• Title/Summary/Keyword: thermal physical properties

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Identication of Bean Yellow Mosaic Virus from Trifolium repens (흰 토끼풀에서 분리한 강낭콩황반모자이크 바이러스의 동정)

  • Ryu Gab Hee;Lee Soon Hyung;La Yong Joon
    • Korean Journal Plant Pathology
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    • v.2 no.1
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    • pp.48-52
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    • 1986
  • The virus isolated from white clover, Trifolium repens showing mosaic symptom was identified as bean yellow mosaic virus (BYMV) based on the host range, physical properties, aphid transmission, serology and morphology of the virus particles. Chenopodium amaranticolor and C. quinoa produced local lesions on the inoculated leaves and chlorotic spot on the upper leaves. Broad bean and cowpea produced local lesions on the inoculated leaves and mosaic with vein necrotic symptoms on the upper leaves. French bean showed vein necrosis on the inoculated leaves, yellow mosaic on the upper leaves and bud blight. The average size of virus particles was 740nm in length. The virus was also transmitted by Myzus persicae. The thermal inactivation point of the virus isolate was $60\;to\;65^{\circ}C$, the dilution end point $10^{-3}\;-\;10^{-4}$ and the longevity in vitro was 3 days Serological tests with the virus purified from Trifolium repens were positive to BYMV antiserum.

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Preparation of Mg(OH)2 Dispersion and its Application to PET Non-woven Textile as Flame Retardant Coating (수산화마그네슘 분산상의 제조와 PET 부직포 섬유의 난연 코팅제 적용)

  • Lim, Hyung-Mi;Hyun, Mi-Kyung;Jeong, Sang-Ok;Lee, Dong-Jin;Lee, Seung-Ho
    • Journal of the Korean Ceramic Society
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    • v.48 no.6
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    • pp.537-542
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    • 2011
  • Magnesium hydroxide as a non-halogen flame retardant has increasing attention due to its non-toxicity, high decomposition temperature and smoke suppressant ability during combustion. For the application of magnesium hydroxide retardant to the textile by soaking and coating method, the prerequisite for the coating is a small particle size, stable dispersion, and adhesion to the textile. The dispersion of $Mg(OH)_2$ particles and stability of the coating was checked by monitoring the change of transmittance and backscattering by varying the types of dispersion agents, binder, solvent, and $Mg(OH)_2$ source, and their compositions in the coating. The $Mg(OH)_2$ dispersion coating was applied to PET(poly(ethylene terephthalate)) non-woven textile. The physical properties are characterized by surface morphology, amount of coating, particle dispersion, and adhesion test. The flame retardant $Mg(OH)_2$ coated textile has been compared by limited oxygen index(LOI) and thermal gravimetry and differential scanning calorimetry(TG-DSC). It was found that phosphorous additive may give synergistic effect on $Mg(OH)_2$ flame retardant coating to make the flame retardant PET non-woven textile.

A Study on the Infrared Emission Properties and Freeze-thaw Resistance for Calcined Clay by Carburization Treatment (소성 점토의 침탄에 따른 동결융해 저항성 및 적외선 방사특성 연구)

  • Kim, Ki-Ho;Kim, Sang-Myoung;Kang, Byung-Chul
    • Journal of the Korean Ceramic Society
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    • v.45 no.7
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    • pp.387-394
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    • 2008
  • The Physical property changes of calcined clay by carburization were investigated studied. The carburization mechanism is the penetration of carbon which occurred during incomplete fuel combustion into crevice of clay structure. The experiments for elasticity and freeze-thaw resistance were conducted, and the results can be summarized as follows: Dynamic modulus of elasticity and also freeze-thaw resistance of calcined clay by carburization treatment increased more than 92% after testing 300 cycle, which was more improved than 88% of calcined clay. Therefore, it can decrease the possibility of winter-sowing, which is one the weakness of calcined clay. It is on the basis of the fact that the porosity of calcined clay by carburization treatment is about 12%, which indicates smaller pore spaces comparing with the 14% of porosity of calcined clay and those values were calculated by apparent porosity show and also supported by SEM images. Infrared emissivity of calcined clay by carburization treatment and calcined clay were respectively 0.92 and 0.9l at $80^{\circ}C$. However, those values were 0.91 and 0.88 at $200^{\circ}C$, which means infrared emissivity of calcined clay by carburization treatment shows 3.6% higher than the calcined clay. Moreover, within the wavelength range from 3 to $7\;{\mu}m$, while the calcined clay had low infrared emissivity, the calcined clay by carburization treatment had increased infrared emissivity. It is inferred that it was affected by carbon element that has high infrared absorptivity within this wavelength range.

