• Title/Summary/Keyword: thermal treatment.

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Chemical Composition of Thermal Treatment Yam (Dioscorea batatas DECNE.)

  • Kim, Han-Soo;Duan, Yishan;Ryu, Jae-Young;Kim, Sang-Woo;Jang, Seong-Ho
    • Journal of the Korean Applied Science and Technology
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    • v.32 no.1
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    • pp.7-15
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    • 2015
  • In this study, the thermal treatment yam (Dioscorea batatas DECNE.) was analyzed for its proximate and nutritional compositions including mineral, vitamin, amino acids and fatty acids. Thermal treatment yam is mainly consisted of carbohydrate (70.3%) with small amounts of crude protein (15.8%), crude ash (5.1%) and crude fat (1.6%). It was found to be a good source of essential minerals such as K (1100.2 mg/100 g), Mg (99.4 mg/100 g), Ca (54.8 mg/100 g) and Na (44.9 mg/100 g) but Zn (4.8 mg/100 g) and Fe (0.2 mg/100g) content was low. Little amounts of vitamin E (8.3 mg/100g), vitamin C (3.5 mg/100g) and vitamin B1 (2.1 mg/100g) could be found. The amino acid analysis revealed that the yam was superior with respect to serine (1454.2 mg%), lysine (684.6 mg%) and histidine (684.6 mg%). Essential amino acids were calculated to be 2849.3 mg%. The amino acid profiles showed that thermal treatment yam is limiting in isoleucine and phenylaline. Linoleic acid was the most predominant fatty acids with the value of 47.3% followed by palmitic acid (24.7%) and oleic acid (12.7%). And the unsaturated fatty acids including oleic acid and linoleic acid were present in big quantities in thermal treatment yam.

Effects of Antioxidant and Thermal Treatment on the Radiation Resistance of Polypropylene (폴리프로필렌의 내방사선성에 미치는 산화방지제와 열처리의 영향)

  • Park Sung Hyun;Kim Hyung-Il;Kang Phil Hyun;Nho Young Chang
    • Polymer(Korea)
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    • v.30 no.1
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    • pp.10-13
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    • 2006
  • The effects of antioxidants and thermal treatment on the radiation resistance of the gamma-ray irradiated polypropylene (PP) were studied. The PP was blended with various antioxidants and was fabricated into a sheet. The PP sheet was irradiated with gamma-ray to a dosage of 25kGy in the nitrogen atmosphere. The differences in both color and mechanical strength were investigated for the gamma-ray irradiated PP depending on the kind and the content of antioxidant. The residual amount of free radical and the variation of oxidation index were investigated for the gramma-ray irradiated PP with thermal treatment after irradiation. The PP having phosphite antioxidant showed little difference in color after gamma-ray irradiation compared with the PP having phenolic or mine antioxidant. Sufficient amount of free radical could be removed from the gamma-ray irradiated PP by the thermal treatment at $130\;^{\circ}C$ for 30 min. Thermally treated PP showed lower oxidation index than the PP without thermal treatment.

Effect of enzyme treatment on the DSC and TGA behavior of silkworm powder

  • Jo, You-Young;Bae, Sung Min;Kim, HyunBok;Lee, Kwang Gill;Kweon, HaeYong
    • International Journal of Industrial Entomology and Biomaterials
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    • v.37 no.1
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    • pp.29-32
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    • 2018
  • Silkworm powder's thermal property is an important factor for its storage and marketing. This study examined the effect of edible enzyme on the thermal property of silkworm powder using Thermogravimetric Analysis (TGA) and Differential Scanning Calorimetry (DSC). Results of the TGA showed that regardless of the enzyme treatment, the weight loss patterns of silkworm powders exhibited 3 step thermal property deterioration at approximately $80^{\circ}C$, $280^{\circ}C$, and $480^{\circ}C$ due to water evaporation and thermal degradation. This is similar with the DSC which also resulted in all samples two endothermic peaks attributed also to water evaporation and thermal degradation. These results indicated that the use of enzyme such as protease and cellulase might not affect significantly the thermal properties of silkworm powder.

Synthesis of Silicon Carbide Nano-Powder from a Silicon-Organic Precursor by RF Inductive Thermal Plasma (RF 유도 열플라즈마를 이용한 유기 용매로 부터의 탄화규소 나노 분말 합성)

  • Ko, Sang-Min;Koo, Sang-Man;Kim, Jin-Ho;Cho, Woo-Seok;Hwang, Kwang-Taek
    • Journal of the Korean Ceramic Society
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    • v.49 no.6
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    • pp.523-527
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    • 2012
  • Silicon carbide (SiC) has recently drawn an enormous amount of industrial interest due to its useful mechanical properties, such as its thermal resistance, abrasion resistance and thermal conductivity at high temperatures. In this study, RF thermal plasma (PL-35 Induction Plasma, Tekna CO., Canada) was utilized for the synthesis of high-purity SiC powder from an organic precursor (hexamethyldisilazane, vinyltrimethoxysilane). It was found that the SiC powders obtained by the RF thermal plasma treatment included free carbon and amorphous silica ($SiO_2$). The SiC powders were further purified by a thermal treatment and a HF treatment, resulting in high-purity SiC nano-powder. The particle diameter of the synthesized SiC powder was less than 30 nm. Detailed properties of the microstructure, phase composition, and free carbon content were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), a thermogravimetric (TG) analysis, according to the and Brunauer-Emmett-Teller (BET) specific surface area from N2 isotherms at 77 K.

