• Applied Microscopy
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• v.44 no.4
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• pp.133-137
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• 2014

We suggest a facile transmission electron microscopy (TEM) specimen preparation method for the direct (polymer-free) transfer of layer-area graphene from Cu substrates to a TEM grid. The standard (polymer-based) method and direct transfer method were by TEM, high-resolution TEM, and energy dispersive X-ray spectroscopy (EDS). The folds and crystalline particles were formed in a graphene specimen by the standard method, while the graphene specimen by the direct method with a new etchant solution exhibited clean and full coverage of the graphene surface, which reduced several wet chemical steps and accompanying mechanical stresses and avoided formation of the oxide metal.

• Journal of the Korean Society for Precision Engineering
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• v.31 no.7
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• pp.623-626
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• 2014

The LBB (Leak Before Break) concept is based on evaluating the fracture toughness. NUREG 1061, Vol.3 announced that the specimen for evaluating fracture resistance needs to have same thickness or thicker than pipe. Therefore, it is difficult to collect specimen from pipe which has same thickness as a pipe. So, ASTM standard suggested the use of standard specimen with 1 inch thickness. However, it has been known that an application of LBB by test results of standard specimen is conservative compare with that by real pipe. In this study, to supplement such conservatism, the evaluation of fracture resistance characteristics was performed with curved CT specimen, which has same thickness and curvature as a pipe. In addition, fracture resistance characteristics of curved CT specimen were compared with those of CT specimen. For this, shape factor F, hpl and g were obtained from FEM analysis using the limit load method.

• Proceedings of the KSME Conference
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• 2003.11a
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• pp.1240-1245
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• 2003

Reduced activation ferritic steel (JLF-1) is considered as a promising candidate material for blanket or first-wall structure of D-T fusion reactors. The fracture tests of fracture resistance curve (J-R curve) and $J_{IC}$ are desirable to investigate the exact fracture toughness of JLF-1 steel, since it has a high ductility. The fracture toughness of JLF-1 steel is affected by the configuration of test specimen such side groove, specimen thickness or specimen size. In this study, the fracture toughness tests were performed with various size(plane size and thickness) and various side groove of specimens. The test results showed the standard specimen with the side groove of 40 % represented a valid fracture toughness. The fracture resistance curve increased with increasing plane size and decreased with increasing thickness. However, the fracture resistance curve of half size specimen was similar to that of the standard specimen.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.27 no.9
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• pp.1531-1538
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• 2003

This paper compiles solutions of plastic $\eta$ factors and crack tip stress triaxialites for standard and nonstandard fracture toughness testing specimens, via detailed three-dimensional (3-D) finite element (FE) analyses. Fracture toughness testing specimens include a middle cracked tension (M(T)) specimen, SE(B), single-edge cracked bar in tension (SE(T)) and C(T) specimen. The ligament-to-thickness ratio of the specimen is systematically varied. It is found that the use of the CMOD overall provides more robust experimental J estimation than that of the LLD, for all cases considered in the present work. Moreover, the J estimation based on the load-CMOD record is shown to be insensitive to the specimen thickness, and thus can be used for testing specimen with any thickness. The effects of in-plane and out-of-plane constraint on the crack tip stress triaxiality are also quantified, so that when experimental J value is estimated according to the procedure recommended in this paper, the corresponding crack tip stress triaxiality can be estimated. Moreover, it is found that the out-of-plane constraint effect is related to the in-plane constraint effect.

• Proceedings of the KSME Conference
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• 2004.04a
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• pp.13-18
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• 2004

The objective of this study is to investigate fracture toughness and fatigue crack propagation behavior in the Reduced Activation Ferritic Steel (RAFs) JLF-I. The fracture toughness tests were performed with various size(plane size and thickness) and various side groove of specimens. The fatigue crack propagation behavior of the JLF-I steel was investigated by the constant-amplitude loading test for the stress ratios R=O.I, 0.3 and 0.5 respectively. The effects of stress ratios and specimen size on the fatigue crack growth behaviors for JLF-I steel were discussed within the Paris law. The test results showed the standard CT specimen with the side groove of 40 % represented a valid fracture toughness. The fracture resistance curve increased with increasing plane size and decreased with increasing thickness. However, the fracture resistance curve of half size specimen was similar to that of the standard specimen. The fatigue crack propagation rate of a half size specimen was similar to that of a full size specimen at the stress ratios of 0.1, 0.3 and 0.5 respectively. The fatigue crack propagation behavior of this material were evaluated by using a half size specimen.