A Study on Deformation and Strength of High-Strength Polymer Composites Using Automobiles (자동차용 고강도 폴리머 복합재료의 변형과 강도에 관한 연구)

  • Im, Jae-Gyu;Sin, Jae-Hun;Park, Han-Ju;Shoji, T.;Takeda, H.
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.25 no.7
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    • pp.1082-1088
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    • 2001
  • Nowadays study on recycling disused plastics for automobiles was lively progressed. Rubber and talcum powder was added to retrieve degradation of physical properties caused by recycling disused polypropylene. The effect of the temperature, the fatigue load and the loading speed on DEN(double edged notch) specimen which was made by the pp-rubber composites during fracture was studied by. DEN specimen was made on PP-rubber composites through the injection molding. With increasing temperature the fracture strength was linearly decreased and the fracture energy was increased by $0^{\circ}C$ and after that decreased. In the same temperature the fracture strength during increasing the notch radius was hardly increased. The fracture behaviour at low and high loading speed was different entirely. At high loading speed plastic region was small and fracture behaviour was seen to brittle fracture tendency. With increasing fatigue load fracture energy was first rapidly decreased and subsequently steady when radius of notch tip was 2mm, but Maximum load during fracture scarcely varied. The deformation mechanism of polypropylene-rubber composites during fracture was studied by SEM fractography. A strong plastic deformation of the matrix ahead of the notch/crack occurred. The deformation seem to be enhanced by a thermal blunting of the notch/crack.

A Study of Reactively Sputtered Ti-Si-N Diffusion Barrier for Cu Metallization (혼합기체 sputtering 법으로 증착된 Cu 확산방지막으로의 Ti-Si-N 박막의 특성 연구)

  • Park, Sang-Gi;Lee, Jae-Gap
    • Korean Journal of Materials Research
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    • v.9 no.5
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    • pp.503-508
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    • 1999
  • We have investigated the physical and diffusion barrier property of Ti-Si-N film for Cu metallization. The ternary compound was deposited by using reactive rf magnetron sputtering of a TiSi$_2$target in an Ar/$N_2$gas mixture. Resistivities of the films were in range of 358$\mu$$\Omega$-cm, to 307941$\mu$$\Omega$-cm, and tended to increase with increasing the $N_2$/Ar flow rate ratio. The crystallization of the Ti-Si-N compound started to occur at 100$0^{\circ}C$ with the phases of TiN and Si$_3$N$_4$identified by using XRD(X-ray Diffractometer). The degree of the crystallization was influenced by the $N_2$/Ar flow ratio. The diffusion barrier property of Ti-Si-N film for Cu metallization was determined by AES, XRD and etch pit by secco etching, revealing the failure temperature of 90$0^{\circ}C$ in 43~45at% of nitrogen content. In addition, the very thin compound (10nm) with 43~45at% nitrogen content remained stable up to $700^{\circ}C$. Furthermore, thermal treatment in vacuum at $600^{\circ}C$ improved the barrier property of the Ti-Si-N film deposited at the $N_2$(Ar+$N_2$) ratio of 0.05. The addition of Ti interlayer between Ti-Si-N films caused the drastic decrease of the resistivity with slight degradation of diffusion barrier properties of the compound.

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Residual Stress Distribution on the Fillet Weldment used by Finite Element Method (유한요소법을 이용한 필렛용접 이음부의 잔류응력분포)

  • Kim, Hyun Sung;Woo, Sang Ik;Jung, Kyoung Sup
    • Journal of Korean Society of Steel Construction
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    • v.12 no.2 s.45
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    • pp.197-207
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    • 2000
  • A transient heat transfer analysis and thermo-elastic analysis have been performed for the residual stress distribution on the fillet weldment used by finite element method. Specimen is fabricated single-pass fillet welding. This computation was performed for conditions including surface heat flux and temperature dependent thermo-physical properties using by heat input as parameter. Also, cut-off temperature of residual stress estimation by thermo-elastic analysis is determined. The fillet weldment were measured to determined their residual stress distributions for using hole-drilling method. As result, it was found that large tensile residual stress is about material yield strength, and the numerical simulation results for finite element method similar to residual stresses by hole-drilling method and other exiting research. Also, cut-off temperature is effectively determined by temperature which calculated maximum thermal stress equal to material yield strength.

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Effect of Whey Protein Isolate on Ice Recrystallization Characteristics in Whey Protein Isolate/κ-Carrageenan Matrix

