• Title/Summary/Keyword: work hardening

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Study on the Dislocation Structure and Work Hardening of Single-crystal L12-Ni3Al Intermetallic Compounds Prepared by Bridgman Method

  • Chang-Suk Han;Chang-Hwan Bae
    • Journal of the Korean Society for Heat Treatment
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    • v.37 no.5
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    • pp.215-220
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    • 2024
  • Slip lines and dislocation structures developed by deformation at 77 K, 292 K and 500 K have been investigated by an optical microscope and a high-voltage electron microscope. Slip patterns after the deformation by 4-5% at 77 K and 500 K are compared. From the slip line geometry, operation of both primary and secondary {111} slips have been confirmed. However, the primary slip lines formed at 77 K appear coarser and more pronounced than those at 500 K. This indicates that a larger number of dislocations have moved on the same plane at 77 K. Another characteristic difference noted here is that the slip lines are straight and pass through the specimen from one end to the other at 77 K. On the contrary, slip lines are rather faint at 500 K. The typical change found at 77 K is the increase in the [$0{\bar{1}}1$] dipole dislocations and generation of the [$10{\bar{1}}$] screw dipoles upon increase in the strain from 1.2% to 5.2%. This is the indication that the straight dipole dislocations were formed by a pinning effect due to jogs generated by mutual cutting between primary and secondary dislocations. Extremely fine slip has been noted after deformation at 500 K indicating that the usual Frank-Read source is not operative at high temperatures due to the strong KW locking.

Study on the Development and Property of Epoxy Putty with Excellent Low Shrinkage and Cutting Force Using Mercaptan Type and Diamine Type (Mercaptan계와 Diamine계를 이용한 저수축·절삭력이 우수한 Epoxy Putty의 개발 및 물성에 관한 연구)

  • Oh, Seung-Jun;Wi, Koang-Chul
    • Journal of Adhesion and Interface
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    • v.16 no.4
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    • pp.137-145
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    • 2015
  • This study aimed to develop epoxy putty as a multi-purpose connection and restoration material that can be used for material-specific restoration work such as metal, wood, ceramics, earthenware and stone artifacts by replacing synthetic resins currently being used for preservation treatment of cultural assets. Existing synthetic resins have the issue of cutting force resulting from high strength, deflection resulting from long hardening time, contaminating the surface of artifacts through staining on tools or gloves and need for re-treatment resulting from material discoloration. Accordingly, paste type restoration material most widely being used in the field of cultural assets preservation treatment was selected and examined the property to select it as an object of comparison. Based on such process, epoxy putty was developed according to the kind of agent, hardener and filler. For the purpose of solving the issues of existing material and allowing the epoxy putty developed to have similar property, property experiments were conducted by selecting agents and hardeners with different characteristics and conditions. The study findings showed that both kinds are paste type that improved work convenience and deflection issue as a result of their work time of within 5~10 minutes that are about 3~10 times shorter than that of existing material. In regards to wear rate for increasing cutting force, it improved by about 3 times, thereby allowing easy molding. For the purpose of improving the issue of surface contamination that occurs during work process, talc and micro-ballon were added as filler to reduce the issue of stickiness and staining on hand. Furthermore, a multi-purpose restoration material with low shrinkage, low discoloration and high cutting force was developed with excellent coloring, lightweight and cutting force features.

Drying of Alaska Pollack in Controlled Conditions to Identify Major Factors for Textural Properties of Hwangtae (명태 건조과정에서 일어나는 수분과 수분활성도 변화가 명태건조품의 물성에 미치는 영향)

  • Ha, Ju-Yeoup;Lee, Sang-Hyun;Jung, Kyung-Jin;Jo, Young-Duk;Kim, Jae-Cherl
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.39 no.12
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    • pp.1903-1907
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    • 2010
  • Drying curves for raw Alaska pollack seemed to follow typical food dehydration process with a very short initial settling down period. It was evident that there are some differences in drying rates between each part of fish body showing the highest drying rate for fish head followed by that for fish skin and that for flesh, presumably because of differences in water holding capacity of the components of each part. Specifically, the drying curve of fish flesh revealed that a boundary layer, thereby, a time period, existed which showed a big difference in moisture content and/or water activity as drying proceeds. The boundary layer in fish flesh with high moisture content between the layer contributes to reduce drying rate mainly as a consequence of protein aggregation resulting in hardening of fish flesh. The first boundary layer in this work appeared to show within several hours after initiation of drying. For Hwangtae, a naturally cyclic freeze-thaw dried and aged Alaska pollack which was popular in Korea, manufacturing process, it is clear that periodic moistening of boundary layer in fish flesh prohibits hardening fish flesh in boundary layer and enables steady moisture diffusion from inside of the fish flesh to surface of the fish body.

