• Title/Summary/Keyword: 경화공정

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Pervaporation Separation of Isopropyl Alcohol-water Mixtures Using Poly (dimethyl siloxane) Membrane (PDMS 막을 이용한 물과 이소프로판올 혼합액의 투과증발 분리특성)

  • Kim, Ji Seon;Lee, Choong Sub;Cho, Eun Hye;Rhim, Ji Won
    • Membrane Journal
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    • v.23 no.3
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    • pp.245-250
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    • 2013
  • In this study, the pervaporation separation characteristics were investigated for the iso-propyl alcohol (IPA)-water system using PDMS dense membranes. The ratio, 9:1 and 10:1, of the basic material based on RTV-655 and crosslinking agent were used to prepare dense membranes at the reaction temperatures, 40, 60, and $80^{\circ}C$. And these resulting membranes were characterized by pervaporation technique in terms of permeabilities and separation factors for the feed composition of IPA 85 wt% at the operating temperatures, 25, 35, 45, and $55^{\circ}C$. Typical results of permeabilities $148g/m^2{\cdot}hr$ at $55^{\circ}C$ for 9:1 membrane and the selectivity 17 at $55^{\circ}C$ for 10:1 membrane were obtained, respectively.

Thermal Residual Stresses and Spring back Effects on the Frequency Selective Surface Embedded Composite Laminates (주파수 선택막이 삽입된 복합재 평판의 잔류 열응력과 스프링 백 효과)

  • Park, Kyoung-Mi;Seo, Yun-Seok;Chun, Heoung-Jae;Hong, Ic-Pyo;Park, Yong-Bae;Kim, Yun-Jae
    • Journal of the Computational Structural Engineering Institute of Korea
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    • v.26 no.6
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    • pp.475-481
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    • 2013
  • The residual stresses occur in the Frequency Selective Surface(FSS) embedded hybrid composite structures after co-curing due to mismatch among the coefficient of thermal expansions and stiffness values between the FSS and composite materials. The spring backs occur due to these residual stresses. Therefore, in this paper, the spring-backs caused by residual stresses in FSS embedded composite structures were studied with considering effect of symmetric and unsymmetric stacking sequence of composite laminates.

Study on the Peel off Style Low Viscosity Epoxy and Separation Media for a Moving Historic Sites (유구 이전 전용 저점도형 에폭시와 박리제에 관한 연구)

  • Han, Won-Sik;Hong, Tae-Kee;Park, Gi-Jung;Lim, Sung-Jin;Wi, Koang-Chul
    • Journal of Conservation Science
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    • v.24
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    • pp.37-42
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    • 2008
  • Stability of the moving historic sites have something to do with the degree of easiness of work as well as physical property of polymer product. These agents should be able to use without the effect of outer environments like water or low temperature and must have stability during progress of working the peel off Urethane pre-product from Epoxy surface. So, we synthesized low viscosity epoxy resin and hardener with best physical quality and separation media for the moving of historical sites. These products have very good tension strength, adhesion strength, low viscosity and various physical properties that the users want. Particularly, separation media products have good separation of Urethane pre-products surface and Epoxy final product surface.

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The weldability and mechanical property of CP titanium by GTAW (순 타이타늄의 GTAW 용접성 및 기계적 특성)

