• Title/Summary/Keyword: surfaces characteristics

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Biocompatibility study of lithium disilicate and zirconium oxide ceramics for esthetic dental abutments

  • Brunot-Gohin, Celine;Duval, Jean-Luc;Verbeke, Sandra;Belanger, Kayla;Pezron, Isabelle;Kugel, Gerard;Laurent-Maquin, Dominique;Gangloff, Sophie;Egles, Christophe
    • Journal of Periodontal and Implant Science
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    • v.46 no.6
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    • pp.362-371
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    • 2016
  • Purpose: The increasing demand for esthetically pleasing results has contributed to the use of ceramics for dental implant abutments. The aim of this study was to compare the biological response of epithelial tissue cultivated on lithium disilicate ($LS_2$) and zirconium oxide ($ZrO_2$) ceramics. Understanding the relevant physicochemical and mechanical properties of these ceramics will help identify the optimal material for facilitating gingival wound closure. Methods: Both biomaterials were prepared with 2 different surface treatments: raw and polished. Their physicochemical characteristics were analyzed by contact angle measurements, scanning white-light interferometry, and scanning electron microscopy. An organotypic culture was then performed using a chicken epithelium model to simulate peri-implant soft tissue. We measured the contact angle, hydrophobicity, and roughness of the materials as well as the tissue behavior at their surfaces (cell migration and cell adhesion). Results: The best cell migration was observed on $ZrO_2$ ceramic. Cell adhesion was also drastically lower on the polished $ZrO_2$ ceramic than on both the raw and polished $LS_2$. Evaluating various surface topographies of $LS_2$ showed that increasing surface roughness improved cell adhesion, leading to an increase of up to 13%. Conclusions: Our results demonstrate that a biomaterial, here $LS_2$, can be modified using simple surface changes in order to finely modulate soft tissue adhesion. Strong adhesion at the abutment associated with weak migration assists in gingival wound healing. On the same material, polishing can reduce cell adhesion without drastically modifying cell migration. A comparison of $LS_2$ and $ZrO_2$ ceramic showed that $LS_2$ was more conducive to creating varying tissue reactions. Our results can help dental surgeons to choose, especially for esthetic implant abutments, the most appropriate biomaterial as well as the most appropriate surface treatment to use in accordance with specific clinical dental applications.

Physico-chemical Characteristics of Submicron Aerosol at West Inflow Regions in the Korean Peninsula III. Physical-Chemical Behavior and Long-range Transport of PM1 (한반도 서부유입권역에서 대기 중 에어로졸 성분의 물리·화학적 특성 연구 III. 화학적 거동 및 장거리 이동)

  • Park, Taehyun;Ahn, Junyoung;Choi, Jinsoo;Lim, Yongjae;Park, Jinsoo;Kim, Jeongho;Oh, Jun;Lee, Yonghwan;Hong, Youdeog;Hong, Jihyung;Choi, Yongjoo;Lee, Taehyoung
    • Journal of Korean Society for Atmospheric Environment
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    • v.33 no.2
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    • pp.124-138
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    • 2017
  • Physico-chemical measurement of non-refractory submicron particles($NR-PM_1$) was conducted in Baengnyeong Island, Korea using Aerodyne High Resolution Time of Flight Aerosol Mass Spectrometer (HR-ToF-AMS) from 2012 to 2014. Organics and ammoniated sulfate were dominant species in $NR-PM_1$. The organics was found to have similar fractions(approximate 40%) of $NR-PM_1$ during the summer and winter, while the sulfate fractions of $NR-PM_1$ were calculated to be approximately 47% and 31% for the summer and winter, respectively, suggesting the possibility that particles provide non-acidic surfaces for condensation of nitric acid in the winter. The nitrate fractions of approximate 4% and 20% of $NR-PM_1$ were observed in August (summer) and November (winter), respectively, resulting that the relatively low concentration of sulfate in $NR-PM_1$ provided a non-acidic surface for nitric acid condensation and formation of particulate ammoniated nitrate is favored thermodynamically in winter. The new particle formation (NPF) event and particle growth rate were analyzed for each month in 2014 using Scanning Mobility Particle Sizer(SMPS). The Percent of NPF events was the highest in winter, but NPF event was not observed during summer due to relatively high temperature and frequent rainfall. The average particle growth rate was 3.5 nm/h and the highest particle growth rate was 5.5 nm/h in May. We observed the long-range transport of the anthropogenic sulfate from the East Asia during the intensive monitoring period of November between Qingdao and Baengnyeong Island in 2013. The relatively high concentrations of m/z 60 measured in HR-ToF-AMS was observed in May and June at Baengnyeong Island, suggesting the possibility of the influence of biomass burning from the East Asia to the Korean Peninsula.