The High Temperature Deformation Behavior of the Wrought Superalloy 718 (단조용 초내열 718 합금의 고온 변형 거동)

  • Na, Y.S.;Choe, S.J.;Kim, H.M.
    • Analytical Science and Technology
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    • v.9 no.2
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    • pp.179-191
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    • 1996
  • In order to understand the high temperature deformation behavior of superalloy 718, a rotating grade 718 alloy has been compression tested to about 0.7 upset ratio at $927{\sim}1066^{\circ}C$ temperature range and $5{\times}10^{-4}{\sim}5{\times}10^0sec^{-1}$ strain rate. The maximum flow stress was increased with increasing strain rate, and similar behavior was observed with decreasing temperature. At low temperature and high strain rates other than $5{\times}10^{-1}sec^{-1}$, strain softening was occurred mainly by dynamic recovery and deformation twinning processes, while at high temperature and low strain rates strain softening was offseted by dynamic recrystallization. At $5{\times}10^{-1}sec^{-1}$, strain hardening was occurred due to work hardening of the dynamic recrystallized grains. Strain rate sensitivity, m, was varied with strain rates. In the case of lower strain rate tests, m was measured as 0.3 and it was observed that the deformation was mainly controlled by dynamic recrystallization. At higher strain rate, m was lowered to 0.1 and the deformation was controlled by the dynamic recovery and the deformation twinning processes.

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The study on the manufacturing intermediary materials for the carbon nanofiber reinforced Cu matrix noncomposite (일방향 탄소나노섬유 강화 Cu 기지 나노복합재료용 중간재 제조에 관한 연구)

  • 백영민;이상관;엄문광
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2003.10a
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    • pp.46-49
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    • 2003
  • Cu have been widely used as signal transmission materials for electrical electronic components owing to its high electrical conductivity. However, it's size have been limited to small ones due to its poor mechanical properties, Until now, strengthening of the copper at toy was obtained either by the solid solution and precipitation hardening by adding alloy elements or the work hardening by deformation process. Adding the at toy elements lead to reduction of electrical conductivity. In this aspect, if carbon nanofiber is used as reinforcement which have outstanding mechanical strength and electric conductivity, it is possible to develope Cu matrix nanocomposite having almost no loss of electric conductivity. It is expected to be innovative in electric conduct ing material market. The unidirectional alignment of carbon nanofiber is the most challenging task developing the copper matrix composites of high strength and electric conductivity In this study, the unidirectional alignment of carbon nanofibers which is used reinforced material are controlled by drawing process in order to manufacture the intermediary materials for the carbon nanofiber reinforced Cu matrix nanocomposite and align mechanism as well as optimized drawing process parameters are verified via experiments and numerical analysis. The materials used in this study were pure copper and the nanofibers of 150nm in diameter and of $10~20\mu\textrm{m}$ In length. The materials have been tested and the tensile strength was 75MPa with the elongation of 44% for the copper it is assumed that carbon nanofiber behave like porous elasto-plastic materials. Compaction test was conducted to obtain constitutive properties of carbon nanofiber. Optimal parameter for drawing process was obtained by experiments and numerical analysis considering the various drawing angles, reduction areas, friction coefficient, etc Lower reduction areas provides the less rupture of cu tube is not iced during the drawing process. Optimal die angle was between 5 degree and 12 degree. Relative density of carbon nanofiber embedded in the copper tube is higher as drawing diameter decrease and compressive residual stress is occurred in the copper tube. Carbon nanofibers are moved to the reverse drawing direct ion via shear force caused by deformation of the copper tube and alined to the drawing direction.

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Evaluation of Thermal and Shrinkage Stresses in Hardening Concrete Considering Early-Age Creep Effect (초기재령 콘크리트의 크리프를 고려한 온도 및 수축응력 해석)

  • 차수원;오병환;이형준
    • Journal of the Korea Concrete Institute
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    • v.14 no.3
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    • pp.382-391
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    • 2002
  • This study is devoted to the problems of thermal and shrinkage stresses in order to avoid cracking at early ages. The early-age damage induced by volume change has great influence on the long-term structural performance of the concrete structures such as its durability and serviceability To solve this complex problem, the computer programs for analysis of thermal and shrinkage stresses were developed. In these procedures, numerous material models are needed and the realistic numerical models have been developed and validated by comparison with relevant experimental results in order to solve practical problems. A framework has been established for formulation of material models and analysis with 3-D finite element method. After the analysis of the temperature, moisture and degree of hydration field in hardening concrete structure, the stress development is determined by incremental structural formulation derived from the principle of virtual work. In this study, the stress development is related to thermal and shrinkage deformation, and resulting stress relaxation due to the effect of early-age creep. From the experimental and numerical results it is found that the early-age creep p)ays important role in evaluating the accurate stress state. The developed analysis program can be efficiently utilized as a useful tool to evaluate the thermal and shrinkage stresses and to find measures for avoiding detrimental cracking of concrete structures at early ages.

