Journal of Surface Science and Engineering (한국표면공학회지)

The Korean Institute of Surface Engineering (한국표면공학회)
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Effect of Heat Treatment on the Adhesive Strength of Electoless Nickel Deposits

무전해법으로 Slide Glass 위에 도금된 Ni층의 접착력에 미치는 열처리의 영향

  • Hyun, Yong-Min (School of Material Science & Engineering, Hongik University) ;
  • Yu, Sung-Yeol (School of Material Science & Engineering, Hongik University) ;
  • Yoon, Jung-Yun (School of Material Science & Engineering, Hongik University) ;
  • Kim, Bo-Young (School of Material Science & Engineering, Hongik University) ;
  • Kim, Sun-Ji (School of Material Science & Engineering, Hongik University) ;
  • Tahk, Song-Hee (School of Material Science & Engineering, Hongik University) ;
  • Kim, Hee-San (School of Material Science & Engineering, Hongik University)
  • 현영민 (홍익대학교 재료공학부) ;
  • 유성렬 (홍익대학교 재료공학부) ;
  • 윤정윤 (홍익대학교 재료공학부) ;
  • 김보영 (홍익대학교 재료공학부) ;
  • 김선지 (홍익대학교 재료공학부) ;
  • 탁송희 (홍익대학교 재료공학부) ;
  • 김희산 (홍익대학교 재료공학부)
  • Received : 2011.09.15
  • Accepted : 2011.12.30
  • Published : 2011.12.31
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Abstract

Surface modification before coating nickel by coupling agents and/or etchant of glass did not provide enough adhesive strength of electroless nickel deposits on glass. Effect of heat treatments on hardness as well as adhesion of nickel deposits was studied by using tape test for adhesion, nanoindenter for hardness and glancing angle x-ray diffractometer (GAXRD) for phase characterization. Heat treatment improved hardness as well as adhesion. XRD results give that the improvements of adhesion and hardness are due to the formation of $NiSiO_4$ around the interface between the nickel deposits and the glass and the precipitation of $Ni_3P$ causing precipitation hardening, respectively. The details in effects of heat treatment on adhesion and hardness are described here.

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