• Title/Summary/Keyword: $MoS_{2}$ coating

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Synthesis and Electrochemical Properties of Carbon Coated Mo6S8 using PVC (PVC를 원료로 탄소코팅한 Mo6S8의 합성 및 전기화학적 특성)

  • Si-Cheol Hyun;Byung-Won Cho;Byung-Ki Na
    • Korean Chemical Engineering Research
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    • v.61 no.3
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    • pp.348-355
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    • 2023
  • Magnesium secondary batteries are attracting much attention due to their potential to replace conventionally used lithium ion batteries. Magnesium secondary battery cathode material Mo6S8 were synthesized by molten salt synthesis method and PVC as a carbon materials were added to improve electrochemical properties. Crystal structure, size and surface of the synthesized anode materials were measured through XRD and SEM. Charge-discharge profiles and rate capabilities were measured by battery test system. 2.81 wt% PVC coated sample showed the best rate capabilities of 85.8 mAh/g at 0.125 C-rate, 69.2 mAh/g at 0.5 C-rate, and 60.5 mAh/g at 1 C-rate.

A Study on Detection of Small Defects for MoSi2 by Medical Ultrasonic Testing (의학용 초음파검사기에 의한 MoSi2의 미소결함 탐상)

  • Namkoong, Chai-Kwan;Kim, You-Chul
    • Journal of the Korean Society of Safety
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    • v.10 no.4
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    • pp.9-12
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    • 1995
  • Detection of small defects by medical ultrasonic testing when the thermal sprayed coating by $MoSi_2$ on the metal is done. The defects may occur at the bonded surface. So, the detecting method of the defects by non-destructive in spection is desired. Here, in order to examine the possibility of the detection of the small defects by the ultrasonic. The electronic scanning ultrasonic equipment using an array probe developed as the medical ultrasonic diagnostic equipment is applied for the detection of the metal material defects. It's validity is investigated.

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Friction and Wear Properties of Plasma-sprayed Cr2O3-MoO3 Composite Coatings at High Temperature (MoO3가 첨가된 Cr2O3 플라즈마 용사코팅의 고온 마찰 마멸 특성)

  • Lyo, In-Woong;Ahn, Hyo-Sok;Lim, Dae-Soon
    • Journal of the Korean Ceramic Society
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    • v.39 no.9
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    • pp.851-856
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    • 2002
  • Tribological behavior of plasma-sprayed $Cr_2O_3$-based coatings containing $MoO_3$ at 450$^{\circ}C$ was investigated to understand the influence of $MoO_3$. A reciprocal disc-on-plate type tribo-tester was employed to examine fricition and wear behavior of the specimens. The microstructure and phase composition of the coating was characterized with Transmission Electron Microscopy(TEM). The TEM analysis indicated that $MoO_3$ was dispersed into the grain boundary, resulting in the increase of the hardness and density of the coating. Worn surfaces were investigated by scanning electron microscopy and chemistry of the worn surfaces was analyzed using a X-ray Photoelectron Spectrometer(XPS). The results showed that the friction coefficient of the $MoO_3$-added coatings was lower than that without $MoO_3$ addition. The larger protecting layers were observed at the worn surface of plasma spray coated specimens with $MoO_3$ composition in the protecting layer appears to be more favorable in reducing the friction.

Process variables and die life for cold forging (냉간단조용 금형 수명에 미치는 공정 변수의 영향)

  • Lee Y. S.;Choi S. T.;Kwon Y. N.;Rhyim Y. M.;Lee J. H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2005.05a
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    • pp.215-218
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    • 2005
  • For the production of cold forged parts with near-net-shape attributes, the quality of the tool system is responsible for an essential portion of costs fer the finished components. Therefore, a tool lift is one of the important issues on cold forging industry. There are many complicated variables related with tool life, such as material, heat-treatment, coating, lubricant, process design. In this study, heat-treatment of tool material and lubricant are investigated to improve the tool life. Deep cryogenic treatment of tool steel is very efficient to improve the wear resistance due to the fine carbide. And, friction factor of lubricants for cold forging are measured by the ring compression test. Zinc-Phosphate and $MoS_2$ lubricant is effective to sustain the friction factor under 0.1.

