래 수준으로 돌아가는 경향을 보였다. 미취업-취업-취업 집단의 경우에는 취업에 성공한 3차 시점 이후로, 미취업-미취업-취업 집단의 경우에는 취업에 성공한 4차 시점에서 정신건강 수준이 좋아지는 경향을 보였다. 지속적으로 미취업 상태였던 집단에서는 3차 시점에서 정신건강 수준이 상당히 나빠졌다가 여전히 미취업 상태인 4차 시점에서 오히려 완화되는 경향을 보였다. 본 연구의 시사점과 제한점 및 장래 연구의 과제가 논의되었다.iments and numerical analysis of luminescence efficiency in the hole carrier transport layer's thicknes. 나아갈 것이며, 아울러 향후에도 아직 미흡한 분야인 IT 아웃소싱에서 적정수준의 대가지급 방안 및 바람직한 Relationship 에 영향을 미치는 여러 가지 요인에 대해서도 살펴 봄으로써 IT분야의 Outsourcing을 검토하거나, 추진할 때 도움이 될 수 있도록 하고자 한다.개의 총 297개의 데이터를 추출하여 사용하였다. 실험과는 좌측공격 91.7%, 우측공격 100%, 중앙공격 87.5%, 코너킥 97.4%, 프리킥 75%로서 매우 양호한 인식율을 보였다. 사용경험정도가 가입직후 해지에만 영향을 미치는 요인임을 보여준다. 또한 매체의 정보전달 풍부성 (media richness)이 상대적으로 높은 소매점이나 웹사이트를 통해 서비스에 가입한 소비자일수록 가입 직후뿐만 아니라 서비스사용 이후에도 낮은 해지성향을 나타냈다. 이러한 분석결과를 바탕으로 인터넷전화 서비스에 적합한 고객지원 프로그램 설계와 마케팅 매체선정과 관련한 전략적 시사점을 도출한다. 그리고 국내에서 최근 이슈가 되고 있는 차세대 무선인터넷 서비스인 와이브로 출시에 따른 마케팅 및 고객관리와 관련된 시사점을 논의한다.는 교합면에서 2, 3, 4군이 1군에 비해 변연적합도가 높았으며 (p < 0.05), 인접면과 치은면에서는 군간 유의차를 보이지 않았다 이번 연구를 통하여 복합레진을 간헐적 광중합시킴으로써 변연적합도가 향상될 수 있음을 알 수 있었다.시장에 비해 주가가 비교적 안정적인 수준을 유지해 왔다고 볼

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A Survey on the Actual Condition for Dining-out in Busan 4. The Propensity to Dining-out at Suppertime (부산지역의 외식실태조사 4. 저녁때의 외식성향)

  • 김두진
    • The Korean Journal of Food And Nutrition
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    • v.15 no.4
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    • pp.357-363
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    • 2002
  • This study was conducted to find out the actual condition of dining-out and the propensity to dining-out at suppertime according to gender and age in Busan area. The survey was conducted on 792 peoples who live or work in Busan area. The results of the questionnaires are as follows ; The place to dining-out at suppertime were in order of “downtown”and “about the house”Partner to eating-out were in order of “friend” and “family”. Restaurants used frequently at suppertime were in order of “Kalbi R.”, “Korean style R.” and “Sliced raw fish R.”The favorite menu were in order to “So-kalbi”, “Sliced raw fish”and “Pizza” Drinking with a meal was 76.7% of respondents and the kind of liquor frequetly drinking were in order of “Soju” and “Beer” at suppertime. But, the results of the propensity to dining-out were different according to gender and age groups.

A Study on Temperature Characteristics of Various Depth using Infrared Thermography (적외선 열화상기법을 이용한 균열 깊이에 따른 온도특성에 관한 연구)

  • Jung, Ju-Yeong;Yoon, Hyuk-Jin;Cho, Hyun-Woo;Yang, Hui-Seung
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.3
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    • pp.83-89
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    • 2018
  • The thermal characteristics of concrete specimens were analyzed using cement paste specimens with artificial cracks. In order to understand the temperature characteristics of the specimen depending on the crack depth, the specimen was heated and the minimum temperatures of the specimens at which cracks appear were investigated according to the crack depth. It was confirmed that the surface temperature distribution of the specimen varies depending on whether the specimen is cracked or not, because of the single and multiple reflections of the incident energy. Furthermore, as the temperature distribution of the specimen reaches a steady state, the temperature data tends to decrease with the crack depth. Through the observation of the normalized temperatures, it was found that the temperature of the specimens obtained from this experiment reached a steady state after 10 minutes. At this time, the standard deviation of the normalized temperature is around 0.01 or less, and the temperature decreases linearly with increasing crack depth. This result is considered to be closely related to the area where multiple reflections occur in the cracked region. If the correlation between the crack region and the incident energy is analyzed for various specimens, it can be applied to the diffuse reflection of the light.

