• 제목/요약/키워드: standard measurement methods

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Accuracy Improvement of Lattice Parameters Measured from Electron Diffraction Data (전자회절을 이용한 격자상수의 측정 정확도 향상)

  • Lee, Sang-Gil;Song, Kyung;Kim, Jin-Gyu
    • Applied Microscopy
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    • v.41 no.1
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    • pp.75-79
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    • 2011
  • For quantitative analysis of nano-crystal structure, we reported the accuracy improvement method of lattice parameters measured from electron diffraction. For calculation of Au lattice parameters used as a standard crystal structure, it was considered two different acquisition methods (detector and enegy-filter) and three different calculation methods (conventional, least-square and regression fit). As a result, the measurement reliability could be enhanced by using CCD camera which gives higher performance, while energy-filtering did not affect the improvement the camera constant accuracy. Also, the accuracy of lattice parameters could be improved up to $10^{-4}$ order by regression fitting with correction formula. Finally, it is expected that the combination of regression fitting and intensity extraction from energy-filtered precession electron diffraction gives a solution of quantitative structure analysis for unknown nano-crystals.

The Study on the Performance of Clustering Algorithms in the Determination of Combat Fatigues (전투복 표준호수를 결정하기 위한 클러스터링 알고리즘의 성능에 관한 연구)

  • 김석구;김충영
    • Journal of the military operations research society of Korea
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    • v.26 no.2
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    • pp.8-27
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    • 2000
  • This paper evaluates the performance of clustering algorithms in the determination of combat fatigues. Among clustering algorithms, GLVQ in neural clustering methods. and ISODATA algorithm are evaluated in this paper. In order to evaluate, this study used the data sets which showed the body measurement of Korean military personnel. For the comparison of the three methods, the coverage rate and fitness for combat fatigues are evaluated and the convergence of final standard sizes are considered. As a result, the mean of the coverage rate and fitness for combat fatigues obtained with the GLVQ are higher than those obtained with -Means and ISODATA algorithms.

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A Study on Existing Evaluation Method and TES Method about Toughness of Fiber Reinforced Concrete (섬유보강콘크리트의 인성에 대한 기존평가방법과 TES 기법에 관한 연구)

  • 배주성;임정환;김경수
    • Proceedings of the Korea Concrete Institute Conference
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    • 1998.10b
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    • pp.797-802
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    • 1998
  • Fiber reinforcement can significantly improve the properties of concrete. Particulary, toughness or energy-absorbing ability of fiber reinforced concrete is frequently higher than that of unreinforced concrete. Toughness is a measure of energy absorption capacity and used to characterized fiber reinforced concrete's ability to resist fracture when subjected to static, dynamic and impact loads. However, the current standard methods of characterizing the toughness of fiber reinforced concrete have proven to be some inadequate and problems and have caused a great deal of dissent and confusion. This study research some of the inadequate and problems with these toughness measurement methods and proposes the evaluation method for Fiber Reinforced Concrete toughness.

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Approximate methods to evaluate storey stiffness and interstory drift of RC buildings in seismic area

  • Caterino, N.;Cosenza, E.;Azmoodeh, B.M.
    • Structural Engineering and Mechanics
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    • v.46 no.2
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    • pp.245-267
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    • 2013
  • During preliminary design of a RC building located in a seismic area, having quick but reliable analytical measurement of interstory drifts and storey stiffnesses might be helpful in order to check the fulfillment of damage limit state and stiffness regularity in elevation required by seismic design codes. This paper presents two approximate methods, strongly interrelated each other, and addressed to achieve each of these two purposes for frame buildings. A brief description of some already existing methods addressed to the same aims is included to compare the main differences in terms of general approaches and assumptions. Both new approximate methods are then applied to 9 'ideal' frames and 2 'real' buildings designed according to the Italian seismic code. The results are compared with the 'exact' values obtained by the code-based standard calculation, performed via FEM models, showing a satisfactory range of accuracy. Compared with those by the other methods from literature, they indicate the proposed procedures lead to a better approximation of the objective structural parameters, especially for those buildings designed according to the modern 'capacity design' philosophy.

Comparative Analysis of Accuracy between Computerized Tomography and Cephalogram for 3-Dimensional Measurement of Maxillofacial Structure (악안면 3차원 계측시 컴퓨터 단층촬영과 두부 방사선 규격사진의 정확성 비교 분석)

