• Title/Summary/Keyword: synthesis variation

Search Result 253, Processing Time 0.028 seconds

pH Dependent Size and Size Distribution of Gold Nanoparticles

  • Kang, Aeyeon;Park, Dae Keun;Hyun, Sang Hwa;Yun, Wan Soo
    • Proceedings of the Korean Vacuum Society Conference
    • /
    • 2013.08a
    • /
    • pp.267.2-267.2
    • /
    • 2013
  • In the citrate reduction method of gold nanoparticle (AuNP) synthesis, pH of the reaction mixture can have a considerable impact on the size and size distribution of AuNPs. In this work, effects of pH variation upon the size and its distribution were examined systematically. As the initial pH was change from 5.5 to 10.5, it showed an optimal pH around 7.5. At this pH, both of the size and the size distribution showed their minimum values, which was verified by transmission electron microscopy and UV-vis spectroscopy. This occurrence of optimal pH was discussed with the results of in situ monitoring pH during the reaction of AuNP synthesis.

  • PDF

Autoradiographic Observations on Variation of DNA Synthesis in the Developing Extraembryonic Membranes of the Golden Hamster (Golden Hamster 태반형성(胎盤形成)에 있어서 Autoradiography에 의한 분열세포(分裂細胞)의 소장(消長))

  • Lee, Cha-Soo
    • Korean Journal of Veterinary Research
    • /
    • v.23 no.1
    • /
    • pp.1-8
    • /
    • 1983
  • The purpose of the present study is to determine variations in synthesis of DNA in the nuclei of various elements of the golden hamster (Mesocricetus auratus) placenta with increasing gestational age from the eighth day post coitus to parturition. The method employed for such determination was autoradiography following injection of pregnant animals with tritiated thymidine. From the results reported, the following points are concluded. The mitotic activities of the endodermal cells of the visceral yolk sac and of the parietal yolk sac, the trophoblastic cells of the labyrinth and the trophospongium and the giant cells were decreased with increasing gestational age, The placentation was nearly completed by day 13 of pregnancy and the increase in size of labyrinth was by appositional growth from the trophospongial cells. It was considered that the inner trophoblastic cells in the vicinity of the fetal blood vessels were originated from the pure chorion. The interrelation among the various cells and the polyploidal giant cells in the placenta were discussed.

  • PDF

Noise-Robust Speech Detection Using The Coefficient of Variation of Spectrum (스펙트럼의 변동계수를 이용한 잡음에 강인한 음성 구간 검출)

  • Kim Youngmin;Hahn Minsoo
    • MALSORI
    • /
    • no.48
    • /
    • pp.107-116
    • /
    • 2003
  • This paper deals with a new parameter for voice detection which is used for many areas of speech engineering such as speech synthesis, speech recognition and speech coding. CV (Coefficient of Variation) of speech spectrum as well as other feature parameters is used for the detection of speech. CV is calculated only in the specific range of speech spectrum. Average magnitude and spectral magnitude are also employed to improve the performance of detector. From the experimental results the proposed voice detector outperformed the conventional energy-based detector in the sense of error measurements.

  • PDF

Effects of spatial variability of earthquake ground motion in cable-stayed bridges

  • Ferreira, Miguel P.;Negrao, Joao H.
    • Structural Engineering and Mechanics
    • /
    • v.23 no.3
    • /
    • pp.233-247
    • /
    • 2006
  • Most codes of practice state that for large in-plane structures it is necessary to account for the spatial variability of earthquake ground motion. There are essentially three effects that contribute for this variation: (i) wave passage effect, due to finite propagation velocity; (ii) incoherence effect, due to differences in superposition of waves; and (iii) the local site amplification due to spatial variation in geological conditions. This paper discusses the procedures to be undertaken in the time domain analysis of a cable-stayed bridge under spatial variability of earthquake ground motion. The artificial synthesis of correlated displacements series that simulate the earthquake load is discussed first. Next, it is described the 3D model of the International Guadiana Bridge used for running tests with seismic analysis. A comparison of the effects produced by seismic waves with different apparent propagation velocities and different geological conditions is undertaken. The results in this study show that the differences between the analysis with and without spatial variability of earthquake ground motion can be important for some displacements and internal forces, especially those influenced by symmetric modes.

