• 보존과학연구
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• s.34
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• pp.20-29
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• 2013

Paper, textile and wood materials are mainly consisted of cellulose. Cellulose is high molecule and make up the strong crystalline structure by hydrogen bonds. In particular, the polymerization degree of cellulose are closely related to the strength of fiber, and the permanence. the useful life of fiber, also depends on the degradation of this substance. The viscosity of cellulose is considered to be an important indicator of fiber damage in high molecule polymers. The viscosity measurements with CED solution is used to measure the molecular weight and the degree of polymerization of cellulose. Cellulose viscosity of wood fibers is measured with TAPPI standard method T230. However, TAPPI standard method T230 is difficult to completely dissolving the cellulose of high molecular weight and large degree of polymerization, such as Korea traditional papers and fabrics made with mulberry, ramie, cotton fibers. In this study, The high viscosity of hanji and fabric was measured with TAPPI standard method T254. T254 method is that the cellulose specimen with the proper amount of weaker (0.167M CED) solution, and completely dissolved with the stronger (1.0M CED) solution. It was found that cellulose with high degree of polymerization was dissolved more easily in general CED method.

• 한국문화재보존과학회:학술대회논문집
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• 2004.10a
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• pp.33-42
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• 2004

The forged iron axe found in the No. 2 wood-framed tomb (the middle 3rd century) of Hwangseongdong, Gyeongju is rectangular on the plane level. It shows an obtuse angle in the edge part, while the joint part has the both sides folded up and shows the traces of wood. Under the reflected light, the Iron axe shines in metal luster, which is bright light gray or light creamy colors. The result of x-ray diffraction analysis shows that the axe consists of magnetite and geothite, which can explain why the composition and structure of the original ore has been kept intact. The microtexture of the axe has the irregular network of ferrite and pearlite, and tile cementite of tiny amount in the ferrite background. The overall treatment of the texture seems to be thermal with a high ratio of carbon. There are fine-grained magnetite, wolframite, quartz, calcite, mica, hornblende and pyroxene inside the axe. Those must be the impurities that they failed to remove in the refining process. The normal ferrite is composed of pure iron whose $Fe_2O_3$ proportion is from 99.16 to $99.84\;wt.\%$. Other than them, the ferrite parts usually contain $Al_2O_3\;and\;SiO_2$. The irregular network of pearlite also contains Impurities including $Al_2O_3\;and\;SiO_2$ and shows highly diverse patterns of carbon content. It's because the axe was carburized after the material was made to resemble pure iron. The decarbonization work didn't go well along the process marks. It's estimated that the original ore was bloom produced in low-temperature reduction and formed around in $727^{\circ}C$, which is eutetic temperature.

• Journal of the Korean Wood Science and Technology
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• v.51 no.4
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• pp.295-308
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• 2023

This study applied a real-time IoT (Internet of Things) environmental monitoring system to wooden cultural heritages (WCHs) located in suburbs and forests in Korea. It automated the graphs of seasonal Temperature (T) and relative humidity (RH) changes inside the heritage structures and seasonal Performance Index (PI) values. While utilizing line graphs of the existing T and RH change trends and a bar graph expressing the PI values, this study examined the current status of the conservation environment inside the WCHs throughout the year and its diagnosis. Consequently, at higher latitudes, the organic cultural heritage repeatedly experienced large T fluctuations, and the risk of physical and chemical degradation of the materials was greater. However, the RH showed significant seasonal differences, even within the same latitude, indicating that the impact of latitude was not significant. Therefore, the staff in charge must manage RH by considering the surrounding environmental conditions and adjusting the internal environment of the structures. The PI values for the year-round T and RH inside the heritages were confirmed to only be a maximum of approximately 60% of the environmental suitability for conservation throughout the year, depending on the season. The relationship between the germination and growth potential period of xerophilic fungi and the monthly internal temperature and humidity in five heritages located at different latitudes was analyzed. As a result, we could thus determine that four particular months of the year (June-September) represent the periods with the highest risk of damage from xerophilic fungi in the country, regardless of latitude.

