• Title/Summary/Keyword: thermal effects

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Conditions for Rapid Processing of Modified Fish Sauce using Enzymatic Hydrolysis and Improvement of Product Quality 2. Fish Sauce from Sardine Waste and Its Quality (효소분해법에 의한 개량어장유의 속성제조 및 품질에 관한 연구 2. 정어리 폐기물을 이용한 어장유의 속성제조 및 품질)

  • BAE Tae-Jin;HAN Bong-Ho;CHO Hyun-Duk;KIM Jong-Chul;KIM Byeong-Sam;CHOI Soo-Il
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.23 no.2
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    • pp.125-136
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    • 1990
  • To develope a rapid processing method for fish sauce, processing conditions of fish sauce from sardine waste was investigated. The chopped waste was homogenized and hydrolyzed by commercial proteolytic enzymes such as Complex enzyme-2000($2.18\cdot10^4$ U/g solid) and Alcalase($1.94\cdot10^4$ U/g solid) in a cylindrical vessel with 4 baffles and 6-bladed turbine impeller. Optimal temperature for the case of hydrolysis with Complex enzyme-2000 was 50 and that with Alcalase was $55^{\circ}C$. In both cases, the reasonable pH, amount of water for homo-genization, enzyme concentration and hydrolyzing time were 8.0, $40\%$ (W/W), $3\%$ and 100 min, respectively. Heating of the filtrated hydrolysate for 2 hours at $90^{\circ}C$ with $6\%$ of invert sugar was suitable for pasteurization of the hydrolysate and inactivation of enzymes. Flavor, taste and color of the hydrolysate was improved during the thermal treatment in which the browning reaction products might participate and result in antioxidative and bactericidal effects. Combined use of $0.005\%$ of Caryophylli flos with invert sugar was also effective for the improvement of taste. Yield of the fish sauce based on the total nitrogen in the raw sardine waste was $91.2\~92.3\%$ and $87.2\~87.8\%$ of the total nitrogen in the fish sauce was in the form of amino nitrogen. The pH, salinity and histamine content of the fish sauce prepared with $15\%$ of table salt were $6.1\~6.2$, $14.2\~14.4\%$ and less than $10mg\%$, respectively. The fish sauce was stable during the storage of 60 days at $26\pm3^{\circ}C$ on bacterial growth and its quality was also maintained.

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Effects of direct and indirect bonding techniques on bond strength and microleakage after thermocycling (직접 부착법과 간접 부착법이 열순환 후 부착강도와 미세누출에 미치는 영향에 대한 연구)

  • Ozturk, Firat;Babacan, Hasan;Nalcaci, Ruhi;Kustarci, Alper
    • The korean journal of orthodontics
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    • v.39 no.6
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    • pp.393-401
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    • 2009
  • Objective: The purpose of this study was to compare the shear bond strength (SBS) of brackets and microleakage of a tooth-adhesive-bracket complex bonded with a direct and an indirect bonding technique after thermocycling. Methods: Fifty non-carious human premolars were divided into two equal groups. In the direct bonding group a light-cured adhesive and a primer (Transbond XT) was used. In the indirect-bonding group, a light-cured adhesive (Transbond XT) and chemical-cured primer (Sondhi Rapid Set) were used. After polymerization, the teeth were kept in distilled water for 24 hours and thereafter subjected to thermal cycling (500 cycles). For the microleakage evaluation, 10 teeth from each group were further sealed with nail varnish, stained with 0.5% basic fuchsin for 24 hours, and examined under a stereomicroscope. Fifteen teeth from each group were used for SBS testing with the universal testing machine and adhesive remnant index (ARI) evaluation. Data were analyzed using the Mann-Whitney U test, Chi-square test, and Fisher's exact test. Results: There were no statistical differences on SBS and microleakage between the two bonding techniques. The indirect bonding group had a significantly lower ARI score. Bracket failures were obtained between enamel-resin interfaces. Conclusions: The type of bonding technique did not significantly affect the amount of microleakage and SBS.

