• Journal of the Korean Vacuum Society
• /
• v.7 no.1
• /
• pp.59-65
• /
• 1998

Multi-layer diamond-like carbon (DLC) films were deposited by 13.56 MHz r.f. PACVD method. Multi-layer DLC film was composed of 2.5 $mu extrm{m}$ thick pure DLC filml and 0.2$\mu\textrm{m}$ thick Si incorporated DLC (Si-DLC) film as a surface layer. Tribological behaviors of the multi-layer DLC film were investigated with a ball-on-disk type tribometer in ambient atmosphere using AISI 52100 steel ball. Low friction coefficient (<0.1) period increased with increasing the Si content in the surface Si-DLC film. The wear rate after 44,000 cycles and 158,400 cycles were the $2.5\times10^{-8}\sim1.8\times10^{-7}\textrm{mm}^3$/rev. and $7.1\times10^{-9}\sim1.8\times10^{-8}\textrm{mm}^3$/rev.,respectively. The wear rate of the multi-layer DLC film after 158,400 cycles was about 2 times smaller than that of pure DLC films of 2.7 $\mu\textrm{m}$ thickness. This high wear resistance and low friction coefficient was caused by the formation of Si oxide layer on the wear scar surface, as confirmed by the debris composition analysis. It was further shown that this si oxide debris layer on the wear scar surface is formed again even after removing the debris of the steel ball, which maintain the low friction coefficient between multi-layer DLC films and steel ball.

• Tribology and Lubricants
• /
• v.33 no.6
• /
• pp.296-302
• /
• 2017

Ball milling of elemental powders in advance and using an induction heating system for intermetallic coatings are known to enhance the reactivity of combustion synthesis. In this work, the effects of simultaneously applying these two incentive methods on the properties of intermetallic coatings are studied. Ni-Al powder compacts ball-milled with three different ball-to-powder weight ratio mixtures are synthesized and coated on mild steel by combustion synthesis in an induction heating system. Consequently, similar to an electrical heating system, the positive effects of ball milling on the combustion synthesis are confirmed in the induction heating system. The enhancement in synthetic reactivity achieved by applying the two incentive methods at the same time is greater than that by applying each incentive method separately. In particular, the enhancement is remarkable at low reaction temperature. However, there are limitations to improving the reactivity by simultaneously applying the two incentive methods to the combustion synthesis, unlike the reaction temperature. The microstructure and hardness of the coating layer are both influenced by the ball-charging ratio employed in the ball-milling process.

• Journal of Powder Materials
• /
• v.21 no.2
• /
• pp.97-101
• /
• 2014

The 304 stainless steel powders were prepared by high energy ball milling and subsequently sintered by spark plasma sintering, and the microstructural characteristics and micro-hardness were investigated. The initial size of the irregular shaped 304 stainless steel powders was approximately 42 ${\mu}m$. After high energy ball milling at 800 rpm for 5h, the powders became spherical with a size of approximately 2 ${\mu}m$, and without formation of reaction compounds. From TEM analysis, it was confirmed that the as-milled powders consisted of the aggregates of the nano-sized particles. As the sintering temperature increased from 1073K to 1573K, the relative density and micro-hardness of sintered sample increased. The sample sintered at 1573K showed the highest relative density of approximately 95% and a micro-hardness of 550 Hv.

• Journal of Korea Foundry Society
• /
• v.39 no.5
• /
• pp.87-93
• /
• 2019

The effects of mold materials on the microstructure and tensile properties were investigated to develop a mass production technique of aluminum alloy parts with excellent mechanical properties using a lost foam casting method. The microstructures of the plate-shaped cast alloy showed a tendency to be finer in proportion to the thickness of the plate, and a remarkably fine structure was obtained by applying a steel chill or a ball as a mold material compared to general sand. When a steel ball was used, it was observed that the larger the ball, the finer the cast structure and the better the tensile properties. The microstructure and tensile properties of the cast parts with complex shapes were greatly affected by the gating system, but the positive effects of the steel chill and the steel ball as a mold material were clear.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
• /
• 2001.06a
• /
• pp.319-326
• /
• 2001

The sliding wear characteristics of carbon steel castings were Investigated using a ball on disk type tester. The experiment was conducted using high carbon steel wire rods as ball material and carbon steel castings as disk material and different operating conditions, at room temperature under a lubrication and dry conditions. The results showed that the carbon steel castings appeared average wear volume Is lowed after annealing under a lubrication conditions and wear curve linear Increased. The specific wear rate of carbon steel castings Increased with wire diameter lubrication and dry also Increased 125 times In Ory. The sliding wear mechanism were Investigated due to fatigue wear lubrications and abrasive wear dries also wire Included fatigue and abrasive wear by plastic flow.

