• 대한치과보철학회지
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• 제40권4호
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• pp.344-351
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• 2002

The purpose of this study is to compare tensile bond strength between Cr-Co alloy and three denture base resins after surface treatment. Following the manufacturer's instructions, 180 bonded specimens were made from three denture base resins (Lucitone 199. Paladent 20. POSS resin) and three surface treatment methods (sandblasting. metal primer. silicoating) 20 samples were made in each group and a half was ther-mocycled 1000 times between $5^{\circ}C$ and $55^{\circ}C$. The tensile bond strength was measured using an Instron with 5mm/min crosshead speed. Data was analyzed with one-way ANOVA, T-test and Duncan test. The results were as follows : 1. Samples with metal primer coating had significantly high tensile bond strength than the other surface treated groups (p<.05). Significantly low tensile bond strength was shown in sand blasted groups (p<.05). 2. No significant difference was observed in metal primer coating groups before and after ther-mocycling (p>.05) 3. Tensile bond strength was decreased in silicoated samples after thermocycling (p<.05). 4. Of the surface treated groups with metal primer, Lucitone 199 had the greatest bond strength and POSS resin and Paladent 20 were followed (p<.05). 5. Of the surface treated groups with silicoating, POSS resin and Lucitone 199 had greater bond strength than Paladent 20 (p<.05).

• 구강회복응용과학지
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• 제32권3호
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• pp.194-201
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• 2016

목적: 본 연구는 Co-Cr, Ti-6Al-4V 합금에 Zirconium Nitride (이하 ZrN) 적용 시, 의치상 레진과의 접착력을 비교하는 것이다. 연구 재료 및 방법: Co-Cr, Ti-6Al-4V 디스크(직경 10 mm, 두께 2.5 mm)를 각각 14개씩 제작하였고, ZrN 코팅에 따라 2개의 그룹으로 나누었다. Primer로 시편 전처리 후, 의치상 레진(직경 6 mm, 두께 5 mm)을 부착하였다. 표면 측정기를 이용하여 시편의 거칠기를 측정한 후, 만능 시험기를 이용하여 전단결합강도를 측정하였으며, 이원분산분석으로 통계 분석하였다. 시편 표면과 파절 양상을 주사전자현미경을 이용하여 관찰하였다. 결과: ZrN을 코팅한 시편에서 유의하게 높은 표면 거칠기를 나타내었고(P < 0.05), 전단결합강도는 낮았다(P < 0.001). ZrN 코팅 시편에서는 혼합성 파절과 부착성 파절이 함께 나타났다. 결론: Co-Cr, Ti-6Al-4V 합금에서 ZrN 코팅 처리는 의치상 레진과의 결합력을 약화시켰다.

• The Journal of Advanced Prosthodontics
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• 제10권5호
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• pp.361-366
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• 2018

PURPOSE. The aim of this study was to evaluate the effects of relining materials on the flexural strength of relined thermoplastic denture base resins (TDBRs). MATERIALS AND METHODS. For shear bond strength testing, 120 specimens were fabricated using four TDBRs (EstheShot-Bright, Acrytone, Valplast, Weldenz) that were bonded with three autopolymerizing denture relining resins (ADRRs: Vertex Self-Curing, Tokuyama Rebase, Ufi Gel Hard) with a bond area of 6.0 mm in diameter and were assigned to each group (n=10). For flexural strength testing, 120 specimens measuring $64.0{\times}10.0{\times}3.3mm$ (ISO-1567:1999) were fabricated using four TDBRs and three ADRRs and were assigned to each group (n=10). The thickness of the specimens measured 2.0 mm of TDBR and 1.3 mm of ADRR. Forty specimens using four TDBRs and 30 specimens using ADRRs served as the control. All specimens were tested on a universal testing machine. For statistical analysis, Analysis of variance (ANOVA) with Tukey's test as post hoc and Spearman's correlation coefficient analysis (P=.05) were performed. RESULTS. Acry-Tone showed the highest shear bond strength, while Weldenz demonstrated the lowest bond strength between TDBR and ADRRs compared to other groups. EstheShot-Bright exhibited the highest flexural strength, while Weldenz showed the lowest flexural strength. Relined EstheShot-Bright demonstrated the highest flexural strength and relined Weldenz exhibited the lowest flexural strength (P<.05). Flexural strength of TDBRs (P=.001) and shear bond strength (P=.013) exhibited a positive correlation with the flexural strength of relined TDBRs. CONCLUSION. The flexural strength of relined TDBRs was affected by the flexural strength of the original denture base resins and bond strength between denture base resins and relining materials.