Research on Synthesis of Radiation Noise from Moving Target (이동하는 표적의 방사소음 합성기법 연구)

  • 배재휘
    • Journal of the Korea Institute of Military Science and Technology
    • /
    • v.3 no.1
    • /
    • pp.58-65
    • /
    • 2000
  • A target signal simulation method for passive sonar systems is introduced. The method uses multirate signal processing techniques to simulate moving target signals in the multi-path sound propagation environment by introducing Lloyd's mirror and Doppler effect. Time and frequency variation of target signal due to the target maneuvering is also considered to provide realistic ship signatures in the LOFAR gram so that the simulated target is used for sonar operator training. Synthesized target characteristics is analyzed and compared with real target signal in terms of interference pattern and frequency variation in the LOFAR gram.

  • PDF

Sucrose Synthase, UDP-glucose pyrophosphorylase and ADP-glucose Pyrophosphorylnse in Korea Ginseng Roots

  • Yelena V.Sundukova;Lee, Mi-Ja;Park, Hoon
    • Journal of Ginseng Research
    • /
    • v.24 no.2
    • /
    • pp.83-88
    • /
    • 2000
  • The seasonal variation in the activity of sucrose synthase, ADP-glucose pyrophosphorylase and UDP-glucose pyrophosphorylase in roots of Panax ginseng C.A.Meyer have been studied. It was revealed that sucrose synthase and ADP-glucose pyrophosphorylase are adaptive enzymes and can serve as markers of sink strength, while UDP-glucose pyrophosphorylase is the maintenance enzyme. The average day temperature exceeded 24。C appeared to cause the disturbance in refilling process, affecting the starch synthesis. Study on the dependence of oxygen consumption in stele tissue with temperature revealed the sharp accelerating of this process after 24。C.

  • PDF

A STUDY ON THE ROBOTST MODRL-FOLLOWING CONTROL SYSTEMS WITH ONLINEAR PLANT

  • Kwon, Sung-Ha;Shimemura, Etsujiro;Shin, Jae-Woong
    • 제어로봇시스템학회:학술대회논문집
    • /
    • 1991.10b
    • /
    • pp.1934-1938
    • /
    • 1991
  • This paper proposes a robust model following control systems with nonlinear time varying plant. which realies good properties such as asymptotic stability, disturbance rejection and model-following with reduced sensitivity for plant parameter variation. The schemes do not incorporate any parameter identification algorithms, but the adaptation is realized through signal synthesis in a fixed parameter structure.

  • PDF

An Adaptive Photon Mapping in the Use of Automatic Differentiation

  • Namae, Takuya;Makino, Mitsunori
    • Proceedings of the IEEK Conference
    • /
    • 2002.07b
    • /
    • pp.991-994
    • /
    • 2002
  • Photon mapping is an efficient global illumination technique for realistic image synthesis that has been developed in computer graphics. In this paper, an adaptive photon mapping in the use of automatic differentiation is proposed. Since the automatic differentiation is used when photons emit from the light sources through the scene, we can check the variation of surrounding shape. Therefore, we can decrease the number of photons and generate an image in relatively low computational cost.

  • PDF

Synthesis and Properties of Liquid Crystalline Y-shaped Molecules Containing 1,3,4-Oxadiazole

  • Kwon, Eun-Kyoung;Choi, E-Joon
    • 한국정보디스플레이학회:학술대회논문집
    • /
    • 2007.08a
    • /
    • pp.542-544
    • /
    • 2007
  • New liquid crystalline Y-shaped molecules containing 1,3,4-oxadizoles have been synthesized with variation of terminal groups (R = H, $OCH_3$ or $OC_8H_{17}$). The structures of obtained compounds were identified by FT/IR and NMR spectrometry, and their thermal and liquid crystalline properties were investigated by DSC and polarizing optical microscope.

  • PDF

A Study on the Electrical characteristics of LiTCNQ (LiTCNQ 착체의 전기적 특성에 관한 연구)

  • Kim, Yong-Tae;Kang, Hun;Jeong, Soon-Wook;Sohn, Byoung-Chung;Kang, Dol-Yol
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 1988.10a
    • /
    • pp.18-20
    • /
    • 1988
  • The electrical characteristics of LiTCNQ, the most important intermediate in a synthesis of an organic charge transfer complex, was measured. Activation energy of LiTCNQ was estimated from the conductivity variation on the temperature increase.

  • PDF