  • Paek, Jong-Su;Song, Jae-Chul;Lee, Hee-Kyung
    • Journal of Yeungnam Medical Science
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    • v.18 no.1
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    • pp.123-137
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    • 2001
  • Background: The purpose of this study is to evaluate the accuracy of measurements obtained from 3-dimensional computerized tomography and 3-dimensional cephalogram constructed by using the frontal and lateral cephalogram of six human dry skulls. Materials and Methods: After CT scans and each cephalograms were taken, 3-dimensional coordinates (X, Y, Z) of landmarks were obtained using computer programs. In this study, the accuracy of both methods were determined by means of 14 linear measurements compare with caliper measurements. Results: The standard deviation of landmarks of 3-dimensional CT and 3-dimensional cephalogram were 0.23 mm, and 0.30 mm in X axis, 0.27 mm and 0.25 mm in Y axis, and 0.27 mm and 0.31 mm in Z axis. In both methods, the standard deviation were less than 0.5 mm in all landmarks, and the most of landmarks showed less than 1 mm in range. Concerning the accuracy, the mean difference between 3-dimensional CT and manual measurements was 0.33 mm, and 1.13 mm between 3-dimensional cephalogram and manual measurements. The distance between RGo and LGo showed the largest difference (2.03 mm). There were highly significant, and large correlation with manual measurements in both methods (p<0.01). Conclusion: It is concluded that closeness of repeated measures to each skulls reveal the precision of both methods. Computerized tomography and cephalogram for 3-dimensional measurement of maxillofacial structure are equivalent in quality to caliper measurements.

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Study on Development of Embedded Source Depth Assessment Method Using Gamma Spectrum Ratio (감마선 스펙트럼 비율을 이용한 매립 선원의 깊이 평가 방법론 개발 연구)

  • Kim, Jun-Ha;Cheong, Jea-Hak;Hong, Sang-Bum;Seo, Bum-Kyung;Lee, Byung Chae
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.18 no.1
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    • pp.51-62
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    • 2020
  • This study was conducted to develop a method for depth assessment of embedded sources using gamma-spectrum ratio and for the evaluation of field applicability. To this end, Peak to Compton and Peak to valley ratio changes were evaluated according to 137Cs, 60Co, 152Eu point source depth using HPGe detector and MCNP simulation. The effects of measurement distance of PTV and PTC methods were evaluated. Using the results, the source depth assessment equation using the PTC and PTV methods was derived based on the detection distance of 50 cm. In addition, the sensitivity of detection distance changes was assessed when using PTV and PTC methods, and error increased by 3 to 4 cm when detection distance decreased by 20 cm based on 50 cm. However, it was confirmed that if the detection distance was increased to 100 cm, the effects of detection distance were small. And PTV and PTC methods were compared with the two distance measurement method which evaluates the depth of source by the change of net peak counting rate according to the detection distance. As a result of source depth assessment, the PTV and PTC showed a maximum error of 1.87 cm and the two distance measurement method showed maximum error of 2.69 cm. The results of the experiment confirmed that the accuracy of the PTV and PTC methods was higher than two distance measurement. In addition, Sensitivity evaluation by horizontal position error of source has maximum error of less than 25.59 cm for the two distance measurement method. On the other hand, PTV and PTC method showed high accuracy with maximum error of less than 8.04 cm. In addition, the PTC method has lowest standard deviation for the same time measurement, which is expected to enable rapid measurement.

Comparison of VOCs Concentration Characteristic According to Measurement Methods in Exhibition Hall (휘발성유기화합물(VOCs)의 측정방법에 따른 유물 전시관 내 농도 분포 특성 비교)

  • Lim, BoA;Lee, Sun Myung
    • 보존과학연구
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    • s.35
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    • pp.25-44
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    • 2014
  • In this study, measured annual year and seasonal concentrations of VOCs by Active type and Passive type using the measurement and analysis method in the exhibition hall and outdoor. It was compared with the correlation between the methods according the comparison of methods to measured concentrations. As a results, the annual average concentrations of TVOC in exhibition room($906.5{\mu}g/m^3$) was greater than for most of the study period, more than 1.8 times the standard in the Ministry of Environment. ${\Sigma}VOCs$ concentration of exhibition room by Active type was higher than Passive type. Some VOCs was decreased with the lapse of time a temporary increase tendencies was. The annual average I/O ratio of TVOC was 9.0, ${\Sigma}VOCs$ was confirmed to occur in a large amount inside the exhibition hall ${\Sigma}VOCs$ was studied to 34.0. Correlation coefficient of ${\Sigma}VOCs$ was 0.367. Toluene was 0.567 that the survey was the largest analysis to the relationship between the two methods.

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Comparative evaluation of marginal and internal fit of three-unit Co-Cr frameworks fabricated by metal milling and direct metal laser sintering methods (금속 밀링과 직접 금속 레이저 소결 방식으로 제작한 3본 코발트-크롬 구조물의 변연 및 내부 적합도 비교 평가)