Improved Electrical Properties by In Situ Nitrogen Incorporation during Atomic Layer Deposition of HfO2 on Ge Substrate (Ge 기판 위에 HfO2 게이트 산화물의 원자층 증착 중 In Situ 질소 혼입에 의한 전기적 특성 변화)

  • Kim, Woo-Hee;Kim, Bum-Soo;Kim, Hyung-Jun
    • Journal of the Korean Vacuum Society
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    • v.19 no.1
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    • pp.14-21
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    • 2010
  • Ge is one of the attractive channel materials for the next generation high speed metal oxide semiconductor field effect transistors (MOSFETs) due to its higher carrier mobility than Si. But the absence of a chemically stable thermal oxide has been the main obstacle hindering the use of Ge channels in MOS devices. Especially, the fabrication of gate oxide on Ge with high quality interface is essential requirement. In this study, $HfO_xN_y$ thin films were prepared by plasma-enhanced atomic layer deposition on Ge substrate. The nitrogen was incorporated in situ during PE-ALD by using the mixture of nitrogen and oxygen plasma as a reactant. The effects of nitrogen to oxygen gas ratio were studied focusing on the improvements on the electrical and interface properties. When the nitrogen to oxygen gas flow ratio was 1, we obtained good quality with 10% EOT reduction. Additional analysis techniques including X-ray photoemission spectroscopy and high resolution transmission electron microscopy were used for chemical and microstructural analysis.

Control of YAG($Y_{3}Al_{5]O_{12}$) Particle Shape prepared by Sol-Gel Process (솔-젤 공정(工程)을 이용(利用)하여 제조(製造)된 YAG($Y_{3}Al_{5}O_{12}$) 분말 입형제어)

  • Park, Jin-Tae;Kim, Chul-Joo;Yoon, Ho-Sung;Sohn, Jung-Soo
    • Resources Recycling
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    • v.17 no.5
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    • pp.52-59
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    • 2008
  • Sol-gel process applied in this study was carried out by chelation of metal ions and citric acid. From the results of thermal gravimetric analysis and XRD analysis of gel powder obtained through sol-gel and heat treatment, gel powders are mostly amorphous, and crystallize completely at $900^{\circ}C$, and the crystalline structure of YAG increases with increasing calcinations temperature. Since YAG prepared by sol-gel & calcinations process was porous, and the sape and size was irregular and nonuniform, the shape and size of YAG powder had to be controlled. Therefore the effects of organic materials such as ethylene glycol and surfactant on the crystalline structure of YAG powder were investigated. Polyesterification of ethylene glycol and citric acid separated reaction area of metal ions in the solution and decreased the size of YAG primary particles. The addition of Igepal 630 as surfactant formed the droplet in the solution, and increased the size of primary particles which forms the aggregate of YAG In order to obtain monodispersed YAG particles of uniform size, gel powder prepared with organic materials had to be milled before calcination. And milling process was very important for obtaining YAG of uniform size.

A Study of Improving Fuel Droplet Movement with Sonic Wave Radiation (음파를 이용한 연료 입자 운동성 향상에 관한 연구)

  • Min, Sunki
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.20 no.12
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    • pp.608-613
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    • 2019
  • NOx (Nitrogen oxide) in the exhaust gas from vehicle engines is considered one of the most harmful substances in air pollution problems. NOx is made when combustion occurs under high temperature conditions and EGR (exhaust gas recirculation) is normally used to lower the combustion temperature. As the EGR ratio increases, the NOx level becomes low, but a high EGR ratio makes the combustion unstable and causes further air pollution problems, such as CO and unburned hydrocarbon level increase. This study showed that fuel droplets could move more freely by the radiation of sonic wave for the stable combustion. In addition, the engine performance improved with increasing EGR ratio. As a basic study, the effect of sonic wave radiation on the velocity of fuel droplets was studied using CFD software. The results showed that the velocity of small droplets increased more under high frequency sonic wave conditions and the velocity of the large droplets increased at low frequency sonic wave conditions. In addition, an engine analysis model was used to study the effects of the increased combustion stability. These results showed that a 15% increase in EGR ratio in combustion resulted in a 45% decrease in NOx and a 10% increase in thermal efficiency.