• Proceedings of the Korean Society of Precision Engineering Conference
• /
• 1993.10a
• /
• pp.37-41
• /
• 1993

ball screw is a critical machine component which dictates the precison of a given machine tool. The conventional manufacturing method requires the heat treated ball screw to be ground to its final dimensions. This study looks into the the feasibility of replacing the grinding process with a simpler process, namely threading on NC lathe. The purpose is to reduce the capital investment as well as production time in the manufacture of ball screws. Ceramics and CBN cutting tools are compared with respect to their ability to machine hardened steel. It is shown that CBN tools can be successfully utilized to machine precision ball screws with superior suface qualities.

• Journal of Powder Materials
• /
• v.3 no.3
• /
• pp.167-173
• /
• 1996

The effect of ball milling on the pressureless sintering of MoSi$_2$ was investigated. Ball milling was conducted at 70 rpm for 72 hours using different balls and vessels: one used tungsten carbide balls in a plastic vessel(referred as B-powder) and the other stainless steel ball in a stainless steel vessel(referred as C- powder). The powder was compacted with 173MPa and subsequently sintered at the temperature range of 1150 $^{\circ}C$ and 1450 $^{\circ}C$ in H$_2$, atmosphere. Sintered density was measured and scanning electron micrograph was observed. Over 90% of the theoretical density was attained at 1250 $^{\circ}C$ within 10 minutes for C-powders, while the similar densification required a sintering temperature of 1450 $^{\circ}C$ for B-powders. Such a difference in sinterability between B and C-powders was discussed in terms of the effect of particle size reduction and activated sintering caused by Ni and/or Fe introduced during ball milling.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.27 no.3
• /
• pp.335-342
• /
• 2003

In this study, the effects of oxide layer formed on the contact parts of TiN coated ball and steel disk in sliding are investigated. Also wear mechanism to from the oxide layer and the characteristics of the oxide layer formation are investigated. AISI 52100 steel ball is used for the substrate of coated ball specimens. Two types of coated ball specimens were prepared by depositing TiN coating with 1 and 4 ${\mu}{\textrm}{m}$ in coating thickness. AISI 1045 steel is used for the disk type counter-body. To investigate the effect of oxide layer on the contact parts of the two materials, the tests were performed both in air for forming oxide layer on the contact parts and in nitrogen environment to avoid oxidation. And to study the effects of surface roughness of counter-body, TiN coating thickness and contact load of sliding test on the characteristics of oxide layer formation on counter-body, various tests were carried out. From the results, the friction characteristics between the two materials was predominated by iron oxide layer that formed on wear track on counter-body and this layer caused the high friction. And the formation rate of the oxide layer on wear track increased as the real contact area between the two materials increased as the contact load increased, the TiN coating thickness decreased and the surface of counter-body smoothened.

• Proceedings of the KWS Conference
• /
• 1994.05a
• /
• pp.226-228
• /
• 1994

• Corrosion Science and Technology
• /
• v.11 no.5
• /
• pp.165-172
• /
• 2012

The corrosion resistance of epoxy-coated carbon steel was evaluated. The carbon steel surface was subjected to different treatment methods such as steel grit blasting with different size, steel shot ball blasting and power tool treatment. To study the effect of the treatments, the topology of the treated surface was observed by optical 3D microscopy and a pull-off adhesion test was conducted. The corrosion resistance of the epoxy-coated carbon steel was further examined by electrochemical impedance spectroscopy (EIS) combined with hygrothermal cyclic testing. The results of EIS indicated that the epoxy-coated carbon steel treated with steel grit blasting showed an improved corrosion resistance compared to untreated epoxy-coated surfaces or surfaces subjected to shot ball blasting and power tool treatments.