Change in Thermal Diffusivity of Al-Si-Mg-Cu Alloy According to Heat Treatment Conditions at Automotive Engine Operating Temperature (Al-Si-Mg-Cu 합금의 자동차 엔진 사용 온도에서 열처리 조건에 따른 열확산도 변화)

  • Choi, Se-Weon
    • Korean Journal of Materials Research
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    • v.31 no.11
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    • pp.642-648
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    • 2021
  • The precipitation effect of Al-6%Si-0.4%Mg-0.9%Cu-(Ti) alloy (in wt.%) after various heat treatments was studied using a laser flash device (LFA) and differential scanning calorimetry (DSC). Solid solution treatment was performed at 535 ℃ for 6 h, followed by water cooling, and samples were artificially aged in air at 180 ℃ and 220 ℃ for 5 h. The titanium-free alloy Al-6%Si-0.4%Mg-0.9%Cu showed higher thermal diffusivity than did the Al-6%Si-0.4%Mg-0.9%Cu-0.2%Ti alloy over the entire temperature range. In the temperature ranges below 200 ℃ and above 300 ℃, the value of thermal diffusivity decreased with increasing temperature. As the sample temperature increased between 200 ℃ and 400 ℃, phase precipitation occurred. From the results of DSC analysis, the temperature dependence of the change in thermal diffusivity in the temperature range between 200 ℃ and 400 ℃ was strongly influenced by the precipitation of θ'-Al2Cu, β'-Mg2Si, and Si phases. The most important factor in the temperature dependence of thermal diffusivity was Si precipitation.

Effects of Wet Chemical Treatment and Thermal Cycle Conditions on the Interfacial Adhesion Energy of Cu/SiNx thin Film Interfaces (습식표면처리 및 열 사이클에 따른 Cu/SiNx 계면접착에너지 평가 및 분석)

  • Jeong, Minsu;Kim, Jeong-Kyu;Kang, Hee-Oh;Hwang, Wook-Jung;Park, Young-Bae
    • Journal of the Microelectronics and Packaging Society
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    • v.21 no.1
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    • pp.45-50
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    • 2014
  • Effects of wet chemical treatment and thermal cycle conditions on the quantitative interfacial adhesion energy of $Cu/SiN_x$ thin film interfaces were evaluated by 4-point bending test method. The test samples were cleaned by chemical treatment after Cu chemical-mechanical polishing (CMP). The thermal cycle test between Cu and $SiN_x$ capping layer was experimented at the temperature, -45 to $175^{\circ}C$ for 250 cycles. The measured interfacial adhesion energy increased from 10.57 to $14.87J/m^2$ after surface chemical treatment. After 250 thermal cycles, the interfacial adhesion energy decreased to $5.64J/m^2$ and $7.34J/m^2$ for without chemical treatment and with chemical treatment, respectively. The delaminated interfaces were confirmed as $Cu/SiN_x$ interface by using the scanning electron microscope and energy dispersive spectroscopy. From X-ray photoelectron spectroscopy analysis results, the relative Cu oxide amounts between $SiN_x$ and Cu decreased by chemical treatment and increased after thermal cycle. The thermal stress due to the mismatch of thermal expansion coefficient during thermal cycle seemed to weaken the $Cu/SiN_x$ interface adhesion, which led to increased CuO amounts at Cu film surface.

Principles and Applications of Non-Thermal Technologies for Meat Decontamination

  • Yewon Lee;Yohan Yoon
    • Food Science of Animal Resources
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    • v.44 no.1
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    • pp.19-38
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    • 2024
  • Meat contains high-value protein compounds that might degrade as a result of oxidation and microbial contamination. Additionally, various pathogenic and spoilage microorganisms can grow in meat. Moreover, contamination with pathogenic microorganisms above the infectious dose has caused foodborne illness outbreaks. To decrease the microbial population, traditional meat preservation methods such as thermal treatment and chemical disinfectants are used, but it may have limitations for the maintenance of meat quality or the consumers acceptance. Thus, non-thermal technologies (e.g., high-pressure processing, pulsed electric field, non-thermal plasma, pulsed light, supercritical carbon dioxide technology, ozone, irradiation, ultraviolet light, and ultrasound) have emerged to improve the shelf life and meat safety. Non-thermal technologies are becoming increasingly important because of their advantages in maintaining low temperature, meat nutrition, and short processing time. Especially, pulsed light and pulsed electric field treatment induce few sensory and physiological changes in high fat and protein meat products, making them suitable for the application. Many research results showed that these non-thermal technologies may keep meat fresh and maintain heat-sensitive elements in meat products.