A Study on the Environmental Characteristics of the Pedestrian District in Freiburg, Germany - Focusing on Identity as a Historical City as related to the Waterscape and Paving Environments - (독일 프라이부르크시 보행자전용구역의 환경특성 - 수경 및 포장환경을 통해 본 역사적 정체성을 중심으로 -)

  • Hong, Youn-Soon
    • Journal of the Korean Institute of Landscape Architecture
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    • v.38 no.2
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    • pp.64-74
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    • 2010
  • Freiburg, as the German Capital of the Environment, is well known to Koreans, and relationships with Korean cities are deeply extended. This study attempts to grasp the features of the historical and cultural environment in Freiburg's old town center pedestrian district through the investigation of the historical value of environmental elements and the way they are transmitted along with the components of city identity. Through the literature studies confirms that. The main canal in Freiburg, called Gewerbeknale, is valued both for its existence during the city construction period and for being an infrastructure to supply water to the Bachle(small urban canal) and Brunnen(fountain). In spite of a recipient environment in the middle of the 19th century, the traditional mosaic pavement has a new value as an mediator between citizens and the environment through the adaptations that have occurred in the city. This study has verified the dialectical repetition of crisis and conquest through the historical succession of environmental elements. The historical continuance of environmental elements has a strong influence on the acquisition of sameness and Individuality in city identity factors. The result of this study recommends the historical value of environmental elements that have survived in the urban environment, and verifies the necessity of a concrete strategy for preservation and related practical efforts.

A study on the pulse wave factor according to BMI and period of sterility on female (난임 여성의 체질량지수(BMI), 불임기간에 따른 맥파 연구)

  • Kim, Gyeong-Cheol;Kim, Yi-Soon
    • Korean Journal of Oriental Medicine
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    • v.18 no.2
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    • pp.139-149
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    • 2012
  • Objectives : This is the study to understand of the pulse wave factor according to BMI and period of sterility on female, and to confirm the relationship of pulse wave factor among left and right inch, bar and cubit. Methods : The Questions and measurement of the pulse wave were operated with subjects(76 sterile females using on public health center). The measurement of the pulse wave was operated in 6 part of left and right inch, bar and cubit. The pulse wave was prior measured in part of left bar (i.e. interior pulsation part of radial process styloides in left hand), and next was measured in part of left inch and bar. And the pulse wave was operated samely in part of right inch, bar and cubit. Results : The results were as follows. The pulse energy of 6 part of left and right inch, bar and cubit was showed statistical significance and decreased in order of left inch, right inch, left cubit, right cubit, left inch, right bar. The left and right inch and cubit were showed numerical value of normal range, but left and right bar were showed lower pulse eneregy than normal range. Also left and right cubit were showed lower than left and right inch, and higher than left and right bar. In BMI, The pulse energy of left and right inch, cubit and the average of right hand was not showed statistical significance in the range of low-weight, normal, over-weight and obesity. But in the left and right bar and the average of left hand, the pulse energy of over-weight and obesity group were showed significantly higher than low-weight group. And the pulse wave factor was divided the pattern of h1 showing high numerical value in inch (Ap, As, Aw) and the pattern of Wm showing high numerical value in bar and cubit (RAI, Ad) Conclusions : The low pulse energy of bar was significant observation on the setting of oriental medical diagnostic index on sterilitas. Also, in the numerical value pattern of diverse pulse wave factor, it was divided the pattern of high numerical value in inch and the pattern of high numerical value in bar and cubit. On this, we think that the studies need in the future.

A Recovery Technique of PDF File in the Unit of Page (PDF 파일의 페이지단위 복구 기법)

  • Jang, Jeewon;Bang, Seung Gyu;Han, Jaehyeok;Lee, Sang Jin
    • KIPS Transactions on Computer and Communication Systems
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    • v.6 no.1
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    • pp.25-30
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    • 2017
  • The influence of the data deletion method which is one of anti-forensic techniques is substantial in terms of forensic analysis compared to its simplicity of the act. In academic world, recovery techniques on deleted files have been continuously studied in response to the data deletion method and representatively, the file system-based file recovery technique and file format based recovery technique exist. If there's metadata of deleted file in file system, the file can be easily recovered by using it, but if there's no metadata, the file is recovered by using the signature-based carving technique or the file format based recovery technique has to be applied. At this time, in the file format based recovery technique, the file structure analysis and possible recovery technique should be provided. This paper proposes the page recovery technique on deleted PDF file based on the structural characteristics of PDF file. This technique uses the tag value of page object which constitutes one page of PDF file. Object is extracted by utilizing each tag value as a kind of signature and by analyzing extracted object, the metadata of PDF file is recombined and then it's reconfigured page by page. Recovering by page means that even if deleted PDF file is damaged, even some pages consisting of PDF file can be recovered. Generally, if the file system based file is not recoverable, deleted file is recovered by applying the signature based carving technique. The technique which we proposed in this paper can recover PDF files that are damaged. In the digital forensic perspective, it can be utilized to recover more data than previously.