• Proceedings of the Korea Concrete Institute Conference
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• 2002.05a
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• pp.157-162
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• 2002

This study is intended to present a reference data for effective quality control of concrete through comparing the rebound value of P type schmidt hammer with the compressive strength with variation of mix proportion and curing condition. According to the results, the air-curing specimen shows the higher rebound value than standard specimen except high strength in the whole. Also the vertical stroke shows higher rebound value than horizontal stroke in standard specimen, however, the rebound value of the two does not show prominent difference in air-curing specimen. The estimation equation of compressive strength derived from this experiment estimates the compressive strength more largely than the estimation equation in P type schmidt hammer manual. Therefore it is thought that the new estimation equation that fits our condition will have to be presented.

• Journal of the Korean Society for Precision Engineering
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• v.24 no.11
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• pp.84-90
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• 2007

In this study, design and manufacturing of plastic injection mold with cavity pressure/temperature sensors were performed fur tensile test specimen. International standard system for plastic tensile specimen was applied to design an injection molding system. Cavity pressure and temperature sensors were placed on the side of fixed platen of the injection mold to prevent them from external impact damage. Injection molding experiments with variations of injection speed and melt temperature were performed and then tensile test of the manufactured polycarbonate specimens was also performed. It was shown that injection molding processing parameters can have effect on the mechanical properties of the plastic injection molded part.

• Journal of the Korea institute for structural maintenance and inspection
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• v.4 no.1
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• pp.139-145
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• 2000

In this experimental program specimens. designed by the test variables, such as percentage of steel fiber incorporated, were constructed and tested to evaluate the flexural performance of reinforced steel fiber concrete beams. Based on the test results reported in this study, the following conclusions are made. Comparing with the load-displacement relationship of standard specimen, specimen over 0.5% of steel fiber incorporated, could be improved significantly flexural performance, such as capacity, ductility, and crack pattern. As increasing in quantity of steel fiber incorporated(0.5%~2.0%), the flexural strength of each specimen was shown the enhancement of 13%~40% in comparision with the standard specimen BSS.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.38 no.12
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• pp.1435-1440
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• 2014

The effects of the specimen size and temperature on the compressive strength of ATJ graphite were investigated. Compressive tests were conducted in accordance with ASTM C 965 at room temperature, $700^{\circ}C$ and $900^{\circ}C$. Three types of cylindrical specimen at room temperature were used in uniaxial tests, where the diameter-to - length ratios were one to two for the ASTM standard specimen, one to one for the Type I specimen, and one to 0.5 for the Type II specimen. Two kinds of cylindrical specimens, with and without antioxidant coating, were tested at elevated temperature. The Compressive strength of the expanded specimens(Type I, II) were slightly higher than that of standard specimen at room temperature. The compressive strength of a specimen with antioxidant coating increased as the temperature increased to $900^{\circ}C$. In contrast, that of the non-coated specimen decreases sharply due to the oxidation of the specimen.

• Journal of the Korea Institute of Building Construction
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• v.1 no.1
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• pp.143-150
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• 2001

Permanent-Form is one of system forms for reducing human labor, work costs, oscillation, noise, construction wastes and so on. Permanent-Form is made from precast method in facilities, and carried in construction site to assemble with no demolding. The biggest expense to produce permanent-Form is about manufacturing mold. This papers about structural efficiency evaluation, construction efficiency test. The result of this study is below. (1) In the compressive strength test of column. Fly ash specimen and polymer specimen's strength developed as each 8%, 14% to comparison with standard specimen. The reason of this result from form section area increase and form's reinforcing bar (2) The Degree of column crack in permanent form is lower than another one's The glass fiber's fiber reinforcement effect brings like this. (3) In the flexural load test of beam, the early crack load and maximum load of permanent form use specimen showed 20% higher than standard specimen's. (4) In field application experiment, an constructional error is satisfied with the allowable margin of error, $\pm$5mm (5) When the concrete is placed into the form inside, The transformation degree of permanent form is lower than plywood form's. (6) The concrete packing ability of permanent form is satisfactory. (7) The bonding strength of permanent form shows enough strength - 6kgf/$\textrm{cm}^2$.