• 보존과학연구
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• s.31
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• pp.155-171
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• 2010

Wooden cultural heritages have many factors of fires and structural characteristics vulnerable to the fire extinguishing. Also, they are surrounded with forests and so remote from fire stations, which make it difficult to handle it quickly when fires break out. Wooden cultural heritages made of wood materials belong to the general fire in a Class A. Taking characteristics such as a smoldering and a backfire from the that fire of wooden materials into consideration, extinguishing the fire by the cooling system is the most effective. If the fire can't be put out at the early stage, it is almost impossible to protect wooden cultural heritages from the fire, because wooden structures can be destroyed in a high temperature and in a short time and it takes around average 7 minutes to reach its peak of flames in the process of a fire. According to the geographical and environmental situation of the cultural heritages, currently, the fire-prevention facilities such as the auto fire detector for the prompt detection, the water mist fire suppression system for the 1st early and urgent fire suppression and the outdoor fire hydrant and the water curtain etc. for the 2nd full-scale suppression and the prevention of the fire gaining force are being installed for the wooden cultural heritages.

• Korean Journal of Heritage: History & Science
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• v.40
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• pp.413-430
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• 2007

This study analyzed the foreign substances in waterlogged archaeological woods and compounds in soil where waterlogged archaeological wood was buried, in order to examine the relationship between burial environment and foreign substances in waterlogged archaeological wood. The XRF(X-ray Fluorescence Spectroscopy) and EDX(Energy Dispersive X-ray) analysis were conducted to examine the effect of iron(Fe) to blacken the waterlogged wood. The XRF results showed that investigated soil contained Si, Al, and Fe. Wood ash contained more sulfur and Fe than any other elements in the EDX analysis. Cellulose and hemicellulose were significantly reduced at the surface of wood, which is the blackened part of waterlogged wood. Foreign substances changed the surface color. These problems could be solved by removal of foreign substances in waterlogged archaeological wood using EDTA(Ethylene Diamine Tetra Acetic acid). The optimum condition to remove Fe from waterlogged wood by EDTA was investigated. To do this, the concentration of Fe removed was measured with various concentration of EDTA-2Na. The optimum pH of EDTA-2Na was figured to be 4.1 to 4.3. As the concentration of EDTA increased, the extracted concentration of Fe also increased. In the case of 0.4 wt% of EDTA-2Na, about 60ppm of Fe was eliminated and was stabilized after 48 hours. In the case of EDTA-3Na, the optimum pH was 7 to 8, and about 10 ppm of Fe was eliminated at 0.4 wt% of EDTA-3Na. In the case of EDTA-4Na, the optimum pH was 10 to 11, and about 20 ppm of Fe was eliminated at 0.4 wt% of EDTA-4Na. In conclusion, the iron(Fe) in waterlogged archaeological wood was removed by EDTA treatment and it increased the whiteness of the surface.

• 보존과학연구
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• s.23
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• pp.197-214
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• 2002

It is very important to determine the age of the Cultural Properties in archeology. In about 1950, W.F. Libby and a team of scientists at the University of Chicago developed the Radiocarbon Dating technique. Radiocarbon($^14$C) Dating is probably one of the most widely used and best known absolute dating methods. Radiocarbon ages are conventionally specified to the year 1950. This year is 0 BP year. BP is the initial of Before Present. The $^14$C within an organism is continually decaying into stable carbon isotopes. When $^14$C decays, it emits a $\beta$ - particle with an energy content of 156 KeV and becomes 14N. Only the $\beta$ - particle is detected by Liquid Scintillation Counting. $^14$C has a half life of 5730 years. It has been used to date samples as old as 50,000 years. Radiocarbon determinations can be obtained on organic material : wood, charcoal, shell, etc. The results of radiocarbon dating using Benzene Synthesizer and Liquid Scintillation Counter are KCP539 $4030\pm60$BP year, KCP540 $3980\pm60$BP year, KCP575 $4870\pm50$, KCP576 $100\pm50$BP year, KCP577 $130\pm50$BP yea and KCP578 $210\pm70$BP year.