Effect of Heat Treatment on the Physical Properties of LM PET Jacquard Fabrics (저융점 폴리에스터 자카드직물의 물성에 대한 열처리 효과)

  • Lee, Sun Young;Kim, Jeong Hwa;Kim, Eui Hwa;Lee, Jung Soon;Lee, Seung Goo
    • Textile Coloration and Finishing
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    • v.25 no.3
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    • pp.206-214
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    • 2013
  • There has been an increasing demand for high performance and energy-saving of blind. In order to develop the eco-friendly blind textiles, heat treatment process has been utilized for LM(Low Melting) polyester fabrics and the changes of the physical properties of the treated fabrics were examined according to temperature of heat treatment. Morphology, surface reflectance, contact angle, luster, thermal property and mechanical property of heat treated LM polyester fabrics were investigated. As results, morphology analysis of thermal treated fabrics confirmed that degree of fusion of LM polyester yarns improved with increase of temperature. Surface reflectance of thermal treated fabrics decreased with increase of temperature. Luster and contact angle of a water droplet on thermal treated fabrics increased slightly with increase of temperature. The mechanical properties of the fabrics by KES-FB system were found to be temperature-dependent and especially, bending and shear properties among them were highly related to temperature.

Mechanical and thermal properties of 3D printing metallic materials at cryogenic temperatures

  • Jangdon Kim;Jaehwan Lee;Seokho Kim
    • Progress in Superconductivity and Cryogenics
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    • v.26 no.2
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    • pp.24-30
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    • 2024
  • Metal 3D printing is utilized in various industrial fields due to its advantages, such as fewer restrictions on production shape and reduced production time and cost. Existing research on 3D printing metal materials focused on changes in material properties depending on manufacturing conditions and was mainly conducted in a room temperature environment. In order to apply metal 3D printing products to cryogenic applications, research on the properties of materials in cryogenic environments is necessary but still insufficient. In this study, we evaluate the properties of stainless steel (STS) 316L and CuCr1Zr manufactured by Laser Powder Bed Fusion (LPBF) in a cryogenic environment. CuCr1Zr is a precipitation hardening alloy, and changes in material properties were compared by applying various heat treatment conditions. The mechanical properties of materials manufactured using the LBPF method are evaluated through tensile tests at room temperature and cryogenic temperature (77 K), and the thermal properties are evaluated by deriving the thermal conductivity of CuCr1Zr according to various heat treatment conditions. In a cryogenic environment, the mechanical strength of STS 316L and CuCr1Zr increased by about 150% compared to room temperature, and the thermal conductivity of CuCr1Zr after heat treatment increased by about 6 to 10 times compared to before heat treatment at 40 K.

Effect of Copper Addition on Mechanical and Thermal Properties of SKD11 Stainless Steel (Cu 첨가에 따른 SKD11의 기계적, 열적 특성 변화)

  • Choi, Gwang Mook;Chae, Hong-Jun
    • Journal of Korea Foundry Society
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    • v.39 no.6
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    • pp.103-109
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    • 2019
  • Cu-added SKD11 was manufactured through the casting process and the effects of Cu addition with different contents (0, 1, 2 and 3 wt%) and aging treatment on microstructure, mechanical characteristics such as tensile strength and hardness, and thermal conductivity were investigated. The microstructure was analyzed by FE-SEM and XRD, the mechanical characteristics by Rockwell hardness tester and Tensile tester, and the thermal conductivity by Laser flash. As a result, SKD11 containing Cu had higher hardness than as-received SKD11. The hardness of as-cast SKD11 containing 1 wt% Cu was 42.4 HRC, whereas the hardness of asreceived SKD11 cast alloy was 19.5 HRC, indicating that the hardness was greatly improved when Cu was added. In the case of tensile strength, Cu-added SKD11 cast alloy had lower tensile strength than as-received SKD11, and the tensile strength tended to increase as Cu content increased. After heat treatment, however, tensile strength of as-received SKD11 was significantly increased, whereas in the case of Cu-added SKD11, as the Cu contents increased, the tensile strength increased less and even reduced at 3 wt% Cu. The thermal conductivity of Cu-added SKD11 cast alloy was about 13 W m-1 K-1, which was lower than that of the asreceived SKD11 cast alloy (28 W m-1 K-1). After the heat treatment, however, the thermal conductivity of as-received SKD11 was reduced, while the thermal conductivity of the SKD11 added with Cu was increased. Thermal conductivity was generally larger with less Cu content, and this tendency became more pronounced after heat treatment.