Experimental Application of Consolidants Using Artificially Weathered Stones(II): Focusing on Accelerated Weathering Test (인공풍화암을 이용한 강화제의 적용실험 연구(II): 촉진풍화실험을 통한 강화처리 암석의 내구성 평가)

  • Lee, Jae Man;Lee, Myeong Seong;Park, Sung Mi;Lee, Mi Hye;Kim, Jae Hwan
    • Journal of Conservation Science
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    • v.29 no.3
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    • pp.249-259
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    • 2013
  • This study was experimented on accelerated weathering test using salt and freeze-thaw to prove effects of consolidants and consolidation for stone cultural heritage. The samples used four kinds of stones (Gyeongju Namsan Granite, Iksan Granite, Yeongyang Sandstone and Jeongseon Marble) which to distributed by three type of weathering grade (Fresh, Weathered Stone and Highly Weathered Stone) added for thermal treatment. The samples were treated with three consolidants (Wacker OH 100, Remmers KSE 300 and 1T1G), and tested by 500 cycles with freezing-thawing and 50 cycles of salt weathering test. As a results of freezing-thawing test, the crack and destruction occurred from some samples. And total immersed samples maintained effect of consolidation to 200 cycles. Also, The rock particle was fall off and gradually destructed by salts weathering test. The consolidated sample relatively had fewer changes by the weathering than not treated sample. The sprayed sample had not continuous effect on weathering.

Effects of Fume silica on synthesis of New Austria Tunnel Method Resin for new material in space aviation (우주항공의 신소재를 위한 New Austria Tunnel Method 수지합성에 대한 Fume silica의 영향)

  • Kim, Kijun;Lee, Jooho;Park, Taesul;Lee, Joo-Youb
    • Journal of the Korean Applied Science and Technology
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    • v.31 no.4
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    • pp.595-601
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    • 2014
  • The microstructures of NATM were examined by SEM, FT-IR spectra, tensile properties, mole % of [NCO/OH], and particle size analyzer. Growing concerns in the environment-friendly industries have led to the development of solvent-free formulations that can be cured. We had synthesized NATM(New Austria Tunnel Method) resin having the ability to protect stainless steel against corrosion. Comparing with general NATM resin and coatings, this resin that synthesized with polyurethane and epoxy was highly stronger in intensity and longer durability. Hybrid resin was composed of polyols, MDI, epoxy, silicone surfactant, catalyst and crosslink agent, and fillers. Moreover, fillers such as fume silica not only accelerated the curing rate but also improved the physical property as thermal barriers. The rigid segments of synthetic resin in mechanical properties were due to fume silica and the increase the mole% of [NCO/OH] for corrosion protection. In conclusion, the hybrid resin microstructure with crosslink agent and fume silica are good material for thermosetting coating of metal substrates such as stainless steel.

A STUDY ON THE DISTORTION OF THE COPINGS FOR CERAMOMETAL CROWNS DURING REPEATED FIRING (도재전장금관을 위한 코핑의 변형에 관한 연구)

  • Lee, Ki-Hong;Chung, Hun-Young;Lee, Sun-Hyung;Yang, Jae-Ho
    • The Journal of Korean Academy of Prosthodontics
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    • v.35 no.4
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    • pp.706-718
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    • 1997
  • Ceramometal crowns are common restorations in fixed prosthodontics because of their casting accuracy, the high strength properties of the metal, and the cosmetic appearance of porcelain. However, deterioration of the initial fit of the metal coping has been observed after the porcelain firing cycle. The distortion due to repeated firing makes it difficult to fit crown margin and elicits microleakage. The major causes of distortion are the residual stress that accumulate during wax-up, casting, cold work and the induced stress caused by the mismatch of porcelain-metal thermal contraction. This study examined the marginal fit changes of metal copings in relation to repeated firing and the effects of heat treatment that reduce the distortion resulted from residual stress. The marginal changes of the copings that were treated with conventional method and those treated with heat before repeated firing, were evaluated. The metal die which represented preparations of a maxillary central incisor was fabricated, and 45 wax patterns were cast with nonprecious metal alloys. The heat treatment of each group was performed as follows. Group 1(control) : Casting - Devesting - Cold work - Firing Group 2 : Casting - Heat treatment - Devesting - Cold work - Firing Group 3 : Casting - Devesting - Cold work - Reinvesting - Heat treatment - Devesting - Firing The copings were fired 3 times. After each firing, the marginal fit changes were measured with inverted metallurgical microscope at the 4 reference points located at labial, lingual, and both proximal surface. Measurements were compared, and statistically analyzed. The results were as follows ; 1. In all groups, the highest value of marginal fit changes of the copings studied were found after the first firing cycle. 2. When the distortion of each experimental group at the first firing cycle were compared, group 1 exhibited the greatest changes($20-27{\mu}m$), followed by group 2($9-13{\mu}m$), and group 3($8-10{\mu}m$). 3. The copings treated with heat before devesting(group 2) revealed significantly smaller marginal fit changes than the copings treated with conventional method(group 1). (p<0.01) 4. The copings treated with heat after reinvesting(group 3) revealed significantly smaller marginal fit changes than the copings treated with conventional method(group 1). (p<0.01) 5. No siginificant differences in marginal fit changes were found between the copings treated with heat before devesting(group 2) and the copings treated with heat after reinvesting(group 3). (p>0.01)

