• Title/Summary/Keyword: standard calibration

Search Result 1,148, Processing Time 0.034 seconds

Development of Float Water Level Meter Portable Calibration System (부자식 수위계 이동형 교정시스템 개발)

  • Hong, Sung-taek;Kim, Il-han;Choi, Jong-woong;Shin, Gang-wook
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
    • /
    • 2016.10a
    • /
    • pp.411-414
    • /
    • 2016
  • K-water institute is a calibration and test institute accredited by international standard calibration center for water-level meters. Due to the absence of on-site calibration system and procedure for Float Water Level Meter, the calibration was performed only in the standard calibration laboratory. In this study, mobile calibration system and procedure were developed to calibrate Float Water Level Meter on site using scale bar and camera. It is possible to obtain reliable water-level data and achieve consistent data management.

  • PDF

Determination of Chemical Composition of Toasted Burley Tobacco by Near Infrared Spectroscopy (근적외선분광법을 이용한 버어리 토스트엽의 화학성분 분석)

  • 김용옥;정한주;백순옥;김기환
    • Journal of the Korean Society of Tobacco Science
    • /
    • v.17 no.2
    • /
    • pp.177-183
    • /
    • 1995
  • This study was conducted to develop the most precise NIR(near infrared spectrometric) calibration for rapid determination of chemical composition in ground samples of toasted burley tobacco using stepwise, stepup, principal component regression(PCR), partial least square(PLS) and modified partial least square(MPLS) calibration method. The number of wavelength(W) selected by stepup multiple linear regression using: second derivative spectra was as follows: total sugar(TS)-4 W, nicotine-9 W, total nitrogen(TN)-2 W, ash-8 W, total volatile base(TVB)-5 W, chlorine4 W, L of color-6 W, a of color-6 W and b of color-7 W. Comparing the calibration equations followed by each chemical components, the most precise calibration equation was MPLS for 75, a and b of color, PLS for nicotine, ash, TVB, chlorine and L of color and stepup for TN. The standard error of calibration(SEC) and standard error of performance(SEP) between result of near infrared analysis and standard laboratory analysis were 0.18, 0.40% for 75, 0.06, 0.08% for nicotine, 0.18, 0.16% for TN, 0.33, 0.46% for ash, 0.04, 0.03% for TVB, 0.08, 0.06% for chlorine, 0.54, 0.58 for L of color, 0.22, 0.22 for a of color and 0.27, 0.27 for b of color, respectively. The SEC and SEP of ash and TVB were within allowable error of standard laboratory analysis, nicotine, TN and chlorine were 1.2-2.0 times and 75 were 2.1-4.0 times larger than allowable error of standard laboratory analysis. The ratio of SEC and SEP to mean were 1.5, 1.6% for L of color, 3.7, 3.8% for a of color and 1.8, 1.8% for b of color, respectively. Key words : burley tobacco chemistry, near infrared spectroscopy.

  • PDF

Simultaneous Determination of Tryptophan and Tyrosine by Spectrofluorimetry Using Multivariate Calibration Method (다변량 분석법을 이용한 Tryptophan과 Tyrosine의 형광분광법적 정량)

  • Lee, Sang-Hak;Park, Ju-Eun;Son, Beom-Mok
    • Journal of the Korean Chemical Society
    • /
    • v.46 no.4
    • /
    • pp.309-317
    • /
    • 2002
  • A spectrofluorimetric method for the simultaneous determination of amino acids (tryptophan and tyrosine) based on the application of multivariate calibration method such as principal component regression and partial least squares (PLS) to luminescence measurements has been studied. Emission spectra of synthetic mixtures of two amino acids were obtained at excitation wavelength of 257 ㎚. The calibration model in PCR and PLS was obtained from the spectral data in the range of 280-500 ㎚ for each standard of a calibration set of 32 standards, each containing different amounts of two amino acids. The relative standard error of prediction ($RSEP_a$) was obtained to assess the model goodness in quantifying each analyte in a validation set. The overall relative standard error of prediction ($RSEP_m$) for the mixture obtained from the results of a validation set, formed by 6 independent mixtures was also used to validate the present method.