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The Effects of Surface Porfiles and Coatings on the Tribological Behaviors of the Surfaces of Piston Skirt (피스톤 스커트 표면의 트라이볼로지 거동에 미치는 표면형상과 코팅의 영향)

  • Cho, Dae-Hyun;Chung, Soon-Oh;Won, Young-Duck;Han, Man-Cheol;Lee, Young-Ze
    • Tribology and Lubricants
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    • v.24 no.3
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    • pp.122-128
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    • 2008
  • To reduce the friction losses and the wear amounts in the piston assembly two methods were proposed. One is the modification of surface profile of the skirt part. The surface coating is another method to protect the sliding surfaces. To modify the profile of the skirt surfaces the surfaces were ground to have three different shapes of profiles. Also, several coatings, such as graphite, TiN, and $MoS_2$, and DLC, were used to protect the surfaces of the piston skirts. The specimens of the skirt and the cylinder bores were tested with the reciprocating wear tester. SAE 5W40 engine oil was used in boundary lubrication regime. Among several coatings the graphite and DLC coatings were very effective to reduce the friction forces. Especially, DLC film represented much better tribological performances than the others. The friction coefficient of the graphite coating was the lowest, but the graphite coating was not effective to protect the surfaces.

저가형 IR Window의 AR Coating 특성 연구

  • Han, Myeong-Su;Park, Chang-Mo;Kim, Jin-Hyeok;Sin, Gwang-Su;Kim, Hyo-Jin;Go, Hang-Ju
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.178-178
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    • 2010
  • 칼코게나이드계 재료를 사용한 비냉각 적외선 센서의 윈도우를 제작하여 그 특성을 조사하였다. 조성을 EDS로 분석한 결과 Ge-Se-Sb로 구성되어 있음을 확인하였다. 두께 2mm인 윈도우 모재를 양면 경연마한 후 코팅 설계치로 8-12um 영역에서 평균 투과도가 95.6%로 나타났다. 이온빔보조증착장치를 이용하여 Ge, ZnS, $YF_3$ 소스로 코팅한 결과 투과도는 동일파장영역에서 약 94%로 나타났다. 칼코게나이드 원재료의 투과도는 약 69%로써 12um 영역 부근에서 강한흡수를 보였다. 코팅면의 거칠기 값(Ra)은 약 1.5 nm로써 매우 매끄러운 면을 얻었으며, 단면 SEM 측정 결과 설계치와 유사한 박막 두께를 얻었다.

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Bone Ingrowth and Enhancement of Bone Bonding Strength at Interface between Bone and HA Coated Stainless Steel (HA 코팅된 스테인레스강과 뼈의 계면에서의 경조직 성장 및 결합력 향상)

  • Kim, C.S.;Kim, S.Y.;Kim, D.H.;Khang, G.
    • Proceedings of the KOSOMBE Conference
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    • v.1996 no.05
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    • pp.133-136
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    • 1996
  • We investigated how hydroxyapatite (HA) coating onto a porous super stainless steel (S.S.S, 22Cr-20Ni-6Mo-0.25N) affects bone ingrowth in a dog transcortical femoral model. Implants were histologically evaluated after 4 and 48 weeks of implantation, and the bone bonding strength at the bone/implant interface was examined by employing the pull-out test. The direct osseous tissue bonding onto the HA-coated S.S.S was observed, but the uncoated stainless steels had thin fibrous tissue layers. The mean interface strength of the HA-coated S.S.S was 1.5 and 2.5 times greater than those of the S.S.S and the 316L SS after one year of implantation, respectively. In preliminary studies, no toxic responce was observed from a cytotoxicity test of the S.S.S, having similar corrosion resistance to titanium. Our results suggest that early osteoconductive nature of HA coating may induce long term osteointegration for a bioinert substrate.

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The Effects of Dielectric Coatings on Electron Emission from Tungsten

  • Al-Qudah, Ala'a M.;Alnawasreh, Shady S.;Madanat, Mazen A.;Trzaska, Oliwia;Matykiewicz, Danuta;Alrawshdeh, Saad S.;Hagmann, Mark J.;Mousa, Marwan S.
    • Applied Microscopy
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    • v.47 no.1
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    • pp.36-42
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    • 2017
  • Field electron emission measurements were performed on dielectric-coated tungsten emitters, with apex radii in the nanometer and micrometer range, which were prepared by electrochemical etching in NaOH solution. Measurements were performed in a field electron microscopy (FEM) with a base pressure <$10^{-6}$ Pascal ($10^{-8}$ mbar). Four different types of dielectric were used, namely: (1) Clark Electromedical Instruments epoxylite resin, (2) Epidian 6 produced by Ciech Sarzyna S. A., (3) a Radionox solution of colloidal graphite; and (4) Molyslip 2001 E compound ($MoS_2$ and MoS). Current-voltage measurements and FEM images were used to investigate the characteristics of these composite emitters, and to assess how the different types of dielectric coating affect the suitability of the composite emitter as a potential electron source.