• 대한치과보철학회지
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• 제58권4호
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• pp.300-305
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• 2020

목적: 인공치의 표면처리가 3D 프린팅 의치상레진과의 전단결합강도에 미치는 영향을 알아보고 임상적용에 있어 참고하기 위함이다. 재료 및 방법: 3D 프린팅 의치상레진을 3D 프린터를 이용하여 시편을 제작하였고, 인공치의 표면처리는 sandblasting, 프라이머의 적용 유무에 따라 5가지 군으로 나누어, 각 군마다 10개씩 진행하였다. Universal testing machine을 이용하여 전단 결합 강도를 측정하였고, 측정값은 one-way ANOVA로 통계분석 후 Turkey test를 통해 사후검정하였다. 이후 파절된 시편을 주사전자현미경을 이용하여 관찰하였다. 결과: 평균전단결합강도는 표면 처리 하지 않은 군에서 가장 낮은 값을 나타내었으며, 프라이머 처리한 군에서 유의하게 높은 결과 값을 나타내었다(P < .05). 또한 프라이머 처리한 군에서 대부분 응집파절을 나타내었다. 결론: 3D 프린팅 의치상레진에 인공치를 결합 시 인공치의 기계적·화학적 표면처리는 전단결합강도를 증가시켜 3D 프린팅 방식을 사용하여 의치를 제작할 경우 기계적·화학적 표면처리를 통해 인공치의 탈락을 줄일 수 있으며, 특히 sandblasting 과 프라이머를 처리하는 방법이 추천된다.

• The Journal of Advanced Prosthodontics
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• 제4권1호
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• pp.30-36
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• 2012

PURPOSE. The aim of this in-vitro investigation was to describe the effect of reinforcement with different fibers on impact strength of heat polymerized poly-methyl methacrylate (PMMA) denture base resin and to analyze the effect of surface treatment of the fibers on the impact strength. MATERIALS AND METHODS. The specimens were fabricated from the dies formed as per standard ASTM D4812. 2% by weight of glass, polyethylene and polypropylene fibers were incorporated in the PMMA resin. The Izod impact testing was performed on the unnotched specimens and the values obtained were analyzed using appropriate one way ANOVA, followed by unpaired t-test. Fractured ends of the samples were subjected to the SEM analysis. RESULTS. The polypropylene fibers with plasma treatment showed the highest impact strength ($9.229{\times}10^2$ J/m) followed by the plasma treated polyethylene fibers ($9.096{\times}10^2$ J/m), untreated polypropylene fibers ($8.697{\times}10^2$ J/m), untreated polyethylene fibers ($7.580{\times}10^2$ J/m), silane treated glass fibers ($6.448{\times}10^2$ J/m) and untreated glass fibers ($5.764{\times}10^2$ J/m). Also the surface treatment of all the fibers has shown the significant improvement in impact strength. Findings of the SEM analysis justified the improvement in impact strength after surface treatment. CONCLUSION. Reinforcement with the fiber is an effective method to increase the impact strength of PMMA denture base resin. The surface treatment of fibers further increases the impact strength significantly.

