• 한국전기전자재료학회논문지
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• 제23권1호
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• pp.10-13
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• 2010

The plasma processing technologies of thin film deposition and surface treatment technique have been applied to many industrial fields. This study is purposed Large-area uniformity and surface treatment on the stainless substrate. We treat surface of stainless by $CF_4$ plasma. $CF_4$ plasma is generated by using SPM(Scanning plasma method)which is kind a of CVD. Generally, SPM has been used for uniform surface treatment using a crossed electromagnetic field. The optimum discharge condition has been studied for the gas pressure, the magnetic flux density and the distance between substrate and electrodes. In result, contact angle is increased by surface treatment using $CF_4$ Plasma. Therefore we expect that SPM to control contact angle is applied to many industries.

• Journal of Advanced Marine Engineering and Technology
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• 제35권5호
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• pp.600-607
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• 2011

고탄소강은 사용자가 요구하는 특성을 만족시키기 위해 침탄, 질화, 고주파담금질 등에 의해 표면처리 되어져 왔다. 그러나 기존의 처리 방법은 모두 처리물 전체를 가열하거나 균일한 가열을 하지 못하여 표면처리 후 변형의 문제와 처리후의 후가공의 경비문제, 그리고 극히 일부분만 경화가 필요한 부품에는 적용하기 어려운 문제점이 있었다. 이러한 문제를 해결할 수 있는 표면처리법으로로써 레이저열처리 방법이 대두대고 있으며, 레이저열처리는 레이저 빔을 피처리물의 표면에 조사하고 적당한 속도로 이동을 하게 되면 레이저조사부위가 급속하게 가열되고 레이저 빔이 통과한 후에는 표면의 열이 내부로 열전도 되어 급속히 자기냉각(self-quenching)됨으로써 표면에 새로운 기계적 성질을 갖게 하는 열처리법이다. 본 연구에서는 기존의 CW Nd:YAG 레이저 열원보다 효율이 좋은 HPDL을 이용한 고효율, 고기능의 고탄소강 열처리 후 재료적 물성을 평가하였다. 그 결과 레이저빔의 조사속도 및 온도변화에 따른 열처리부 및 모재 부분에 대한 경도특성 및 미세조직의 특성을 명확히 할 수 있었다.

• 한국전기전자재료학회논문지
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• 제14권10호
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• pp.821-827
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• 2001

In this study performed to identify a degradation mechanism in macromolecular insulating material, the contact angel, surface potential decay, surface resistivity, and XPS analysis were compared after exposure of FRP laminate to plasma discharge. In the case of contact angle, the surface of specimen untreated showed weak hydrophobic property of 73。. However, the contact angle was decreased to 20。in the plasma-treated specimen. In the case of chemical changes arising form plasma treatment, carboxl radicals were generated mainly in the surface treated, which was rapidly changed to the hydrophilic one. In the corona potential decay study to determine the electrical changes of the surface, positive charges were rapidly decreased when compared with negative charges, leading to negative property in the surface of specimen not treated. However, in the case of the hydrophilic surface, lots of carboxl radicals acting as positive polarity were generated, resulting in positive surface. Owing to such positive surface, charges of negative polarity applied were rapidly decreased.

• 한국전기전자재료학회논문지
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• 제18권5호
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• pp.450-456
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• 2005

In this paper, the effect of adhesion properties of semiconductive-insulating interface layer of silicone rubber on electrical properties was investigated. The modifications produced on the silicone surface by oxygen plasma were accessed using ATR-FTIR, contact angle and Surface Roughness Tester. Adhesion was obtained from T-peel tests of semiconductive layer haying different treatment durations. In addition, ac breakdown test was carried out for elucidating the change of electrical property with duration of plasma treatment. From the results, the treatment in the oxygen plasma produced a noticeable increase in surface energy, which can be mainly ascribed to the creation of O-H and C=O. It is observed that adhesion performance was determined by surface energy and roughness level of silicone surface. It is found that at dielectric strength was increased with improving the adhesion between the semiconductive and insulating interface.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1994년도 춘계학술대회 논문집
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• pp.141-143
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• 1994

One of the Principal problems encountered in the use of filer reinforced composites is to establish an active fiber surface to achieve maximum adhesion between resin and fiber surface. Now, we want to develope new process that will overcome the disadvantage of the chemical coupling agent and achieve maximum adhesion at the interface between resin and fiber by active plasma treatment on the glass fiber surface. In this study. we investigated the effect of plasma treatment on the wettability of glans surface .

