• 제목/요약/키워드: time of extraction

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추출방법을 달리한 브라운 스톡의 무기질 및 유리아미노산 분석 (The Analysis of Minerals and Free Amino Acid in Brown Stockwith Extracted Methods Varied)

  • 장혁래;이보순;최수근
    • 한국조리학회지
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    • 제14권3호
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    • pp.210-222
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    • 2008
  • This study showed that the brown stock, which is the base of demi-glace sauce, extracted by using a high pressure heating extractor is more advantageous than that extracted by the traditional extraction method for the mass production. We compared the former with the latter in terms of minerals and free amino acids. The results of this study are summarized as follows. When mineral contents were compared, the brown stock extracted by high.pressure heating extraction showed the tendency of increase in mineral contents in proportion to heating temperature and heating time, but, from extraction temperature of 140$^{\circ}C$, the contents of K, Mg, Na and P decreased with the increase of extraction time. In addition, mineral contents in the brown stock extracted by high-pressure heating extraction were generally lower than those in brown stock extracted by the traditional extraction method. This result was produced probably because materials were added repeatedly in the traditional method. Amino acids contents in brown stock according to the extraction methods were also examined. They increased with the increase in the number of extractions in the brown stock extracted by the traditional method, and those in the brown stock extracted using a high pressure heating extractor increased with the increase in heating temperature and extraction time. The results of this study are expected to be useful as a practical material for the mass production of brown stock products.

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카오스 특징 추출에 의한 용접 결함의 초음파 형상 인식 (Ultrasonic Pattern Recognition of Welding Defects Using the Chaotic Feature Extraction)

  • 이원;윤인식;이병채
    • 한국정밀공학회지
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    • 제15권6호
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    • pp.167-174
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    • 1998
  • The ultrasonic test is recognized for its significance as a non-destructive testing method to detect volume defects such as porosity and incomplete penetration which reduce strength in the weld zone. This paper illustrates the defect detection in the weld zone of ferritic carbon steel using ultrasonic wave and the evaluation of pattern recognition by chaotic feature extraction using time series signal of detected defects as data. Shown in the time series data were that the time delay was 4 and the embedding dimension was 6 which indicate the geometric dimension of the subject system and the extent of information correlation. Based on fractal dimension and lyapunov exponent in quantitative chaotic feature extraction, feature value of 2.15, 0.47 is presented for porosity and 2.24, 0.51 for incomplete penetration The precision rate of the pattern recognition is enhanced with these values on the total waveform of defect signal in the weld zone. Therefore, we think that the ultrasonic pattern recognition method of weld zone defects of ferritic carbon steel by ultrasonic-chaotic feature extraction proposed in this paper can boost precision rate further than the existing method applying only partial waveform.

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생물체(生物體)로부터 천연화합물(天然化合物) 추출(抽出)에 관한 연구(硏究) 제(第)II보(報) : 지방(脂肪)을 제거한 치자로부터 치자색(色) 색소(色素) 추출(抽出)에 관한 연구(硏究) (Studies on the Extraction of Natural Compounds from Plants and Microorganisms Part 2. Extraction of Orange-yellow Pigment from Defatted Gardenia)

  • 유주현;유승곤;양융
    • 한국식품과학회지
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    • 제7권1호
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    • pp.30-36
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    • 1975
  • 미쇄(微碎)한 치자분말(粉末)에서 Orange-Yellow 색소(色素)를 추출(抽出)하면 짧은 시간(時間)에서 $log\;t^{1{\cdot}15}$에 비례(比例)하였고 최적(最適) 추출시간(抽出時間)은 30분(分)이 선정(選定)되었으며 온도(溫度)가 상승(上昇)함에 따라 $log\;T^{3{\cdot}73}$에 비례(比例)하였고 최적(最適) 추출온도(抽出溫度)는 $40^{\circ}C$가 선정(選定) 되었으며 시료(試料) 0.1 g당(當) 용매량(溶媒量)의 증가(增加)에는 $log\;S^{3{\cdot}7}$의 색소(色素) 추출량(抽出量)을 나타냈고, 지방(脂肪)을 완전(完全)히 제거(除去)한 시료(試料)는 전혀 제거(除去)하지 않은 시료(試料)보다 $0.6(O.D\;448\;m{\mu})$만큼의 좋은 추출효과(抽出效果)를 보였다. 이들을 綜合하여, $P_{total}{\simeq}1.15\;log\;t+3.73\;log\;T+3.7\;log\;S-4X-6.4$ $P_{total}$: total amounts of extracted orange-yellow pigment from Gardenia. t: extraction time $(0.5{\sim}60\;min)$ T: extraction temperature $(5{\sim}50^{\circ}C)$ S: volume of solvent $(5{\sim}50\;ml)$ X: fat contents $(0{\sim}15%)$ 와 같은 수정(修正)된 실험식(實驗式)을 유도했다.