• The Journal of Advanced Prosthodontics
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• 제3권3호
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• pp.136-139
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• 2011

PURPOSE. A new light curing urethane dimethacrylate and a cold curing resin with simpler and faster laboratory procedures may have even improved flexural properties. This study investigated the 3-point flexural strengths and flexural moduli of two alternate base materials. MATERIALS AND METHODS. A cold curing resin (Weropress) and a light curing urethane dimethacrylate base material (Eclipse). Along with Eclipse and Weropress, a high impact resin (Lucitone199) and three conventional base materials (QC 20, Meliodent and Paladent 20) were tested. A 3-point bending test was used to determine the flexural strengths and flexural moduli. The mean displacement, maximum load, flexural modulus and flexural strength values and standard deviations for each group were analyzed by means of one-way analysis of variance (ANOVA) (with mean difference significant at the 0.05 level). Post hoc analyses (Scheffe test) were carried out to determine the differences between the groups at a confidence level of 95%. RESULTS. Flexural strength, displacement and force maximum load values of Eclipse were significantly different from other base materials. Displacement values of QC 20 were significantly different from Lucitone 199 and Weropress. CONCLUSION. The flexural properties and simpler processing technique of Eclipse system presents an advantageous alternative to conventional base resins and Weropress offers another simple laboratory technique.

• The Journal of Advanced Prosthodontics
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• 제5권3호
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• pp.287-295
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• 2013

PURPOSE. This study investigated the effect of laser parameters and air-abrasion on the peel strength of silicon-based soft denture liner to different denture resins. MATERIALS AND METHODS. Specimens (N=180) were prepared out of three different denture base resins (Rodex, cross-linked denture base acrylic resin; Paladent, heat-cured acrylic resin; Deflex, Polyamide resin) ($75mm{\times}25mm{\times}3mm$). A silicon-based soft denture liner (Molloplast B) was applied to the denture resins after the following conditioning methods: a) Air-abrasion ($50{\mu}m$), b) Er,Cr:YSGG laser (Waterlase MD Turbo, Biolase Technology) at 2 W-20 Hz, c) Er,Cr:YSGG laser at 2 W-30 Hz, d) Er,Cr:YSGG laser at 3 W-20 Hz, e) Er,Cr:YSGG laser at 3 W-30 Hz. Non-conditioned group acted as the control group. Peel test was performed in a universal testing machine. Failure modes were evaluated visually. Data were analyzed using two-way ANOVA and Tukey's test (${\alpha}$=.05). RESULTS. Denture liner tested showed increased peel strength after laser treatment with different parameters ($3.9{\pm}0.4-5.58{\pm}0.6$ MPa) compared to the control ($3.64{\pm}0.5-4.58{\pm}0.5$ MPa) and air-abraded groups ($3.1{\pm}0.6-4.46{\pm}0.3$ MPa), but the results were not statistically significant except for Paladent, with the pretreatment of Er,Cr:YSGG laser at 3 W-20 Hz. Polyamide resin after air-abrasion showed significantly lower peel strength than those of other groups ($3.1{\pm}0.6$ MPa). CONCLUSION. Heat-cured acrylic resin, PMMA, may benefit from Er,Cr:YSGG laser treatment at 3 W-20 Hz irradiation. Air-abrasion of polyamide resins should be avoided not to impair their peel bond strengths to silicon-based soft denture liners.

• 대한치과보철학회지
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• 제40권4호
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• pp.386-395
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• 2002