Design of Discriminant Function for White and Yellow Coating with Multi-dimensional Color Vectors (다차원 컬러벡터 기반 백태 및 황태 분류 판별함수 설계)

  • Lee, Jeon;Choi, Eun-Ji;Ryu, Hyun-Hee;Lee, Hae-Jung;Lee, Yu-Jung;Park, Kyung-Mo;Kim, Jong-Yeol
    • Korean Journal of Oriental Medicine
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    • v.13 no.2 s.20
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    • pp.47-52
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    • 2007
  • In Oriental medicine, the status of tongue is the important indicator to diagnose one's health, because it represents physiological and clinicopathological changes of inner parts of the body. The method of tongue diagnosis is not only convenient but also non-invasive, therefore, tongue diagnosis is one of the most widely used in Oriental medicine. But tongue diagnosis is affected by examination circumstances a lot. It depends on a light source, degrees of an angle, doctor's condition and so on. So it is not easy to make an objective and standardized tongue diagnosis. As part of way to solve this problem, in this study, we tried to design a discriminant function for white and yellow coating with multi-dimensional color vectors. There were 62 subjects involved in this study, among them 48 subjects diagnosed as white-coated tongue and 14 subjects diagnosed as yellow-coated tongue by oriental doctors. And their tongue images were acquired by a well-made Digital Tongue Diagnosis System. From those acquired tongue images, each coating section were extracted by oriental doctors, and then mean values of multi -dimensional color vectors in each coating section were calculated. By statistical analysis, two significant vectors, R in RGB space and H in HSV space, were found that they were able to describe the difference between white coating section and yellow coating section very well. Using these two values, we designed the discriminant function for coating classification and examined how good it works. As a result, the overall accuracy of coating classification was 98.4%. We can expect that the discriminant function for other coatings can be obtained in a similar way. Furthermore, if an automated segmentation algorithm of tongue coating is combined with these discriminant functions, an automated tongue coating diagnosis can be accomplished.

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Characteristics of Carbon-Doped Mo Thin Films for the Application in Organic Thin Film Transistor (유기박막트랜지스터 응용을 위한 탄소가 도핑된 몰리브덴 박막의 특성)

  • Dong Hyun Kim;Yong Seob Park
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.36 no.6
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    • pp.588-593
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    • 2023
  • The advantage of OTFT technology is that large-area circuits can be manufactured on flexible substrates using a low-cost solution process such as inkjet printing. Compared to silicon-based inorganic semiconductor processes, the process temperature is lower and the process time is shorter, so it can be widely applied to fields that do not require high electron mobility. Materials that have utility as electrode materials include carbon that can be solution-processed, transparent carbon thin films, and metallic nanoparticles, etc. are being studied. Recently, a technology has been developed to facilitate charge injection by coating the surface of the Al electrode with solution-processable titanium oxide (TiOx), which can greatly improve the performance of OTFT. In order to commercialize OTFT technology, an appropriate method is to use a complementary circuit with excellent reliability and stability. For this, insulators and channel semiconductors using organic materials must have stability in the air. In this study, carbon-doped Mo (MoC) thin films were fabricated with different graphite target power densities via unbalanced magnetron sputtering (UBM). The influence of graphite target power density on the structural, surface area, physical, and electrical properties of MoC films was investigated. MoC thin films deposited by the unbalanced magnetron sputtering method exhibited a smooth and uniform surface. However, as the graphite target power density increased, the rms surface roughness of the MoC film increased, and the hardness and elastic modulus of the MoC thin film increased. Additionally, as the graphite target power density increased, the resistivity value of the MoC film increased. In the performance of an organic thin film transistor using a MoC gate electrode, the carrier mobility, threshold voltage, and drain current on/off ratio (Ion/Ioff) showed 0.15 cm2/V·s, -5.6 V, and 7.5×104, respectively.