• Title/Summary/Keyword: 경도법

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Thermal Flux Analysis for the Wearable NOx Gas Sensors (웨어러블 NOx 가스센서의 열유동 해석)

  • Jang, Kyung-uk
    • Journal of IKEEE
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    • v.23 no.3
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    • pp.793-799
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    • 2019
  • In this study, the diffusion process and the thermal energy distribution gradient of the sensor were confirmed by using the finite element analysis program (COMSOL) of the mesh method to analyze the thermal diffusion in the wearable fabric (Nylon) + MWCNT gas sensor. To analyze the diffusion process of thermal energy, the structure of the gas sensor was modeled in a two dimension plane. The proposed modeling was presented with the characteristic value for the component of the sensor, and the gas sensor designed using the mesh finite element method (FEM) was proposed and analyzed by suggesting the one-way partial differential equation in the governing equation to know the degree of thermal energy diffusion and the thermal energy gradient. In addition, the temperature gradient 10[K/mm] of the anode-cathode electrode layer and the gas detection unit was investigated by suggesting the heat velocity transfer equation.

Rheological Properties of Rehydrated Freeze Dried Instant Rice (동결건조 즉석미반의 리올로지적 성질)

  • Kim, Kwan-Yu;Lee, Shin-Young;Joo, Hyun-Kyu
    • Applied Biological Chemistry
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    • v.32 no.4
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    • pp.332-337
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    • 1989
  • Rheological properties of rehydrated freeze dried instant rice were investigated in comparison with that of cooked rice. The time changes in reciprocal hardness of instant rice grains at various rehydration temperatures$(60{\sim}90^{\circ}C)$ could be expressed by the first order reaction rate equation regardless of rehydration temperature and reaction rate constant increased as the rehydration temperature increased. Activation energy for rehydrating instant rice was 6.1 kcal/g-mol. Analysis of compressive stress relaxation test showed that the viscoelastic properties of both rehydrated instant rice and cooked rice grains could be expressed by 6-elements generalized Maxwell model. Rehydrated instant rice revealed higher relaxation decay than that of cooked rice and showed the elastic property increased by increasing the rehydration temperature.

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Determination of Polyol Concentration Affecting to the Transparent Bar Soap Using Design of Experiment Method (실험 계획법을 이용한 투명비누에 영향을 미치는 폴리올 농도 결정)

  • Cho, Wan-Goo
    • Journal of the Korean Applied Science and Technology
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    • v.29 no.1
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    • pp.54-62
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    • 2012
  • In this experiment, the optimum concentration of polyols which were used for making transparent soaps was determined using design of experiment (DOE) method. Dipropylene glycol and 1,3 butylene glycol with short chains enhanced the transparency of soap, however, polyethylene glycol 400, glycerin and diglycerin made the soap opaque. The hardness of soap was increased as increasing the concentration of propylene glycol, diglycerin, dipropylene glycol and polyethylene glycol 400. The hardness, transparency, absorbance of water, and friction solubility could be optimized by controlling the concentration of dipropylene glycol, polyetylene glycol, sugar, and triethanolamine.

Prediction of Soluble Solid and Firmness in Apple by Visible/Near-Infrared Spectroscopy (가시광선/근적외선 분광분석법을 이용한 사과의 당도 및 경도 측정)

  • 최창현;이강진;박보순
    • Journal of Biosystems Engineering
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    • v.22 no.2
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    • pp.256-265
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    • 1997
  • The objectives of this study were to examine the ability to predict soluble solid and firmness in intact apples based on the visible/near-infrared spectroscopic technique. Two cultivars of apples, Delicious and Gala, were handled, tested and analyzed separately. Reflectance spectra, Magness-Tayor (MT) firmness, and soluble solids in apples were measured sequentially. Maximum and minimum diameters, height, and weight of apples were recorded before the MT firmness tests. A spectrophotometer was used to collect reflectance spectra of intact apples over a wavelength range of 400 to 2, 498 nm. The W firmness tests were conducted using a standard 11.1mm (7/16 in.) MT probe mounted in an Instron universal testing machine. A digital refractormeter was used to measure soluble solid contents in the apples. Apple samples were divided into a calibration set and a prediction set. The calibration set was used during model development, and the prediction set was used to predict soluble solids and firmness from unknown spectra. The method of partial least square (PLS) analysis was used. An unique set of PLS loading vectors (factors) was developed for soluble solid content and firmness. The PLS model showed good correlations between predicted and measured soluble solids of intact apples in 860~1078 nm of the wavelengths. However, the PLS analysis was not good enough to predict the apple firmness.