Analysis of Optimum Design of Stepped Bar Horn for 20kHz Metal Ultrasonic Welding (20kHz 급 금속 초음파 융착용 스텝형 바 혼의 최적설계)

  • Kim, Jisun;Kim, Jaewoong;Kim, In-ju;Seo, Joowhan
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.20 no.12
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    • pp.94-101
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    • 2019
  • In this study, the FEM technique was applied to design the shape of the horn that transmits ultrasonic vibration energy to the base material, and the shape of the welding horn with a one-wavelength bar shape used in the 20kHz region was designed. The shape design of the horn was performed by applying the rod longitudinal vibration theory to Ansys APDL (Ansys Parametric Design Language). Twenty-five models were designed using the ratio of the area of the input and output surfaces of the vibration and the length of the horn to derive the appropriate horn shape. The horn was designed with a total length of 130mm, a step length of 65mm, and an output area of 28.79mm. The horn was fabricated using the optimized dimensions, and the vibration and displacement characteristics of the horn were evaluated using the measurement system. Finally, a uniform longitudinal step horn was designed, and more than 97.4% of the uniformity of the tip was secured. The amplitude ratio of the optimized horn was improved by 51%.

A Study on the Reduced Rebound Method of Surface Finishing Spray Photocatalytic Mortar (표면 마감 광촉매 스프레이 모르타르의 리바운드량 저감 방안 연구)

  • Baek, Hyo-Seon;Park, Jeong-Hwan
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.9
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    • pp.604-609
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    • 2020
  • There are various methods of finishing concrete surfaces, and when considering workability, the spray method is effective, but rebound occurs. The allocation of rebound occurrence control should be adjusted according to the materials used. Thus, a basic study was conducted on multiple techniques for reducing the rebound incidence that are suitable for surface finishing materials containing a photocatalyst. A prior study derived the reduction effect and optimal mix ratio for photocatalytic performance. Based on that study, the rebound reduction was verified according to the specifications of the content and the mechanical durability characteristics of the mixed materials. Rebound, compressive strength, flexural rigidity, and table flow tests were done. The flow was fixed at 170±10 mm considering the workability of the mortar spray equipment. For the experimental variables, the rebound number was adjusted to the silica sand variables relative to the cement weight, and silica sands No. 5 and No. 7 were used. The results show the highest compression strength in the final S-1 variable, and the amount of rebound was minimized. These results were sufficiently filled with the bindings of the silica pores, which increased the binding force between the aggregates, resulting in a lower amount of rebound.

Effects of Differential Heating by Land-Use types on flow and air temperature in an urban area (토지 피복별 차등 가열이 도시 지역의 흐름과 기온에 미치는 영향)

  • Park, Soo-Jin;Choi, So-Hee;Kang, Jung-Eun;Kim, Dong-Ju;Moon, Da-Som;Choi, Wonsik;Kim, Jae-Jin;Lee, Young-Gon
    • Korean Journal of Remote Sensing
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    • v.32 no.6
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    • pp.603-616
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    • 2016
  • In this study, the effects of differential heating by land-use types on flow and air temperature at an Seoul Automated Synoptic Observing Systems (ASOS) located at Songwol-dong, Jongno-gu, Seoul was analyzed. For this, a computation fluid dynamics (CFD) model was coupled to the local data assimilation and prediction system (LDAPS) for reflecting the local meteorological characteristics at the boundaries of the CFD model domain. Time variation of temperatures on solid surfaces was calculated using observation data at El-Oued, Algeria of which latitude is similar to that of the target area. Considering land-use type and shadow, surface temperatures were prescribed in the LDAPS-CFD coupled model. The LDAPS overestimated wind speeds and underestimated air temperature compared to the observations. However, a coupled LDAPS-CFD model relatively well reproduced the observed wind speeds and air temperature, considering complicated flows and surface temperatures in the urban area. In the morning when the easterly was dominant around the target area, both the LDAPS and coupled LDAPS-CFD model underestimated the observed temperatures at the Seoul ASOS. This is because the Kyunghee Palace located at the upwind region was composed of green area and its surface temperature was relatively low. However, in the afternoon when the southeasterly was dominant, the LDAPS still underestimated, on the while, the coupled LDAPS-CFD model well reproduced the observed temperatures at the Seoul ASOS by considering the building-surface heating.

