• Proceedings of the Korean Vacuum Society Conference
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• 2014.02a
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• pp.273.1-273.1
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• 2014

Graphene, a two dimensional plane structure of $sp^2$ bonding, has been promised for a new material in many scientific fields such as physics, chemistry, and so on due to the unique properties. Chemical vapor deposition (CVD) method using transitional metals as a catalyst can synthesize large scale graphene with high quality and transfer on other substrates. However, it is difficult to control the number of graphene layers. Therefore, it is important to manipulate the number of graphene layers. In this work, homogeneous solid solution of Cu and Ni was used to control the number of graphene layers. Each films with different thickness ratio of Cu and Ni were deposited on $SiO_2/Si$ substrate. After annealing, it was confirmed that the thickness ratio accords with the composition ratio by X-ray diffraction (XRD). The synthesized graphene from CVD was analyzed via raman spectroscopy, UV-vis spectroscopy, and 4-point probe to evaluate the properties. Therefore, the number of graphene layers at the same growth condition was controlled, and the correlation between mole fraction of Ni and the number of graphene layers was investigated.

• Water Engineering Research
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• v.1 no.3
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• pp.209-222
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• 2000

A spectral formalism was applied to quantify the sampling errors due to spatial and/or temporal gaps in soil moisture measurements. The lack of temporal measurements of the two-dimensional soil moisture field makes it difficult to compute the spectra directly from observed records. Therefore, the space-time soil moisture spectra derived by stochastic models of rainfall and soil moisture was used in their record. Parameters for both models were tuned with Southern Great Plains Hydrology Experiment(SGP'97) data and the Oklahoma Mesonet data. The structure of soil moisture data is discrete in space and time. A design filter was developed to compute the sampling errors for discrete measurements in space and time. This filter has the advantage in its general form applicable for all kinds of sampling designs. Sampling errors of the soil moisture estimation during the SGP'97 Hydrology Experiment period were estimated. The sampling errors for various sampling designs such as satedlite over pass and point measurement ground probe were estimated under the climate condition between June and August 1997 and soil properties of the SGP'97 experimental area. The ground truth design was evaluated to 25km and 50km spatial gap and the temporal gap from zero to 5 days.

• Proceedings of the Korean Vacuum Society Conference
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• 2010.08a
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• pp.85-85
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• 2010

Graphene, the building block of graphite, is one of the most promising materials due to their fascinating electronic transport properties. The pseudo-two-dimensional sp2 bonding in graphene layers yields one of the most effective solid lubricants. In this poster, we present the correlation between electrical and nanomechanical properties of graphene layer grown on Cu/Ni substrate with CVD (Chemical Vapor Deposition) method. The electrical (current and conductance) and nanomechanical (adhesion and friction) properties have been investigated by the combined apparatus of friction force microscopy/conductive probe atomic force microscopy (AFM). The experiment was carried out in a RHK AFM operating in ultrahigh vacuum using cantilevers with a conductive TiN coating. The current was measured as a function of the applied load between the AFM tip and the graphene layer. The contact area has been obtained with the continuum mechanical models. We will discuss the influence of mechanical deformation on the electrical transport mechanism on graphene layers.

• Implantology
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• v.22 no.4
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• pp.210-218
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• 2018

Purpose: The purpose of this study was to investigate the validity and reproducibility of a method based on cone-beam computed tomography (CBCT) technology for the visualization and measurement of gingival soft-tissue dimensions. Material and Methods: A total of 66 selected points in soft-tissue of the ex vivo head of an adult pig were investigated in this study. For the measurement of radiographic thickness (RT), wet soft-tissue surfaces were lightly covered with barium sulfate powder using a powder spray. CBCT was taken and DICOM files were assessed for soft-tissue thickness measurement at reference points. A periodontal probe and a rubber stop were used for the measurement of trans-gingival probing thickness (TPT). After flap elevation, actual thickness of soft-tissue (actual thickness, AT) was measured. Correlation analysis and intraclass correlation coefficients analysis (ICC) were performed for AT, TPT, and RT. Results: All variables were distributed normally. Strong significant correlations of AT with RT and TPT values were found. The two ICC values between TPT vs. AT and RT vs. AT differed significantly. Conclusion: Our results indicated that correlation of RT was stronger than that of TPT with AT. We concluded that soft tissue measurement with CBCT could be a reliable method, compared to the trans-gingival probing measurement method.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.36 no.1
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• pp.29-35
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• 2023