• 한국건축시공학회지
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• 제13권5호
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• pp.457-464
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• 2013

Traditionally, the material used for the form in reinforced concrete construction has been wood or steel. But recently, aluminum forms have been widely used in wall structures such as apartment buildings. Aluminum is light, easy to handle, and economically advantageous, but the hydrogen gas created due to its reaction with the alkali component in concrete gives rise to air pockets on the concrete's surface, and deteriorates the surface's finishability. In this research, to determine the influence of aluminum material on concrete, the cement paste W/C and its chemical reactivity in alkali and acid solution were analyzed. As a prevention plan, the influence of the number of applications of calcium hydroxide and various surface coating materials was analyzed. Through the analysis, it was found that the surface voids on the aluminum form are the result of the reaction of hydrogen gas with an alkali such as $Ca(OH)_2$. This can be prevented by the surface treatment of $Ca(OH)_2$, separating material and coating material. However, poor surface form and damages to the form are expected to cause quality degradation because of the aluminum-concrete interaction. Therefore, thorough surface treatment, rather than the type of separating material or coating material, is considered the most important target of management.

• 한국전기전자재료학회논문지
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• 제23권1호
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• pp.65-69
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• 2010

In this study, we compared two methods(an acid treatment in strong acid reflux and a heat treatment in air atmosphere) for hydrophilic surface treatment of multi-walled carbon nanotubes(MWNT) to enhance the capcity of $RuO_2$/MWNT composite electrode materials for ultracapacitor. Both treatments generated a number of defects on the surface of MWNT by the breakage of $\pi$ bond in graphene layer at which carboxyl groups were introduced. However, the degree of hydrophilicity generated by strong acid treatment was higher than that by heat treatment in air, which was revealed by the quantitative measurement of surface carboxyl groups by using Boehm titration. The increased hydrophilicity save rise to an improved dispersity of $RuO_2$ nanoparticles on MWNT. Finally, the improved dispersity resulted in the capacity enhancement of composite electrode materials for ultracapacitor.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2002년도 추계학술대회 논문집 Vol.15
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• pp.236-239
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• 2002

Surface states of silicone polymer treated by plasma were investigated by the analysis by x-ray photoelectron spectroscopy (XPS) and surface voltage decay. Plasma treatment causes the silica-like oxidative layer, which is confirmed with XPS, and lowers surface resistivity with increasing the plasma treatment time. Using the decay time constant of surface voltage, the calculated surface resistivity was compared with the value directly measured by a voltage-current method. A good agreement between two methods was obtained. In addition, we estimated the thermal activation energy for surface conduction, Based on our results, we could understand the relationship between surface chemical states and surface electrical properties.

• 한국표면공학회지
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• 제44권6호
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• pp.246-249
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• 2011

Surface modification before coating nickel by coupling agents and/or etchant of glass did not provide enough adhesive strength of electroless nickel deposits on glass. Effect of heat treatments on hardness as well as adhesion of nickel deposits was studied by using tape test for adhesion, nanoindenter for hardness and glancing angle x-ray diffractometer (GAXRD) for phase characterization. Heat treatment improved hardness as well as adhesion. XRD results give that the improvements of adhesion and hardness are due to the formation of $NiSiO_4$ around the interface between the nickel deposits and the glass and the precipitation of $Ni_3P$ causing precipitation hardening, respectively. The details in effects of heat treatment on adhesion and hardness are described here.

• 한국염색가공학회지
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• 제34권2호
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• pp.102-108
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• 2022

The physicochemical properties of stainless steel fibers which were modified by oxygen plasma treatment were analyzed through microscopy and XPS analysis. The wettability of the surface of the stainless steel fiber was observed by measuring water contact angle to find out the effect of the plasma treatment time on the surface characteristics of the stainless steel fiber. In addition, in order to understand the effect of oxygen plasma treatment on the deterioration of the stainless steel fiber properties, the physical properties due to plasma treatment was investigated by measuring the weight reduction, tensile strength, elongation, tensile modulus of the stainless steel fibers according to the treatment time. As a result, the stainless steel fiber surface was etched by the oxygen plasma and the surface became more wettable by the introduction of hydrophilic functional groups. However the physical properties of the stainless steel fiber were not significantly deteriorated even if the surface of the stainless steel fiber made hydrophilic.