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Analysis on Heating Effects of the Vertical Type Geothermal Heat Pump System

  • Kang, Youn Ku;Ryou, Young Sun;Jang, Jae Kyung;Kim, Young Hwa
    • Journal of Biosystems Engineering
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    • v.39 no.2
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    • pp.69-75
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    • 2014
  • Purpose: This paper is aimed at analyzing the heating performance of the vertical closed loop type Geothermal Heat Pump System (GHPS) distributing the farm site and providing basic data of the GHPS. Method: Seedling greenhouse heating was made from October 2012 to May 2013. The seedling greenhouse was divided into 4 sectors (A, B, C and D zone, total $3,300m^2$) with different temperatures. It was heated from 5PM to 8AM, and during the night the greenhouse was covered by non-woven fabric thermal curtains along the upper 2m of the greenhouse for temperature maintenance. In order to analyze the heating performance of the GHPS, power consumption and operating time of the GHPS, inlet and outlet water temperature of the condenser, temperatures of each zone of the greenhouse, and ambient temperature were measured. Results: When operating only one heat pump unit, heat generated in the condenser decreased as the experiment progressed and power consumption increased correspondingly. However, the heating coefficient of performance decreased from 3.3 to 2.0 rapidly. Also, when operating two heat pump units, heat generated in the condenser decreased and power consumption increased. Heating coefficient of performance decreased from 4.5 to 3.7 rapidly. When the set temperature of the greenhouse was $13.7{\sim}20.1^{\circ}C$ and minimum ambient temperature was $-20.8{\sim}4.8^{\circ}C$, the annually accumulated heat and power consumption were 520,623 kW, 142,304 kW, respectively. Conclusion: When the set temperature of the greenhouse was $13.7{\sim}20.1^{\circ}C$ and the minimum ambient temperature was $20.8{\sim}4.8^{\circ}C$, the annually accumulated heat and power consumption were 520,623 kW, 142,304 kW, respectively. When operating only one heat pump unit, the heating COP was 2.0~3.3, and when operating 2 heat pump units, it was 3.7~4.5. If several heat pumps are installed in one GHPS, it is suggested that all heat pumps be operated except in special cases. Because the scale of the water pumps are set to the scale of when all heat pump units are operating, if even one unit is not operating, the power consumption will increase. That becomes the cause of COP decrease.

Analytical Evaluation of Residual Stresses in Dissimilar Metal Weld for Cast Stainless Steel Pipe and Low-Alloy Steel Component Nozzle (스테인리스주강 배관과 저합금강 기기노즐 이종금속용접부 잔류응력의 해석적 평가)

  • Park, June-Soo;Song, Min-Seop;Kim, Jong-Soo;Kim, In-Yong;Yang, Jun-Seog
    • Proceedings of the KWS Conference
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    • 2009.11a
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    • pp.100-100
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    • 2009
  • This paper is concerned with numerical analyses of residual stresses in welds and material's susceptibility to stress corrosion cracking (SCC) for the primary piping system in nuclear power plants: Both the dissimilar metal weld (DMW) for stainless steel to low alloy steel joints and the similar metal weld (SMW) for forged stainless steel to cast stainless steel joints are considered. Thermal elasto-plastic analyses using the finite element method (FEM) are performed to predict residual stresses generated in fabrication welding and its related processes for both the DMW and SMW, including effects of quenching for cast stainless steel piping, machining of the DMW root, and grinding of the SMW root. As a result, the effect of quenching should be included in the evaluation of residual stresses in the SMW for the cast stainless steel piping. It is deemed that residual stresses in both the DMW and SMW would not affect the SCC susceptibility of the welds providing that the welding processes are completed without any weld repair on the inside wall of the joint. However, the grinding process if performed on the safe-end to piping weld, would produce a high level of residual stresses in the inner surface region and thus a stress improvement process (e.g. buffing) should be considered to reduce susceptibilities to SCC.

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