• Title/Summary/Keyword: test methods

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Quantitative Analysis of Heavy Metals in Packaging Papers

  • Jo, Byoung-Muk;Jeong, Myung-Joon
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.39 no.5
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    • pp.45-51
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    • 2007
  • This study was carried out to investigate various heavy metal contents in packaging papers by pre-treatments for ICP-ES (Inductively Coupled Plasma Emission Spectrometry) analysis. Pre-treatment methods of heavy metals in this study include extraction, migration and decomposition methods (dry ashing, $HNO_3-HClO_4-HF,\;HNO_3,\;and\;H_2SO_4-HNO_3$). Test results were compared with conventional extraction (water) and migration (3% acetic acid) methods. The five representative heavy metals (Cd, As, Pb, Cr and Hg) were analyzed. For Cd, Hg, and As, the results were below detection limit of the instrumental technique. It was considered that the migration test was a better method compared to extraction test, but all the decomposition methods showed much higher detection values than the extraction or migration test. In case of recycled corrugated containers, 3% acetic acid solution extracted about 25% of chromium and 30% of lead compared to the content by decomposition methods. Among all decomposition methods, the nitric acid - perchloric acid - hydrofluoric acid treatment brought a slightly higher detection value than others, but there was no significant difference among them except sulfuric acid - nitric acid method.

A Study on the Disturbance Effects with Sampling Methods of Soft Clay (연약 점성토의 시료채취방법에 따른 시료교란도의 영향에 관한 연구)

  • 박춘식;장정욱;김종환
    • Proceedings of the Korean Geotechical Society Conference
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    • 2002.10a
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    • pp.577-584
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    • 2002
  • We have employed two methods to remove slime at the end of the sampler in clay layers. The first method is a sampling process that harnesses low pressure to clean up the ground around the sampler tip. The second method, in consideration of a disturbed layer, involves a technique of inserting the sampler 50 cm deep into the ground before cleaning up the verge of the sampler by using high pressure. Physical and mechanical properties of these two methods have been compared and analyzed to investigate how different sampling methods affect degree of disturbance. The first method shows little disturbance since the unconfined compression test results in quite greater E$\_$50//q$\_$u/ in the first method than in the second method. On the other hand, the consolidation test results in a slightly greater compression index in the second method than in the first method, when their indexes are compared in the same depth. This suggests that the second method demonstrates less disturbance than the first method does. It is assumed that the second method may reduce disturbance slightly, However, we suspect that choosing any of the two methods would not obtain a considerable difference in sampling.

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Comparison of the Power of Bootstrap Two-Sample Test and Wilcoxon Rank Sum Test for Positively Skewed Population

  • Heo, Sunyeong
    • Journal of Integrative Natural Science
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    • v.15 no.1
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    • pp.9-18
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    • 2022
  • This research examines the power of bootstrap two-sample test, and compares it with the powers of two-sample t-test and Wilcoxon rank sum test, through simulation. For simulation work, a positively skewed and heavy tailed distribution was selected as a population distribution, the chi-square distributions with three degrees of freedom, χ23. For two independent samples, the fist sample was selected from χ23. The second sample was selected independently from the same χ23 as the first sample, and calculated d+ax for each sampled value x, a randomly selected value from χ23. The d in d+ax has from 0 to 5 by 0.5 interval, and the a has from 1.0 to 1.5 by 0.1 interval. The powers of three methods were evaluated for the sample sizes 10,20,30,40,50. The null hypothesis was the two population medians being equal for Bootstrap two-sample test and Wilcoxon rank sum test, and the two population means being equal for the two-sample t-test. The powers were obtained using r program language; wilcox.test() in r base package for Wilcoxon rank sum test, t.test() in r base package for the two-sample t-test, boot.two.bca() in r wBoot pacakge for the bootstrap two-sample test. Simulation results show that the power of Wilcoxon rank sum test is the best for all 330 (n,a,d) combinations and the power of two-sample t-test comes next, and the power of bootstrap two-sample comes last. As the results, it can be recommended to use the classic inference methods if there are widely accepted and used methods, in terms of time, costs, sometimes power.

Economic Design of Zero-Failure Reliability Qualification Test (경제적인 무고장 신뢰성 인증시험 설계)

  • Kwon, Young-Il
    • Journal of Korean Society for Quality Management
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    • v.39 no.1
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    • pp.71-77
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    • 2011
  • In the fields of reliability application, the most commonly used test methods for reliability qualification are zero failure tests since they require fewer test samples and less test time compared to other test methods that guarantee the same reliability with a given confidence level. An economic zero failure test plan is developed that minimizes the total cost related to perform a life test to guarantee a specified reliability of a product with a given confidence level and a numerical example is provided to illustrate the use of the proposed test method.

Determination of Opening Size of Geotextiles (토목섬유의 유효구멍크기 측정방법 및 측정결과 평가)

  • Cho, Sam-Deok;Kim, Ju-Hyong;Lee, Kwang-Wu
    • Proceedings of the Korean Geotechical Society Conference
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    • 2006.03a
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    • pp.111-120
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    • 2006
  • Opening size of 3 types of geotextile were tested using dry and wet sieving methods to evaluate characteristics of test methods and to compare the test results. Judging from test results, dry sieving method is a poor test, having many problems causing many errors but a simple-quick test. Wet sieving method is a very specific test avoiding many of the problems of dry sieving such as electrostatic charges, trapping in the geotextiles and so on. However, one of wet sieving tests, KSK ISO12956, takes long time to complete a test and is too strict to handle loss of granular material. Generally, opening size of a geotextile by wet sieving test is smaller than that of dry sieving test. Especially, opening size by KSF 2126 which is one of wet sieving test but disused at present anymore is similar or smaller than that by KSK ISO12956 method.