Reflection Signal Analysis for Time Division Multiplexing of Fiber Optic FBG Sensors (광섬유 FBG 센서의 시간 분할 다중화를 위한 반사 신호의 분석)

  • Kim, Geun-Jin;Kwon, Il-Bum;Yoon, Dong-Jin;Hwang, Du-Sun;Chung, Young-Joo
    • Journal of the Korean Society for Nondestructive Testing
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    • v.30 no.1
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    • pp.6-12
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    • 2010
  • Fiber optic sensor using fiber Bragg grating(FBG) probes is used for monitoring strain and temperature distributed on the wide surfaces of large structures. In this paper, in order to use many FBG probes in one optical fiber line, we propose a complex multiplexing technology which is composed of two techniques, one is time division multiplexing and another is wavelength division multiplexing. However, we only investigate the characteristics of time division multiplexing because FBG sensors basically can be operated by wavelength division multiplexing. We calculate the optimal reflectivities and the lengthwise location of five FBG probes in serial connection in order to obtain the unique reflected intensities from the FBG probes. We fabricate five FBG probes with the reflectivities of 13%, 16%, 25%, 40% and 80%, which are determined by the theoretical calculation, and observe the signal reflected from each FBG in the time domain from the experiment. There are differences between experimental and theoretical results caused by the signal noise and the differences of reflectivities of FBG probes. But the experimental results shows the reflected signals of five FBG probes which prove the availability of complex multiplexing.

Surface Characterization of Rocks after Treated with Developed Consolidants (개발 강화제 처리 전후의 암석 표면에 나타나는 특성 변화 연구)

  • Kim, Jeong-Jin;Jang, Yun-Deuk;Won, Jong-Ok;Kang, Young-Soo
    • Journal of the Mineralogical Society of Korea
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    • v.25 no.2
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    • pp.105-115
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    • 2012
  • The consolidants have been widely used for the consolidation of decaying heritage stone surfaces. In this study, X-ray diffraction analysis, polarized and stereo-microscope and scanning electron microscope were used to study the surface characterization of granite, sandstone and marble, and to assess the efficiency and the effects of the developed condolidants in the field. The developed consolidants used in this experiment are 100%1T1G and 3%40nm/97%1T1G. The effects of consolidants are 3%40nm/97%1T1G${\gg}$100%1T1G in granite, 3%40nm/97%1T1G>100%1T1G in sandstone, and 3%40nm/97% 1T1G=100%1T1G in marble. The characteristics of rock surface when treated with consolidants show different result according to consolidantes type. This result of treating with consolidant can be used for the conservation of an decaying heritage stone.

The Effect of Surfactants in $\textrm{NH}_4\textrm{OH}$ on Silicon Surfaces and Particle Removal (계면 활성제 첨가한 암모니아수의 소수성 실리콘 웨이퍼와의 반응 세정 효과)

  • Park, Jin-U;Park, Jin-Gu;Kim, Gi-Seop;Song, Hyeong-Su
    • Korean Journal of Materials Research
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    • v.9 no.9
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    • pp.872-877
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    • 1999
  • The purpose of this research was to investigate the characteristics and the cleaning efficiency on HN(sub)4OH solutions added with H(sub)2O(sub)2 and surfactants. NH(sub)4OH solutions added with surfactants did not show much changes in pH and redox potential (Eh) as a function of NH(sub)4OH concentration compared with NH(sub)4OH solution. However H(sub)2O(sub)2 added NH\ulcornerOH solutions showed the decrease of pH and the increase of Eh as the concentration of NH(sub)4OH increased. The decrease of surface tension from 72 dynes/cm to 38 dynes/cm was observed in solutions added with surfactant but not in H(sub)2O(sub)2. The etch rates of silicon in NH(sub)4OH solutions(NH(sub)4OH:H(sub)2O= 1 : 5) showed at least 50 times higher than those in H(sub)2O(sub)2 and surfactant added NH(sub)4OH solutions(NH(sub)4OH:H(sub)2O(sub)2= 1 : 1 : 5) solution removed the PSL particles (0.67$\mu\textrm{m}$ in diameter) on Si wafers effectively at all temperatures investigated. NH(sub)4OH solution added with a surfactant could not remove particles at room temperature, however it was possible to remove particles at higher temperatures, 5$0^{\circ}C$ and 8$0^{\circ}C$.