  • Hong, Jae-Keun;Kim, Jee-Hoon;Lee, Chae-Hoon;Yeom, Jong-Taek;Kang, Chung-Yun
    • Proceedings of the KWS Conference
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    • 2009.11a
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    • pp.57-57
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    • 2009
  • 산업의 고도화에 따른 구조물의 사용 환경이 열악해지고 최근 에너지저감과 환경문제 개선을 위한 경화의 요구에 따라 뛰어난 내식성 및 우수한 고비강도 특성을 갖고 있는 타이타늄 및 타이타늄합금의 활용에 대한 연구가 많은 주목을 받고 있다. 이에 따라 타이타늄 신합금의 개발뿐만 아니라 기존에 개발되어 비교적 보편적으로 적용되고 있는 타이타늄 부품의 제조 및 성형기술에 대한 수요도 급증하고 있다. 특히, 기기 및 부품 제조를 위한 용접/접합기술도 매우 중요한 요소기술로 자리메김하고 있다. 타이타늄은 산소, 수소 등의 침입형 원소와의 친화력이 강한 활성이 큰 금속으로 용접시 고온에 노출되면 급격히 산화 및 취화 등의 문제를 발생한다. 따라서 타이타늄의 용접시에는 $426^{\circ}C$이상의 온도에서는 대기로부터 용접부가 차단되도록 하는 쉴딩기술이 매우 중요하다. 타이타늄의 용접은 일반적으로 아크용접, 전자빔 용접, 레이저 용접 및 확산접합 등이 적용되고 있으나 용접입열 조정이 용이하고 아크 안정성이 높고 용접부의 기계적 특성이 우수한 GTA 용접이 작업성을 고려하여 가장 많이 적용되고 있다. 본 연구에서는 미국용접학회(AWS)의 타이타늄 용접가이드를 분석 및 소개하였고, 1t 이하의 박판 CP Ti를 대상으로 GTAW 용접부 미세조직 및 기계적 특성을 분석하였다. 이때, 용접 비드폭 제어 및 펄스 용접기술을 통하여 박판 타이타늄의 최적 GTAW 공정변수 제어기술을 분석하였다.

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A Study on the Low Cycle Fatigue Characteristics for the Structural Low Carbon Steels (構造용 低炭素鋼材의 低사이클 疲勞特性에 관한 硏究)

  • 김영식;노재충;한명수
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.13 no.2
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    • pp.307-315
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    • 1989
  • In recent years, the fatigue design method by analysis for the mechanical components and the welded structures has much increased, instead of the fatigue design method by rule that has been widely used from the past days. When a fatigue design is conducted by that method, the basic informations, fatigue life curves are mainly obtained from the results of the strain controlled low cycle fatigue test. From these point of views, the low cycle fatigue test is coming to be given a much importance lately. In this paper, the strain controlled low cycle fatigue properties at room temperature in air environment were investigated for the low carbon forged steel, SF45A, and the rolled steel for the welded structure, SM 41B. Throughout the test, strain ratio, R, was maintained constant with the fully reversed condition, -1. As the experimental results, the cyclic stress-strain behaviours of the test materials were different each other, but the low cycle fatigue life-time of them appeared to show little difference in the region of this test conditions.

Preparation and Characterization of Hard Coating Materials Based on Silane Modified Boehmite Hybrid Materials (Bohemite 나노졸을 이용한 내구성 코팅재료의 제조와 특성에 관한 연구)

  • Jeon, Seong Je;Kim, Woong;Lee, Jai Joon;Koo, Sang Man
    • Applied Chemistry for Engineering
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    • v.17 no.6
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    • pp.580-585
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    • 2006
  • UV-thermal dually curable coating materials were prepared by the sol-gel method. Nano-sized colloidal boehmite was treated with various organo silane coupling agents. These materials could be well dispersed in various alcohols and relatively polar organic solvents such as tetrahydrofuran and acetonitrile. The coating films were prepared by a spin coating method on various substrates, which were characterized by FT-IR, Si/Al CP MAS NMR spectra, UV-Vis spectrophotometer, FE-SEM, Taber abraser, haze meter, and pencil hardness tester. The effects of molar ratio and types of silane coupling agents, curing method and ion-shower treatment were investigated. Dually curable coating method offered an optimally good quality film in both hardness and transmittance. The transparency and the hardness of the prepared films were increased with amounts of 3-(trimethoxysilyl)propylmethacrylate, and (3-glycidyloxypropyl)trimethoxysilane, respectively. The adhesion between coated layer and substrate could be enhanced by ion-shower treatment.

Studies on the Synthesis and Characteristic of Silica-PMMA Nano Hybrid Material (실리카-PMMA 나노 하이브리드 코팅액 제조 및 특성에 관한 연구)

  • Son, Dae Hee;Kim, Dae-Sung;Lee, Seung-Ho;Kim, Song Hyuk;Lee, Gun-Dae;Park, Seong Soo
    • Applied Chemistry for Engineering
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    • v.23 no.1
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    • pp.53-58
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    • 2012
  • In order to improve the surface hardness of transparent plastic films, an organic-inorganic hybrid coating solution was sunthesized by the sol-gel method. Coating solutions that were prepared colloidal silica (CS), poly methyl methacrylate (PMMA), vinyltrimethoxysilane (VTMS), and [3-(methacryloyloxy)]propyltrimethoxy silane (MAPTMS) was varied with synthesizing parameters such as kinds of organic silane and weight ratio of CS to PMMA. Such coating solution was bar coated on the PET film, cured, and investigated on the chemical and physical properties of coating film. The organic-inorganic hybrid coating solutions have better properties at the pencil hardness and adhesion of coating film than those of an organic material such as PMMA.