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Evaluation of Durability on MMA-Modified Polymer Paste for Coating materials (코팅재로서 MMA 개질 폴리머 페이스트의 내구성능 평가)

  • Yeon, Kyu-Seok;Lee, Hyun-Jong;Joo, Myung-Ki;Jin, Xing-Qi;Lee, Chi-Won
    • Proceedings of the Korea Concrete Institute Conference
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    • 2005.11a
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    • pp.807-810
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    • 2005
  • In this study, MMA-modified paste of coating material for protecting the concrete structures was developed. The coating material was applied to cement concrete specimens by brush, roller and spray in each of which one, two and three layers to survey, by the cold-hot iterative test, the neutralization test, the chloride ion permeation test and the ante-abrasion test, the affect of painting methods and layers influencing on the durability of coating material. Results of the cold-hot iterative test showed that, regardless of the painting methods and layers, the defects such as crack or fuzz on surface were not produced. As the number of painting layers increased, the neutralization prevention as well as the chloride ion permeation prevention effects were increased. On the other hand, no difference was found between the painting methods. Reducing weight by abrasion of polymer paste coating material was $20\%$ comparing to that of cement mortar.

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Study for Inspection Method of Electronic Components Using 3-D X-ray Imaging Technology (3차원 X-ray 영상 기법을 이용한 전자부품 검사 기술 연구)

  • Sim, Hyeok-Hun;Park, Gi-Nam;Kim, Jong-Hyeong;Park, Hui-Jae
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.16 no.5
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    • pp.157-161
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    • 2007
  • There are technological changes to reduce the size and weight of electronic components and to accommodate multi-functions in them. To meet this trend, more complicated technological processes are required. To maintain the processes, more accurate inspection systems are also necessary. Therefore, new inspection methods are needed, which is differ from conventional inspection methods such as electrical test methods ICT(In-Circuit Test), FCT(Function Test) and visual test using optical equipments. One of the possible approaches is non-destructive test using X-ray. In this paper, an inspection method using X-ray is developed and applied to inspection of soldering state and internal defects of electronic components.

Comparison and Evaluation of Load test Methods for Aluminum Car Body (알루미늄 차체 하중 시험 방법에 관한 비교 평가)

  • 서승일;박춘수;신병천
    • Proceedings of the KSR Conference
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    • 2003.10a
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    • pp.187-191
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    • 2003
  • Aluminum carbody for rolling stocks is light and perfectly recycled, but includes severe defects which are very dangerous to fatigue strength. Static load test has been performed up to date to assess structural safety of the carbody. However, static load test is not sufficient to evaluate fatigue strength of the carbody, because fatigue failure is caused by dynamic load. In this study, the established load test methods for carbody are described and the characteristics of the methods are discussed. Also, a testing method to simulate dynamic loading condition is proposed for evaluation of fatigue strength of the carbody The results by the proposed testing method are compared with the results by the static load test and new findings are discussed.

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Finite Element Analysis of BLDC Motor Characteristic according to Magnetic Property Measurement Methods (자성 측정 방법에 따른 BLDC 전동기의 전자계 특성해석)

  • Kim, Ji-Hyun;Ha, Kyung-Ho;Kwon, Oh-Yeoul;Cha, Sang-Yoon;Kim, Jae-Kwan
    • Proceedings of the KIEE Conference
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    • 2008.07a
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    • pp.697-698
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    • 2008
  • This paper deals with finite element characteristic analysis of brushless DC motor according to magnetic property measurement methods. Magnetic property data for non-oriented (NO) electrical steel for electric motors are measured by the Epstein test which is considered as the international standards. Data from Epstein test may result in discrepancy from motor characteristic tests due to innate anisotropic property of NO electrical steel. Finite element analysis were performed for a BLDC motor by various measurement methods such as Epstein test, Ring test and single sheet test (SST), and calculated results were compared with considering anisotropic property conditions.

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Stress mode proposal for an efficient ESD test (효율적인 ESD(ElectroStatic Discharge) test를 위한 Stress mode 제안)

  • Gang, Ji-Ung;Chang, Seog-Weon;Kwack, Kae-Dal
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.1289-1294
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    • 2008
  • Electrostatic discharge(ESD) phenomenon is a serious reliability concern. It causes approximately most of all field failures of IC. To quality the ESD immunity of IC product, there are some test methods and standards developed. ESD events have been classified into 3 models, which are HBM, MM and CDM. All the test methods are designed to evaluate the ESD immunity of IC products. This study provides an overview among ESD test methods on ICs and an efficient ESD stress method. We have estimated on all pin combination about the positive and negative ESD stress. We make out the weakest stress mode. This mode called a worst-case mode. We proposed that positive supply voltage pin and I/O pin combination is efficient because it is a worst-case mode.

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