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스피루리나(Spirulina platensis)로부터 미백과 주름개선 생리활성 물질 분리를 위한 초음파 추출공정 개발 (Ultrasound-assisted Extraction for Development of Skin Whitening and Anti-wrinkling Cosmetic Materials from Spirulina platensis)

  • 김소희;전성진;김준희;염서희;김진우
    • 한국수산과학회지
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    • 제54권3호
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    • pp.271-279
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    • 2021
  • Ultrasound-assisted extraction (UAE) conditions, including extraction time, extraction temperature, and ethanol concentration, were optimized to increase the total flavonoid content (TFC), tyrosinase inhibitory activity (TIA), and collagenase inhibitory activity (CIA) of Spirulina platensis through central composite design (CCD). For the optimization of the three dependent variables, a quadratic regression model was derived from 17 experimental sets for the simultaneous maximization of TFC, TIA, and CIA. The predicted optimal UAE conditions were 44.0 min of extraction time, 82.8℃ of extraction temperature, and 96.0% of ethanol concentration. Under these conditions, 0.93 mg QE/g DM of TFC, 81.9% of CIA, and 92.1% of TIA were predicted. The CCD-based UAE optimization enabled an increase in TFC, CIA, and TIA, thereby confirming that the S. platensis extract can be used in the development of a cosmetic material with skin whitening and anti-wrinkle effects.

Optimization of Extraction Conditions for the Antibacterial Activity by Clove against Streptococcus mutans Using Evolutionary Operation-Factorial Design Technique

  • Choi, Ung-Kyu;Kim, Mi-Hyang;Kwon, Dae-Jun;Kwon, O-Jun;Lee, Nan-Hee
    • Food Science and Biotechnology
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    • 제17권5호
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    • pp.899-903
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    • 2008
  • This study was conducted in order to elucidate the optimum conditions for the extraction of clove that can be used to elicit antibacterial activity against Streptococcus mutans using the evolutionary operation (EVOP)-factorial design technique. Higher antibacterial activity was achieved in a higher extraction temperature of $80^{\circ}C$ ($r=0.7983^{**}$) and in a longer extraction time of 26 hr ($r=0.6867^*$). Antibacterial activity was not effected by differentiation of ethanol concentration in the extraction solvent (r=-0.0683). The maximum antibacterial activity of clove against S. mutans as determined by the EVOP-factorial design technique was obtained at an extraction temperature of $80^{\circ}C$, an extraction time of 26 hr and a 50% ethanol concentration. Furthermore, the population of S. mutans decreased from an initial concentration of 6.850 to 4.195 log CFU/mL in the third set that is more than 2.6 log cycles by EVOP-factorial design technique.

Optimum Conditions for the Extraction of Effective Substances from the Stem of Opuntia fiscus-indica

  • Lee, Gee-Dong;Kim, Jung-Ok;Joo, Gil-Jae;Kwon, Joong-Ho
    • Food Science and Biotechnology
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    • 제14권2호
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    • pp.190-195
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    • 2005
  • The conditions for the extraction of effective substances from the stem of Opuntia ficus-indica were optimized by a response surface methodology. The total extract yield was maximized under the temperature of $97.77^{\circ}C$, at a time duration of 145.82 min and a water to sample ratio 16.59 mL/g. Moreover, the optimum conditions for the extraction of effective substances were as follows: $84.95^{\circ}C$, 156.50 min and a water/sample ratio of 7.46 mL/g for the phenolics content; and $97.11^{\circ}C$, 139.03 min and a water/sample ratio of 10.91 mL/g for the pectin content. The range of optimum extraction conditions in consideration of the physicochemical properties of the extracts were shown to be as $95-100^{\circ}C$ as the extraction temperature, 120-180 min as extraction time and a water to sample ratio of 5-18 mL/g.