This study would like to measure and compare water sorption and solubility of acrylic resins, with 3 different polymerizing methods, and tensile strength between denture base resin and relining rosins. For this experiment, 3 different acrylic resins were used; heat polymerizing resin: Vertex (Dentmex, Zeist, Holland), autopolymerizing resin: Tokuso Rebase (Tokuyama Corp, Tokyo, Japan), and light curing resin: Mild Rebaron LC(GC Corp, Tokyo, Japan) The results were as follows ; 1. Tokuso Rebase showed the lowest water sorption. followed by Mild Rebaron LC and Vertex. Among resins, there were some signigicant differences (P<0.05). 2. Vertex showed the lowest solubility, followed by Mild Rebaron LC and Tokuso Rcbase. Among resins, there were some signigicant differences (P<0.05). 3. Intact Vertex showed the highest tensile strength, and Mild Rebaron LC had a more tensile strength than Tokuso Rebase. Between Vertex and the other resins, there were some signigicant differences (P<0.05) However, between Mild Rebaron LC and Tokuso Rebase, there was no statistical difference (P>0.05). About 50% of Rebaron LC showed cohesive fracture. 4. Tensile strength has more decreased after thermocycling than before, but there was no statistical difference (P>0.05).

• 구강회복응용과학지
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• 제16권3호
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• pp.211-220
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• 2000

The use of autopolymerizing-cured resin and light-cured resin for direct relining of complete and partial dentures has been popular. This investigation compared the adhesion of autopolymerizing-cured reline resin(Tokuso Rebase, Mild Rebaron) or light-cured reline resin(Mild Rebaron LC, Lighton-U) to metal base or resin base. Cylindrical samples were made from metal($Biosil^{(R)}$) or heat-cured resin(QC-20) and were prepared to produce a flat bonding surface. Cylindrical metal samples were roughened by scratch or by scratch and sandblast and were treated with primer(MR Bond) after scratch and sandblast. And then, liners were prossesed to the cylindrical metal or resin samples according to the manufacturer's recommendations so as to bond metal base or resin base. The specimens were tested in pure tension by using an Instron Univesal testing machine for the four direct reline resins. The results were as follows ; 1. In comparison with tensile bond strength of material relined on resin base or metal base, the case of resin base produced significantly higher tensile bond strength than the case of metal base. 2. Metal surface pretreatment or primer improved the tensile bond strength between the reline resin and the metal($Biosil^{(R)}$) base. 3. The tensile bond strength of Mild Rebaron LC relined on resin base or metal base were similar to those of the other reline resins.

• 대한치과보철학회지
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• 제45권3호
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• pp.310-320
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• 2007

Statement of the problem. The fracture of acrylic resin dentures remains an unsolved problem. Therefore, many investigations have been performed and various approaches to strengthening acrylic resin, for example, the reinforcement of heat-cured acrylic resin using glass fibers, have been suggested over the years. But problems such as poor workability, rough surface, poor adhesion of glass fiber resin complex are not solved yet. Purpose. The aim of the present study was to investigate the effect of short glass fibers on the transverse strength of heat-polymerized denture base acrylic resin and roughness of resin complex after abrasion test. Material and methods. To avoid fiber bunching and achieve even fiber distribution, glass fiber bundles were mixed with acrylic resin powder in conventional mixer with a non-cutting blade, to produce the glass fiber($10{\mu}m$ diameter, 3mm length, silane treated) resin composite. Glass fibers were incorporated at 0%, 3%, 6% and 9% by weight. Transverse strength were measured. After abrasion test, surface roughness was evaluated and scanning electron microscope view was taken for clinical application. Results. 1. 6% and 9% incorporation of 3mm glass fibers in the acrylic resin enhanced the transverse strength of the test specimens(p<0.05). 2. Before abrasion test, incorporation of 0%, 3%, 9% glass fiber in the resin showed no dirrerence in roughness statisticaly(p>0.05). 3. After abrasion test, incorporation of 0%, 3%, 6% glass fiber in the resin showed same surface roughness value statistically(p>0.05). 4. In SEM, surface roughness increased as the percentage of the fibers increased. 5. In the areas where glass fiber bunchings are formated, a remarkably high roughness was noticed. Conclusion. 6% and 9% addition of silane-treated short glass fibers into denture base acrylic resin increased transverse strength significantly. Before and after abrasion test, incorporation of 0%, 3%, 6% glass fiber in the resin showed same surface roughness value statistically.