Herein we investigated the effect of the conductive agent on the electrochemical performance of the SiOx anode. SiOx anodes have a relatively low volume expansion (~160%) compared to Pure-silicon, but have a problem in that they have a poor electrical conductivity characteristic. In this study, physical and electrochemical measurements were performed using two 0-dimensional amorphous carbon conductive agents with different crystallinity and surface area. The crystal structure of the conductive agents and the local graphitization degree were analyzed through XRD and Raman, and the surface area of the particles was observed through BET. In addition, the electrical performance according to the graphitization degree of the conductive agents was confirmed through a 4-point probe. As a result of the electrochemical cycle and rate performance, it was confirmed that the performance of SiOx using a conductive agent having a low graphitization degree and a high surface area was improved. The results in this study suggest that the graphitization degree and surface area of the amorphous carbon conductive agent may play an important role in the SiOx electrode.

• Bulletin of the Society of Naval Architects of Korea
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• v.12 no.2
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• pp.59-66
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• 1975

Recently, as the dimensions of energy carriers increase, especially in draft, a reliable prediction of the ship motions at finite depths of water becomes necessary. The purpose of this paper is to probe the effect of finite water depth on the hydrodynamic forces and ship motions, particularly heave and pitch, in longitudinal regular head waves, by comparing the experimental value of Freakes and Keay with the author's theoretical value obtained by applying the modified strip theory to the Mariner class ship. It is confirmed that generally the hydrodynamic coefficients in the equations of motion increase with decreasing water depth, and the wave exciting forces and moments decrease with decreasing water depth. Amplitudes of heave and pitch in longitudinal regular head waves decrease as the water depth in the range where the length of the incident wave is comparatively long. The effects of Froude Number on the hydrodynamic coefficients increase with decreasing water depth and is more noticeable in the case of heave than pitch. In heave, generally the discrepancy between the experimental value and the theoretical value is relatively small in the case of $F_n=O$, but it is very large in the case of $F_n=0.2$. It is considered that the trend stems from the ignorance of the three dimensional effect and the other effects due to shallowness of water on the hydrodynamic coefficients in the theoretical calculation. An extension of methods for calculating the two dimensional hydrodynamic forces to included the effect of forward speed should be recommended. It is required that more experimental works in finite water depths will be carried out for correlation studies between the theoretical calculation, according tp modified strip theory, and model experiments.

• Journal of Plant Biology
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• v.34 no.2
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• pp.121-127
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• 1991

Total soluble proteins from three developmental stages of induced root nodules of Canavalia lineata were compared with those of non-nodulated roots by SDS-PAGE and two dimensional (2-D) gel electrophoresis. Thirteen nodule-specific protein (nodulin) bands were identified by the former and 30 nodule specific protein spots were detected by the latter method respectively. Some of the nodulins were detected differentially depending on the nodule's developmental stages. For example, only three leghemoglobin (Lb)-like protein spots appeared at stage I (d<2 mm), but two additional Lb-like protein spots appeared at stage II (d <4-5 mm). pI value and molecular weight of nomomers of Lb-like protein were narrower and greater than those of soybean, ranging from 4.4 to 5.0 and 15.7 kd respectively. Northern blot hybridization of total RNAs from roots and root nodules using soybean Lb cDNA as a probe made it clear that Lb gene was expressed tissue-specifically only in the root nodules.odules.

• Journal of the Korean Society for Precision Engineering
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• v.23 no.8 s.185
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• pp.72-79
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• 2006