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Preparation and Characterization of Pure Titanium Ingots Prepared by Electron Beam Melting (전자빔용해법에 의한 고순도 티타늄 잉고트의 제조 및 분석)

  • Kim, Won-Baek;Lee, Gang-In;Choe, Guk-Seon;Seo, Chang-Yeol;Yang, Dong-Hyo
    • Korean Journal of Materials Research
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    • v.7 no.7
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    • pp.608-617
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    • 1997
  • 전자빔 용해법에 의해 고순도 티타늄잉고트 및 버튼시편을 제조하였다. 이들 중 18개의 금속불순물을 GDMS(Glow Discharge Mass Spectrometry)로 그리고 탄소, 질소, 산소의 함량을 고온연소법으로 측정한 후 이들과 전기비저항, 경도와의 관계를 조사하였다. 99%와 99.6%스폰지를 용해한 경우 대부분의금속불순물들이 대폭 감소하는 큰 휘발 정련효과가 나타났으며 비금속불순물들의 경우는 장비의 진공상태에 따라 큰 영향을 받으며 정련효과를 기대할 수 없었다. 금속 불순물중 철은 가장 제거하기 어려운 원소로 밝혀졌으며 이는 원료 스폰기중에서 철이 주불순물이기 때문이며 추가적인 예비정련이 필요한 것으로 나타났다. 상온 및 액체질소온도에서의 전기비저항은 가스불순물의 량이 증가함에 따라 직선적으로 증가하였으며 이들의 저항비($\rho$$_{RT}$ /$\rho$$_{N2}$)는 가스불순물의 총량이 1,000ppm이하의 경우 불순물량이 감소함에 따라 급격하게 저하하였으며 이 이상인 경우 완만하게 감소하였다. 이들의 경도는 가스불순물의 량이 증가하였으며 산소당량의 평방근에 비례하는 것으로 나타났다.다.

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레이저 용접에 따른 재료의 물성 평가

  • Song, Hyeon-Su;Kim, Gyeong-Jong;Hwang, Hyeon-Tae;Kim, Tae-Gyeong
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.05a
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    • pp.41.2-41.2
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    • 2009
  • 최근 자동차 시장에서는 레이저 열처리에 대한 관심이 집중되고 있다. 이는 현재까지 사용되어 왔던 점용접에 비해 이음부 형상에 제한이 적고 자유도가 높으며 짧은 시간내에 용접을 마쳐 열변형의 문제가 적기 때문이다. 이러한 이점 때문에 자동차 시장의 기술개발 동향이 차체 부품의 경량화와 원가절감을 위한 신기술 개발로 레이저 가공 기술을 접목시키고 있으며 이러한 신공정 개발은 지속적으로 확대되어 가고 있는 추세이다. 본 실험에서는 차체 접합을 위하여 신기술로 대두 되고 있는 레이저 용접법으로 박판을 접합하였다. 실험 조건은 동일한 재료 두 판을 합쳐 전력량을 변화시켰으며, 전력량의 한 조건을 잡아 용접 속도에 변화를 주었다. 용접 샘플의 물성을 평가하기 위하여 제품 내부의 구조를 비파괴 시험법을 통하여 분석하여 내부적 결함 및 내부 구조를 관찰하고, 열영향부 및 용접부 내부의 조직을 관찰하여 신기술에 대해 재료적 물성을 평가하고자 한다. 평가방법은 산업용 단층 촬영기(CT X-RAY)를 이용하여 재료를 파괴하지 않고 용접상태에 따른 내부구조를 분석하였으며, 용접부, 열영향부 그리고 모재 부분에 대해 경도를 측정하여 용접조건에 따른 경도양상을 관찰하였다. 또한 부위별로 조직을 관찰하여 재료 내부의 상을 관찰하였다.

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Effect of Temperature on Sintering Properties in Zirconia Fabricated by Plasma Activated Sintering (Plasma Activated Sintering법으로 제조된 지르코니아의 소결특성에 미치는 온도의 영향)