• Journal of the Korea Furniture Society
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• v.23 no.4
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• pp.479-484
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• 2012

Tree-ring dating can be used to date scientifically prehistoric timbers, historical buildings or woodcrafts. It gives a calendar year to each tree ring and produces the felling dates of logs or wood panels. In this study, we applied tree-ring dating to a medicine cabinet in Seoul Museum of History. We obtained tree-ring data from radial or cross section by taking photographs with a digital camera. The cabinet were dated A.D. 1821 to the last ring. It was about 50 year older than the previous medicine cabinets. Tree-ring patterns indicated that the origin of woods for the cabinet would be near Sorak mountains.

• Journal of the Korean Wood Science and Technology
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• v.39 no.1
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• pp.33-40
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• 2011

In this study, we identified wood species used in manufacturing Streetcar No. 381 from Seoul Museum of History. This Streetcar No. 381 is an important cultural heritage as one of the 2 streetcars remained in Seoul. It is important to preserve this streetcar through restoration and to maintain without any damage or degradation. The information on species of wood members should be needed for its original restoration. Thus, 6 interior and 1 exterior wood members were sampled and identified microscopically. Among the 7 wood members identified, 2 were found to be douglas-fir ($Pseudotsuga$), 2 lauan ($Shorea$), 1 exotic hard pine of ponderosa group ($Pinus$), 1 larch ($Larix$), and 1 oak of cerris group ($Quercus$), respectively.

• Journal of Conservation Science
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• v.30 no.4
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• pp.329-334
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• 2014

A scientific analysis of ancient textiles provides significant data to understand weaving techniques and culture of textiles in each region and charateristics of materials used at that time. In addition, species identification of waterlogged wooden objects is a scientific analysis method that allow us to verify information of relation of foreign species trade and exchange, of preferable species through kinds of wooden products, and of forest environment as well as method setting of conservation. As a result of a species analysis about historical textiles and a wooden comb in a bronze bowl that were excavated from Hapgang-ri, Dong-Myun, Yungi-gun, Chungcheongnam-do, Textile1 and Textile3 are identified as Urticacese Boehmeri nivea ; ramie, Textie2 is identified as Malvaceae Gossypium herbaceum, and a wooden comb is identified as Betulaceae Betula spp. It is expected that this result will help to make further comparative studies, identifying species of textiles and trees of ancient times.

• 한국문화재보존과학회:학술대회논문집
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• 2005.11a
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• pp.122-134
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• 2005

XRF, EDX, IR analysis was conducted to figure the effect of Fe to blacken the waterlogged wood. The results showed that investigated soil contained more Fe than normal soil by XRF analysis and wood ash contained more sulfur and Fe than any other element by EDX analysis. C-H and C-O peaks were significantly reduced at the surface of wood where is blackened part of waterlogged wood by IR analysis. The optimum condition to remove Fe from waterlogged wood by EDTA was investigated. To do this, removed concentration of Fe was measured at various concentration of EDTA-2Na. The optimum pH of EDTA-2Na was figured to be 4.1 to 4.3 and as the concentration of EDTA was increasing, extracted concentration of Fe was also increased. In the case of 0.4 wt% of EDTA-2Na, 700ppm of Fe was eliminated and was stabilized after 48 hours time lapse. In the case of EDTA-3Na, the optimum pH was 7 to 8, and 10 ppm of Fe was eliminated at 0.4 wt% of EDTA-3Na. In the case of EDTA-4Na, the optimum pH was 10 to 11, and 120 ppm of Fe was eliminated at 0.4 wt% of EDTA-4Na.