We measured grating pitch standards using optical diffractometry and analyzed measurement uncertainty. Grating pitch standards have been used widely as a magnification standard for a scanning electron microscope (SEM) and a scanning probe microscope (SPM). Thus, to establish the meter-traceability in nano-metrology using SPM and SEM, it is important to certify grating pitch standards accurately. The optical diffractometer consists of two laser sources, argon ion laser (488 nm) and He-Cd laser (325 nm), optics to make an incident beam, a precision rotary table and a quadrant photo-diode to detect the position of diffraction beam. The precision rotary table incorporates a calibrated angle encoder, enabling the precise and accurate measurement of diffraction angle. Applying the measured diffraction angle to the grating equation, the mean pitch of grating specimen can be obtained very accurately. The pitch and orthogonality of two-dimensional grating pitch standards were measured, and the measurement uncertainty was analyzed according to the Guide to the Expression of Uncertainty in Measurement. The expanded uncertainties (k = 2) in pitch measurement were less than 0.015 nm and 0.03 nm for the specimen with the nominal pitch of 300 nm and 1000 nm. In the case of orthogonality measurement, the expanded uncertainties were less than $0.006^{\circ}$. In the pitch measurement, the main uncertainty source was the variation of measured pitch values according to the diffraction order. The measurement results show that the optical diffractometry can be used as an effective calibration tool for grating pitch standards.

• Journal of the Korean Magnetic Resonance Society
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• v.12 no.1
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• pp.14-25
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• 2008

To investigate the 3-bond connectivity of human brain metabolites by scalar coupling interaction through 2D-correlation spectroscopy (COSY) techniques using high field NMR spectroscopy. All NMR experiments were performed at 298K on Unity Inova 500 or 600 (Varian Inc.) equipped with a triple resonance probe head with z-shield gradient. Human brain metabolites were prepared with 10% $D_2O$. Two dimensional 2D COSY spectra were acquired with 4096 complex data points in $t_2$ and 128 or 256 increments in $t_1$ dimension. The spectral width was 9615.4 Hz and solvent suppression was achieved using presaturation using low power irradiation of the water resonance during 2s of relaxation delay. NMR data were processed using VNMRJ (Varian Instrument) software and all the chemical shifts were referenced to the methyl resonance of N-acetyl aspartate (NAA) peak at 2.0 ppm. Total 10 metabolites such as N-acetyl aspartate (NAA), creatine (Cr), choline (Cho), glutamine (Gln), glutamate (Glu), myo-inositol (Ins), lactate (Lac), taurine (Tau), ${\gamma}$-aminobutyricacid (GABA), alanine (Ala) were included for major target metabolites. Symmetrical 2D-COSY spectra were successfully acquired. Total 14 COSY cross peaks were observed even though there were parallel/orthogonal noisy peaks induced by water suppression. Except for Cr, all of human brain metabolites produced COSY cross peaks. The spectra of NAA methyl proton at 2.02 ppm and Glu methylene proton ($CH_2(3)$) at 2.11 ppm and Gln methylene proton ($CH_2(3)$) at 2.14 ppm were overlapped in the similar resonance frequency between 2.00 ppm and 2.15 ppm. The present study demonstrated that in vitro 2D-COSY represented the 3-bond connectivity of human brain metabolites by scalar coupling interaction. This study could aid in better understanding the interactions between human brain metabolites in vivo 2D-COSY study. Also it would be helpful to determine the molecular stereochemistry in vivo by using two-dimensional MR spectroscopy.

• Economic and Environmental Geology
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• v.35 no.5
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• pp.465-478
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• 2002

We measured subsidences occurred in a coastal reclaimed land, Noksan industrial complex, from May 2, 1996 to February 21, 1998, using 5 interferograms of JERS-1 L-band SAR. SAR with a spatial resolution of about 16 m can detect the two-dimensional distribution of subsidence that is difficult to be estimated from in situ measurements. Accuracy of the subsidences estimated by 2-pass DInSAR was evaluated using the measurements of Magnetic Probe Extensometer (accuracy of :${\pm}$1 mm) installed at 42 stations. DInSAR measurements were well correlated with the field measurements showing an average correlation coefficient of 0.77. The correlation coefficient was further improved to be 0.87 (with RMSE of 1.44 cm) when only highly coherenced (>0.5) pixels were used. The slope of regression line was 1.04, very close to the unit value. In short, DInSAR measurements have a good linear relation with field measurements so that we can effectively detect a subsidence in the coastal reclaimed area especially using pixels of high coherence (>0.5). The maximum accumulated subsidence was about 60 cm in the study area, while the subsidence in the northern and south western areas were less than 20 cm. The resuts show that DInSAR is extremely useful for geotechnical applications as well as observation of natural deformation.