Strength and Earth Pressure Characteristics of Industrial Disposal Flowable Filling Materials Utilizing Backfiller (뒤채움재로 사용된 산업폐기물 유동화 처리토의 강도 및 토압특성)

  • Bang, Seongtaek
    • Journal of the Korean GEO-environmental Society
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    • v.22 no.3
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    • pp.5-13
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    • 2021
  • Due to population growth and industrial development, the amount of industrial waste is increasing every year. In particular, in a thermal power plant using finely divided coal, a large amount of coal ash is generated after combustion of the coal. Among them, fly ash is recycled as a raw material for cement production and concrete admixture, but about 20% is not utilized and is landfilled. Due to the continuous reclamation of such a large amount of coal ash, it is required to find a correct treatment and recycling plan for the coal ash due to problems of saturation of the landfill site and environmental damage such as soil and water pollution. In recent years, the use of a fluid embankment material that can exhibit an appropriate strength without requiring a compaction operation is increasing. The fluid embankment material is a stable treated soil formed by mixing solidifying materials such as water and cement with soil, which is the main material, and has high fluidity before hardening, so compaction work is not required. In addition, after hardening, it is used for backfilling or filling in places where compaction is difficult because higher strength and earth pressure reduction effect can be obtained compared to general soil. In this study, the possibility of use of fluidized soil using high water content cohesive soil and coal ash is considered. And it is intended to examine the flow characteristics, strength, and bearing capacity characteristics of the material, and to investigate the effect of reducing the earth pressure when applied to an underground burial.

Evaluation of Tension Behavior in FRP Hybrid Bar Affected by UV Exposure and Freezing/Thawing Tests (UV 폭로 및 동결융해 시험을 거친 FRP Hybrid Bar의 인장거동 평가)

  • Yoon, Yong-Sik;Park, Jae-Sung;Park, Ki-Tae;Kwon, Seung-Jun
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.5 no.2
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    • pp.130-136
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    • 2017
  • The present work is for an evaluation of tension behavior and surface deterioration of FRP Hybrid Bar due to UV exposure and freezing/thawing(F/T) actions. For the work, FRP Hybrid Bar is subjected to UV exposure test, then F/T test is performed successively to 180 cycles. In FRP Hybrid Bar, no significant surface deterioration is evaluated after UV exposure. Tension hardening performance, a unique engineering advantage of FRP Hybrid Bar, is still maintained after F/T test. The performance in FRP Hybrid Bar exposed to UV is still effective. FRP Hybrid Bar exposed to UV have almost similar tension behavior of FRP Hybrid Bar without UV exposure. Although F/T cycles increase to 180, steel rebar, FRP Hybrid Bar, and FRP Hybrid Bar exposed to UV show no significant changes in tension behavior. In the work, UV exposure and F/T actions are evaluated to have little negative effect on surface deterioration and tensile performance in FRP Hybrid Bar, however spalling of silica coating due to impact should be considered since it affects bonding strength to outer concrete.

The High Temperature Deformation Behavior of Mechanically (기계적 합금화된 Al-8wt% Fe분말의 고온 변형거동)

  • Jo, Gwon-Gu;Lee, Do-In;An, In-Seop;Heo, Bo-Yeong;Jo, Jong-Chun;Kim, Seon-Jin;Mun, In-Hyeong
    • Korean Journal of Materials Research
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    • v.3 no.1
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    • pp.50-57
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    • 1993
  • Abstract The sintering behavior of the mechanically alloyed AI-8wt%Fe power during vacuum hot pressing was investigated and high temperature deformation behavior of the sintered specimen was studied through compression tests at various strain rates in the temperature range between 35$0^{\circ}C$ and 45$0^{\circ}C$. In 'addition, thermal stablity of the sintered specimem was examined by hardness measurement after annealing the spcimem for 60 hours in the temperature range of 30$0^{\circ}C$ ~50$0^{\circ}C$. The compressive stress increased rapidly with strain and reached the maximum point at the strain about 3%. With slight decrement after reaching the maximum point, the flow stress became constant up to the strain of 30% and it was considered to be due to equilibrium between work hardening and dynamic recrystallization. The hardness of the 60 hrs annealed specimens began to decrease rapidly at 40$0^{\circ}C$ .

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Effects of face-sheet materials on the flexural behavior of aluminum foam sandwich

  • Xiao, Wei;Yan, Chang;Tian, Weibo;Tian, Weiping;Song, Xuding
    • Steel and Composite Structures
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    • v.29 no.3
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    • pp.301-308
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    • 2018
  • Properties of AFS vary with the changes in the face-sheet materials. Hence, the performance of AFS can be optimized by selecting face-sheet materials. In this work, three types of face-sheet materials representing elastic-perfectly plastic, elastic-plastic strain hardening and purely elastic materials were employed to study their effects on the flexural behavior and failure mechanism of AFS systematically. Result showed face-sheet materials affected the failure mechanism and energy absorption ability of AFS significantly. When the foam cores were sandwiched by aluminum alloy 6061, the AFS failed by face-sheet yielding and crack without collapse of the foam core, there was no clear plastic platform in the Load-Displacement curve. When the foam cores were sandwiched by stainless steel 304 and carbon fiber fabric, there were no face-sheet crack and the sandwich structure failed by core shear and collapse, plastic platform appeared. Energy absorption abilities of steel and carbon fiber reinforced AFS were much higher than aluminum alloy reinforced one. Carbon fiber was suggested as the best choice for AFS for its light weight and high performance. The versus strength ratio of face sheet to core was suggested to be a significant value for AFS structure design which may determine the failure mechanism of a certain AFS structure.