  • 신종호;정연길;허성강
    • Journal of the Korean Ceramic Society
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    • v.37 no.9
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    • pp.856-863
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    • 2000
  • 상압 소결법과 통전활성 소결(Plasma Activated Sintering; PAS)법으로 120$0^{\circ}C$부터 150$0^{\circ}C$의 온도범위에서 제조된 지르코니아의 기계적 특성을 ring on ring disk 굽힘시험으로 비교하여 고찰하였다. 모든 소결온도범위에서 PAS법으로 제조된 소결체의 밀도와 경도는 상압 소결법에 의해 제조된 소결체 보다 높게 나타났다. 결정립의 크기는 두 소결법에 의해 제조된 소결체 모두에서 소결온도 증가에 따라 증가하였으나, PAS법으로 제조된 소결체가 상압 소결법으로 제조된 소결체 보다는 결정립 성장이 억제되었다. 파괴인성은 PAS법으로 제조된 소결체의 경우 130$0^{\circ}C$에서 최고값을 나타낸 후 소결온도 증가에 따라 미세하게 감소하였으며, 상압 소결법으로 제조된 소결체의 경우 소결온도 증가에 따라 증가되었다. 소결체의 상분율 변화는 PAS법으로 제조된 경우 전 온도범위 (1200~150$0^{\circ}C$)에서 정방정상만 관찰되었으며, 상압 소결법의 경우 단사정상과 정방정상의 혼합상을 나타내었고, 소결온도 증가에 따라 정방정상의 비율이 증가하였다. 결과적으로 PAS법의 경우 지르코니아의 최적 소결온도는 130$0^{\circ}C$이며, 상압 소결법의 경우 150$0^{\circ}C$임을 알 수 있었으며, 소결체의 파괴인성에 미치는 영향은 결정립 크기 및 정방정상의 분율임을 확인할 수 있었다.

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The Variation of Structure and Physical Properties of XLPE during Thermal Aging Process (가교 폴리에틸렌의 열노화에 따른 구조와 물성의 변화)

  • 이미영;김철환;구철수;김복렬;이영관
    • Polymer(Korea)
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    • v.27 no.3
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    • pp.249-254
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    • 2003
  • The variation of chemical structure and physical properties of crosslinked polyethylene (XLPE) during thermal aging process was investigated. The formation of carbonyl functional group resulting from thermal oxidation reaction of XLPE was monitored using X-ray photoelectron spectroscopy and near infrared (NIR) spectroscopy. It was observed that the intensity of carbonyl peak observed at 1715 nm linearly increased with aging time in NIR spectroscopy. The linear relationship between NIR peak absorbance and aging time confirmed that NIR spectroscopy might be used as a proper tool for monitoring the aging process of polymeric materials. Also the formation of crosslinks during the aging process was monitored using thermal mechanical analysis, stress-strain test, and Shore hardness test. The change in the physical properties, such as the increase in the glass transition temperature from 110 to 132$^{\circ}C$, the decrease in the strain from 265 to 110%, as well as the increase in the shore D hardness from 32 to 50, was observed during the aging process.

ZrO2/TiO2/Organosilane Hybrid Composites via Low Temperature Sol-Gel Process for Hard and Transparent Coating (저온 졸-겔 법을 이용한 투명 하드코팅 필름용 ZrO2/TiO2/Organosilane 복합체 연구)

  • Lee, Su-Hyeon;Choi, Jongwan
    • Journal of the Korean Applied Science and Technology
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    • v.35 no.1
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    • pp.80-88
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    • 2018
  • In this study, we prepared hybrid composites by using low temperature sol-gel process for transparent and hard coating film. The hybrid composites consist of $ZrO_2/TiO_2/organosilane$, of which organosilane was introduced 3-(trimethoxysilyl)propyl methacrylate due to the role of a photocurable ceramic material for low temperature process. The ceramic composites with various composition ratios were coated on a polycarbonate substrate using a sol-gel process of low temperature process, and characterized optical and mechanical properties of coated thin film. The transparencies of coated thin films were 97.5 % or more, and the pencil hardness were 9H or more. In the case of the ZTS-2-1, the nano-indentation hardness was measured at the highest value of 1.14 GPa.

Development of Surface Improvement Technique of Japanese Larch Flooring Board(II) (낙엽송 마루판재의 표면강화 처리기술 개발(II))

  • Park, Sang-Bum
    • Journal of the Korean Wood Science and Technology
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    • v.28 no.1
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    • pp.28-35
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    • 2000
  • This paper deals with a coating technique for hardening surface layer of softwood(Larix leptolepis) flooring board to improve its surface properties such as hardness and abrasion resistance, Two coating methods were applied for surface hardening of the wood in this study. First, several functional monomers were added in UV-curing epoxy acrylate varnish. Secondly, unsaturated polyester varnish was used as under coat and acryl varnish including anti-abrasive agent was used as top coat. The hardness of the treated wood was similar to that of high density hardwood such as keruing by the first coating method. The abrasion resistance of the coated wood was greatly improved by the second method. Adhesion properties and impact resistance of the coated wood surface were also good. It was suggested that the well-coated softwood could be used as interior flooring board for heavy walking as substitute for hardwood.

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