  • Ahn, Jae-Seok;Lee, Jung-Hwan
    • Journal of Technologic Dentistry
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    • v.42 no.2
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    • pp.81-89
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    • 2020
  • Purpose: This in vitro study was conducted to evaluate the marginal and internal fit of three-unit Co-Cr frameworks fabricated by computer-aided metal milling and direct metal laser sintering(DMLS) systems in comparison to conventional casting method. Methods: Three-unit Co-Cr frameworks were fabricated by conventional wax up with casting(CWC), computer-aided metal milling(MM) and direct metal laser sintering(DMLS)(n=10 each). The marginal and internal fit of specimens were examined using a light-body silicone impression material. The thickness of light-body silicone was measured at eight reference points each, divided in the mesio distal and bucco lingual directions. All measurements were conducted by a stereomicroscope. Digital photos were taken at 150× magnification and then analyzed using a measurement software. The Kruskal-Wallis test and Bonferroni correction were used for analyzing the results. Results: The mean(SD) is ㎛ for fabrication methods, the mean marginal fit were recorded respectively, DMLS 39(27), followed by CWC 63(38), MM 220(128). and the mean internal fit CWC 95(47), DMLS 116(49), MM 210(152). In addition, the largest gap was found in the occlusal surface area among the internal measurement areas of all groups. Conclusion: As a result, the direct metal laser sintering method showed better marginal and internal fit than the metal milling method. The marginal and internal fit were statistically different according to the three fabrication methods(p<0.001). Except the MM group, the marginal fit of the CWC and DMLS groups was below the clinical standard of 120 ㎛. Based on the results of this study, it can be applied to clinical use in the future.

A Study on the Factors Causing Analytical Errors through the Estimation of Uncertainty for Cadmium and Lead Analysis in Tomato Paste (불확도 추정을 통한 토마토 페이스트에서 카드뮴 및 납 분석의 오차 발생 요인 규명)

  • Kim, Ji-Young;Kim, Young-Jun;Yoo, Ji-Hyock;Lee, Ji-Ho;Kim, Min-Ji;Kang, Dae-Won;Im, Geon-Jae;Hong, Moo-Ki;Shin, Young-Jae;Kim, Won-Il
    • Korean Journal of Environmental Agriculture
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    • v.30 no.2
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    • pp.169-178
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    • 2011
  • BACKGROUND: This study aimed to estimate the measurement uncertainty associated with determination of cadmium and lead from tomato paste by ICP/MS. The sources of measurement uncertainty (i.e. sample weight, final volume, standard weight, purity, molecular weight, working standard solution, calibration curve, recovery and repeatability) in associated with the analysis of cadmium and lead were evaluated. METHODS AND RESULTS: The guide to the expression of uncertainty was used for the GUM (Guide to the expression of Uncertainty in Measurement) and Draft EURACHEM/CITAC (EURACHEM: A network of organization for analytical chemistry in Europe/Co-Operation on International Traceability in Analytical Chemistry) Guide with mathematical calculation and statistical analysis. The uncertainty components were evaluated by either Type A or Type B methods and the combined standard uncertainty were calculated by statistical analysis using several factors. Expected uncertainty of cadmium and lead was $0.106{\pm}0.015$ mg/kg (k=2.09) and $0.302{\pm}0.029$ mg/kg (k=2.16), on basis of 95% confidence of Certified Reference Material (CRM) which was within certification range of $0.112{\pm}0.007$ mg/kg for cadmium (k=2.03) and $0.316{\pm}0.021$ mg/kg for lead (k=2.01), respectively. CONCLUSION(s): The most influential components in the uncertainty of heavy metals analysis were confirmed as recovery, standard calibration curve and standard solution were identified as the most influential components causing uncertainty of heavy metal analysis. Therefore, more careful consideration is required in these steps to reduce uncertainty of heavy metals analysis in tomato paste.

Nondestructive Methods for the Detection of Internal Decay and the Vitality Measurement of Old-Giant Trees (노거수 활력 측정 및 내부 부후 검출을 위한 비파괴검사법)

  • Gao, Yuliang;Cha, Byeong Jin
    • Korean Journal of Heritage: History & Science
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    • v.42 no.1
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    • pp.144-157
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    • 2009
  • Nondestructive methods to check the vitality of trees and to find out internal decay of old-giant trees include the use of electrical resistance, ultrasound transmission time, microdrilling, and infrared thermography etc. Among these, ultrasound transmission offers some advantages compared to others such as it is an entirely nondestructive detection method and it can be applied to very big trees. However, the ultrasound equipment is comparatively expensive and not broadly spread yet. On the other hand, Shigometer is versatile to be applied to check vitality of the tree and find out internal decay. Electrical conductivity of plant tissues is a very useful characteristics to determine the vitality and internal decay of trees. Electrical resistance of cambial area tells about the vitality of a tree and electrical resistance of heartwood reveals discoloration or decay of it. For determination of the vitality of the tree, the standard equation for calibration of measured electrical resistances should be developed by measuring and analyzing electrical resistance from at least 30-40 trees of the same species with that tree. All the factors, especially tree species, diameter of the stem, and temperature, which can altered the electrical resistance of trees, should be taken into consideration in the development of the equation. If the standard equation is developed for old-giant trees that we should conserve, it will be very useful. In addition, periodical and continued measuring of a certain tree will help to determine the condition of the tree by comparing the measurement with accumulated data of the tree. Measuring electrical resistance of wood might not require the standard equation. But it also needs to check electrical resistance of sound wood of the same tree species. If the stems that should be examined is thicker than 40cm, it is better to use the ultrasound measurement combined to Shigometer.