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Identification and FT-IR Spectrum Analysis of Lichens on Flagpole Support in Beopjusa Temple (법주사 당간지주 지의류의 동정 및 FT-IR 스펙트럼 특성 분석)

  • Kim, Young Hee;Lee, Jeung Min;Choie, Myoungju;Hong, Jin Young;Jo, Chang Wook;Kim, Soo Ji;Jeong, So Young
    • Journal of Conservation Science
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    • v.33 no.5
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    • pp.391-398
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    • 2017
  • This study was conducted to investigate lichen as a typical biomass damage on the surfaces of flagpole-supporting stones in the Beopjusa temple. The lichens present on the flagpole-supporting stones were limited to five species. Two dominant lichen species were identified: Aspicilia sp. and Pertusaria flavicans. One foliose species and one fruticose species, which are rarely observed on crustose lichens, were identified as Xanthoparmelia conspersa and Ramalina sekika, respectively. The lichen inhabiting the black algae layer was confirmed as Leprocaulon textum. ATR-FTIR was performed to analyze the secondary metabolites synthesized by the lichens. By comparing the FTIR spectra of Xanthoparmelia conspersa and Ramalina sekika, the synthesized organic acids were confirmed to differ from each other. Furthermore, the spectral changes and characteristics due to functional groups in the molecules were confirmed.

A Study on the Ultrastructure of Reproductive Organ of Korean Planaria (Dugesia japonica) (한국산(韓國産) 플라나리아(Dugesia japonica Ichikawa et Kawakatsu)생식기관(生殖器官)의 미세구조(微細構造)에 관(關)한 연구(硏究))

  • Chang, N.S.;Kim, W.K.
    • Applied Microscopy
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    • v.15 no.1
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    • pp.31-58
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    • 1985
  • The morphological study on different types of cells of reproductive organ including spermatogenesis in the adult planaria was performed to observe their cytochemical and ultrastructural characteristics. 1. Spermatogenesis The circular luminated material appears immediately inside the nuclear envelope of early spermatid and is found also in the nucleus of sperm, but typical acrosomal structures cannot be observed. Approximately ten of small-sized mitochondria occur around the nucleus in the transitional phase from primary spermatocyte to secondary spermatocyte, but in sperm a long mitochondrion is closely associated with nucleus, parellel to long axis of it. The sperm has a relatively long head connected with two tails via hollow neck. 2. Reproductive organ The penis bulb and the bursa stalk were observed. (1) Penis bulb The cells constituted penis bulb are classified into six types on the basis of ultrastructure of the cells and cytochemistry of the cytoplasmic granules. 1) A-type cells: These cells exhibiting low electron density are mainly occupied by large nucleus. These cells possess two different types of granules: highly electron-dense round granules with an average size of $0.9{\mu}m$, and electron-dense granules exhibit PAS-positive reaction. 2) B-type cells contain PAS-positive granules with the size of about $0.4{\mu}m$. They are rich in free ribosomes and mitochondria. 3) C-type cells are found to be dark cells due to high electron-density. These cells are largely occupied by large nucleus. 4) D-type cells: These cells are seen as light cells which have poorly developed cell organelles. 5) E-type tells: These cells contain a large number of glycogen granules which occupy most of cell. 6) F-type cells: These arc parietal epidermal cells surrounding the genital antrum. These cells are characterized by their finger-like shapes and the presence of a number of electron-dense, irregularly-shaped structures inside cells. The relatively large electron-lucent granules can be also found. The F-type cells possess numerous microvilli on their free surfaces. (2) Bursa stalk The cells constituted bursa stalk are classified into 3 types on the basis of cell shapes and presences of electron-dense or electron-lucent granules. 7) G-type cells with a long cytoplasmic process. They have large nuclei and poorly developed cell organelles. 8) H-type cells: These cells are characterized by the presence of a long cytoplasmic process and relatively highly electron-dense cytoplasmic profile. They have poorly developed cell organelles. 9) I-type cells contain large electron-lucent granules which exhibit negative reactions with three kinds of cytochemical staining methods used in this experiment. The fine electron-dense structures can be found inside these granules.

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