Extraction of La(III) by a nonionic microemulsion containing D2EHPA in hollow fiber contactor

  • Ou, Huilin;Gong, Fuzhong;Tang, Yanxia;Luo, Yan;Liu, Liheng
    • Membrane and Water Treatment
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    • 제12권2호
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    • pp.75-82
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    • 2021
  • This study aimed to prepare a W/O nonionic microemulsion system(MEs) consisting of OP-4[polyoxyethylene(4) nonylphenol], OP-7[polyoxyethylene(7) nonylphenol], 1-hexanol, D2EHPA, kerosene and HCl solution and applied to the extraction of La(III) from chloride aqueous solution within the polysulfone hollow fiber contactor (HFC),laboratory-scale experiments were carried out to investigate the recovery of La(III) using as-prepared microemulsion from the simulation wastewater containing La(III),Al(III) and Fe(III). The right weight ratio(Rs) of OP-4 to OP-7 was firstly confirmed through determination of the solubilization capacity of HCl solution(W0,HCl) in microemulsion, the effect of several factors such as the HCl concentration, temperature and effective extraction time on the extraction efficiency of La(III) was discussed. Results showed that the acceptable Rs was 4:6 to prepare the W/O MEs. The extraction yield of La(III) increased with the increasing of HCl concentration, temperature and effective extraction time and reaches to 97.3% while using five-stage modules. The recovery yield of La(III) from simulation La-bearing wastewater was 90.6%.

생물체(生物體)로부터 천연화합물(天然化合物) 추출(抽出)에 관한 연구(硏究) -제(第) 1 보(報) 치자(梔子)로부터 치자색(色)(Orange-Yellow) 색소(色素)의 추출(抽出)에 관한 연구(硏究)- (Studies on the Extraction on Natural Compounds from Plants and Microorganisms -Part 1. Extraction of Orange-Yellow Pigment from Gardenia-)

  • 유주현;홍윤명;유승곤;김유삼
    • 한국식품과학회지
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    • 제6권1호
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    • pp.1-5
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    • 1974
  • The extraction mode of orange-yellow pigment from Gardenia is depended upon the extraction time, extraction temperature and volume of solvent. The amounts of the extracted-pigment (C) is proportional to the log ${\theta}^{1.15}$ of extraction time $({\theta}:0{\cdots}{\cdots}{\cdots}60$ min.), the log $T^{3.73}$ of extraction temperature $(T:5{\cdots}{\cdots}{\cdots}60^{\circ}C)$ and the log $S^{3.7}$ of volume of solvent $(S:5{\cdots}{\cdots}{\cdots}50ml)$ at $18^{\circ}C$ for 10 minutes. Finally, the general emperical equation was derived as follows; C=1.15 log ${\theta}$+3.73 log T+3.7 log S-7.0

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BBD-RSM을 이용한 민들레로부터 항산화성분의 추출공정 최적화 (Optimization of Antioxidant Extraction from Dandelion (Taraxacum officinale) Leaves Using BBD-RSM)

  • 한경호;장현식;홍인권
    • 공업화학
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    • 제30권4호
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    • pp.408-414
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    • 2019
  • 본 연구에서는 전통적인 열수추출법과 초음파 추출법을 이용하여 민들레에서 항산화성분을 추출하였다. 추출 후 추출수율과 항산화성분인 플라보노이드 함량을 최적화하기 위해 반응표면분석법 중 Box-Behnken 설계모델을 이용하여 추출하였다. 열수추출법의 경우 추출온도, 주정/초순수 부피비, 추출시간을 변수로 설정하였으며, 초음파 추출법의 경우 초음파 조사세기, 주정/초순수 부피비, 초음파 조사시간을 변수로 설정하였다. 열수추출법의 최적 추출조건은 추출온도($45.76^{\circ}C$), 주정/초순수 부피비(41.92 vol.%), 추출시간(1.75 h)이었다. 또한 초음파 추출법의 최적조건은 초음파 조사세기(512.63 W), 주정/초순수 부피비(56.97 vol.%), 추출시간(20.79 min)이었다. 이 조건에서 예상되는 반응치는 수율(22.09 wt.%), 플라보노이드 함량(28.98 mg QE/mL dw)으로 산출되었다. 또한 실제실험 결과 오차는 3% 이하로 나타나 최적화의 타당성을 입증하였다.

Extraction of Docosahexaenoic Acid (DHA) from Lyophilized Thraustochitrium sp.

  • CHO, JOONG-HOON;GWI-SUK HEO;JI-WON YANG
    • Journal of Microbiology and Biotechnology
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    • 제6권5호
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    • pp.358-360
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    • 1996
  • Solvent extraction, soxhlet method, and supercritical fluid extracion were considered, respectively, as the method of choice for the recovery of DHA from lyophilized Thraustochitrium sp., and the results of corresponding extraction were compared. Supercritical fluid extraction seems to be the most appropriate process with respect to time, process simplicity, and extractant intoxicity.

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