  • Chun, Ji-Yeon;Kim, Ji-Min;Min, Sang-Gi
    • Food Science of Animal Resources
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    • v.32 no.5
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    • pp.627-634
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    • 2012
  • This study was carried out to investigate the physical and thermal properties of ${\kappa}$-carrageenan (${\kappa}$-car) gel added whey protein isolate (WPI) as a cryoprotectant. The concentration of ${\kappa}$-carrageenan was fixed at 0.2 wt%. The mean ice crystal size of the WPI/${\kappa}$-car was decreased according to increasing whey protein isolate concentration. The temperature of gel-sol (Tg-s) and sol-gel (Ts-g) transition of WPI/${\kappa}$-car maxtrix was represented in the order of 3.0, 0.2, 5.0 and 1.0 wt%. In addition, the transition temperature of gel-sol of WPI in sucrose solution were showed in order of 1.0, 5.0, 0.2 and 3.0 wt% depending on whey protein isolate concentration. The shape of ice crystal was divided largely into two types, round and rectangular form. 1.0 wt% WPI/${\kappa}$-car matrix at pH 7 and 9 showed minute and rectangular formation of ice crystals and whey protein isolate in sucrose solution at a concentration of 1.0 wt% WPI/${\kappa}$-car matrix at pH 3 and 5 showed relatively large size and round ice crystals. The ice recrystallization characteristics and cryprotective effect of ${\kappa}$-carrageenan changed through the addition of different concentrations of whey protein isolate. It seems that the conformational changes induced interactions between whey protein isolate and ${\kappa}$-carrageenan affected ice recrystallization.

Measurement of Properties of Domestic Bentonite for a Buffer of an HLW Repository (고준위폐기물 처분장의 완충재용 국내산 벤토나이트의 특성 측정)

  • Yoo, MalGoBalGaeBitNaLa;Choi, Heui-ju;Lee, Min-soo;Lee, Seung-yeop
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.14 no.2
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    • pp.135-147
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    • 2016
  • The buffer in geological disposal system is one of the major elements to restrain the release of radionuclide and to protect the container from the inflow of groundwater. The buffer material requires long-term stability, low hydraulic conductivity, low organic content, high retardation of radionuclide, high swelling pressure, and high thermal conductivity. These requirements could be determined by the quantitative analysis results. In case of South Korea, the bentonites produced in Gyeongju area have been regarded as candidate buffer/backfill materials at KAERI (Korea Atomic Energy Research Institute) since 1997. According to the study on several physical and chemical characteristics of domestic bentonite in the same district, this is the Ca-type bentonite with about 65% of montmorillonite content. Through this study, we present the criteria for the performance evaluation items and methods when collecting new buffer/backfill materials.

An Addition Effect of Amine and Cethyl Trimethyl Ammonium Bromide on Alkali-treatment of Polyester (폴리에스테르직물의 수산화나트륨 처리시 아민과 CTAB의 첨가효과)

  • Lee Jung Soon;Ryu Hyo Seon
    • Journal of the Korean Society of Clothing and Textiles
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    • v.16 no.3 s.43
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    • pp.335-344
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    • 1992
  • This study was conducted to investigate the influence of addition of cetyl trimethyl ammo­nium bromide (CTAB), and amine [ethylamine (EA) or ethylene diamine (EDA)] to aqueous sodium hydroxide (NaOH) solution on polyester alkaline hydrolysis, The experimental vari­ables such as CTAB concentration, EA or EDA concentration, NaOH concentration, tempera­ture and time were compared, and the changes in physical and chemical properties of alkaline­hydrolyzed PET fabrics depending on their treated conditions were measured, The results are as follows: 1. By adding CTAB and amine in aqueous NaOH solution, increasing effect on weight loss of PET fabrics was obtained in simultaneous addition of CTAB and EDA, but not in CTAB and EA. 2. By adding CTAB & EDA simultaneously, increasing effect on weight loss was obtained regardless of EDA concentration, time and temperature, and it was more effective at lower NaOH concentration. :l. The increase of void space (or irregularly grooved surface), of softness, of wickability, of dyeability on PET fabric, and the decrease of tensile strength, of molecular weight were observed according to the weight loss on the PET fabrics. These changes were equal to all alkaline-hydrolyzed PET fabrics regardless of addition of CTAB and amine. l. There was little changes on crystallinity, thermal behavior when PET fiber was treated with ,aqueous NaOH solution with CTAB and EDA. These results supported that increasing effect on weight loss take place without inducing of fine structural change of PET fibers.

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Study on the characteristics and biodegradable of synthetic PLGA membrane from lactic acid and glycolic acid (젖산 및 글리콜산에서 합성된 PLGA 멤브레인의 특성과 생분해성에 관한 연구)

  • Xie, Yuying;Park, Jong-Soon;Kang, Soon-Kook
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.16 no.4
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    • pp.2958-2965
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    • 2015
  • The PLGA(Poly lactide-co-glycolide) Copolymer have been actively applied to the medical implant material as biomaterials. PLGA membrane was able to alveoloplasty with osteotomy for favorable degradation characteristics and possibilities for sustained drug delivery. In this study, PLGA membrane was prepared using phase inversion method, and examined to optical method analysis(NMR, IR), mechanical property measurement (tearing strength) and thermal characteristic analysis(DSC). In addition, the biodegradation characteristics of the PLGA membrane filled with a PBS(Phosphate Buffered Solution) of the water bath ($60^{\circ}C$) according to the degree of surface degradation in the degradation time, the pH change of the solution and change of the mass of the membrane were measured.