Evaluation of Exposure to Isocyanates Used in Furniture Industry (가구산업에 사용되는 이소시안화물 폭로에 대한 평가)

  • Lee, Su-Gil;Lee, Nae-Woo;Pisaniello, Dino. L
    • Journal of the Korean Society of Safety
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    • v.21 no.2 s.74
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    • pp.138-142
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    • 2006
  • Occupational asthma is commonly known to be induced by isocyanate exposure. Spray painters generally use isocyanates for 2-pack spray painting to coat wooden panel surfaces in the furniture industry in South Australia. Due to a lack of actual exposure data, this study conducted environmental and dermal/ocular monitoring from a company in the furniture industry. According to this study, there was no significant airborne contamination, due to the use of high volume low pressure (HVLP) spray guns, low concentration of hardener in paint solutions and appropriate respirator like full face-air line respirator. There was no significant HDI detection in the general work area around the spray booths. Owing to the use of disposable nitrile gloves during the spray painting, no significant dermal exposure was found. According to color monitoring, there was a possible dermal exposure from surfaces in the workplace, unless either protective gloves were worn or appropriate working practices like clean-up process and storage in a secure places. No eye contamination was detected from the spray painters. No significant exposure levels from inhalational, dermal, ocular were found. The area of most concern was work practices.

Characteristics of Flame Hardening Process for 12Cr Steels (12Cr 강의 이동 화염경화 공정 특성)

  • Kim Gwang-Ho;Lee Min-Ku;Kim Kyeong-Ho;Kim Whung-Whoe;Rhee Chang-Kyu;Kim Gil-Mu
    • Journal of Surface Science and Engineering
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    • v.39 no.2
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    • pp.49-56
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    • 2006
  • In this study, the movable flame hardening process of 12Cr steel for a uniform hardness and desirable residual stress have been investigated. For this, the temperature cycles have been controlled accurately as a function of the three processing variables, the flame intensity $I_f$, the scanning velocity $V_s$, and the initial flame holding time $t_h$, where the standard surface temperature $T_{s,\;max}$, was maintained at $960^{\circ}C$. The optimized conditions were $V_s=0.68mn/s\;and\;t_h=67sec$ for the $C_3H_8:O_2\;=\;5:20l/min,\;V_s=0.80mm/s$ and $t_h=56sec$ for the $C_3H_8:O_2=6:24l/min,\;V_s=1.01mm/s\;and\;t_h=48sec$ for the $C_3H_8:O_2=7:28l/min,\;and\;V_s=1.15mm/s$ and $t_h=39sec$ for the $C_3H_8:O_2$=8:32 l/min. The optimally flame-hardened surface exhibited uniform distributions of the hardness and residual compressive stress over the treated area with moderate levels of $470{\sim}490HV_{0.2}$in hardness and $-300{\sim}-450MPa$ in residual stress, which were acceptable on the basis of the acceptance criteria of Siemens AG-KWU and GE Power Generation Engineering.

Thermal Deformation Analysis of L-shaped Composite During Cure Process by Viscoelastic Model (점탄성을 고려한 L-형상 복합재료 성형시 열변형 해석)

  • Seong, Dong-Yun;Kim, Wie-Dae
    • Composites Research
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    • v.33 no.4
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    • pp.220-227
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    • 2020
  • When curing the composite, the fibers have little thermal deformation, but the resin changes its properties with time and temperature, which leads to residual stress in the product. Residual stress is caused by the difference in the coefficient of thermal expansion of the fibers and resin during the curing process and the chemical shrinkage of the resin. This difference causes thermal deformation such as spring-in and warpage. Thermal deformation of composite structure is important issue on quality of product, and it should be considered in manufacturing process. In this study, a subroutine was developed to predict thermal deformation by applying 3-D viscoelastic model. The finite element analysis was verified by comparing the results of the plate analysis of the 2-D viscoelastic model. Spring-in of L-shaped structure was predicted and analyzed by applying the 3-D viscoelastic model.