Development of Calibration System of Helium Permeation Type Standard Leaks (헬륨 투과형 표준리크 교정장치 개발)

  • Hong S.S.;Lim I.T.;Shin Y.H.
    • Journal of the Korean Vacuum Society
    • /
    • v.15 no.4
    • /
    • pp.347-353
    • /
    • 2006
  • A helium permeation type standard leak calibration system has newly developed by using dynamic gas expansion method. The measurement range was extended lower to $10^{-6}$ Pa L/s for participating CCM (Consultative Committee for Mass and Related Quantities) standard leak key comparison. For the system, pressure ratios of high and ultra-high vacuum chamber and porous plug conductance for helium gas were determined. By using the system, a permeation type standard leak of $5.6{\times}10^{-4}$ Pa L/s range was calibrated. The calibration result showed that the difference between standard commercial leak was 11.1 %.

An automatic calibration technique for piezoelectric pressure transducers (압전형 압력센서의 교정기법 자동화)

  • Hong, Sung-Soo;Choi, Ju-Ho;Yoo, Jun
    • 제어로봇시스템학회:학술대회논문집
    • /
    • 1996.10b
    • /
    • pp.1368-1371
    • /
    • 1996
  • This paper presents an automatic calibration technique for piezoelectric low pressure transducer, which is useful to measure a pressure within 500 psi. This system with automatic calibration function and error correction algorithm generates standard dynamic pressure for the calibration of sensor. With the compensation for the offset voltage and the pressure error, the accuracy and the usefulness of the proposed scheme is validated.

  • PDF

An Automatic Calibration Technique for Piezoelectric Pressure Transducers (압전형 압력센서의 교정기법 자동화)

  • 홍성수;최주호
    • Proceedings of the Korean Society of Precision Engineering Conference
    • /
    • 1996.11a
    • /
    • pp.1012-1016
    • /
    • 1996
  • This paper presents an automatic calibration technique for piezoelectic low pressure transducer, which is useful to measure a pressure within 500 psi. This system with automatic calibration function and error correction algorithm generates standard dynamic pressure for the calibration of sensor. With the compensation for the offset voltage and the pressure error, the accuracy and the usefulness of the proposed scheme is validated.

  • PDF

Calibration Update for the Measuring Total Nitrogen Content in Rice Plant Tissue Using the Near Infrared Spectroscopy

  • Kwon, Young-Rip;Song, Young-Eun;Choi, Dong-Chil;Ryu, Jeong
    • KOREAN JOURNAL OF CROP SCIENCE
    • /
    • v.54 no.1
    • /
    • pp.29-35
    • /
    • 2009
  • The aim of the present study was to update the calibration that is used for the measurement of the total nitrogen content in the rice plant samples by using the visible and near infrared spectrum. Before the equation merge, correlation coefficient of calibration equation for nitrogen content on each rice parts was 0.945 (Leaf), 0.928 (Stem), and 0.864 (Whole plant), respectively. In the calibration models created by each part in the rice plant under the various regression method, the calibration model for the leaf was recorded with relatively high accuracy. Among of those, the calibration equation developed by Partial least squares (PLS) method was more accurate than the Multiple linear regression (MLR) method. The calibration equation was sensitive based on variety and location variations. However, we have merged and enlarged various of the samples that made not only to measure the nitrogen content more accurately, but also later sampling populations became more diversified. After merging, $R^2$ value becomes more accurate and significantly to 0.950 (L.), 0.974 (S.), 0.940 (W.). Also, after removal of outlier, R2 values increased into 0.998, 0.995, and 0.997. In view of the results so far achieved, Standard error of prediction (SEP) and SEP (C) were reduced in the stem and whole plant. Biases were reduced in the leaf, stem as well as whole plant. Slopes were high in the stem. Standard deviation reduced in the stem but $R^2$ was high in the stem and whole plant. Result was indicated that calibration equation make update, and updating robust calibration equation from merge function and multi-variate calibration.

The Error Analysis of the Rain-Gauges typed of Tipping Bucket according to Rainfall Intensity (강우강도에 따른 전도형 우량계의 오차특성 분석)

  • Shin, Gang-Wook;Hong, Sung-Taek;Lee, Dong-Keun
    • Proceedings of the KIEE Conference
    • /
    • 2005.07d
    • /
    • pp.2507-2509
    • /
    • 2005
  • Because the rain gauges of tipping bucket type can easily use the digital signal, the rain gauges are widely used for the meteorological observation. In general, the resolution of rain gauges of tipping bucket type can be categorized by the 0.1mm, 0.5mm, and 1.0mm classes. But, the error of the tipping bucket rain gauges is made by the intensity of rainfalls and is expected to make the standard calibration method for error measurement. Thus, we developed the hardware of standard calibration facility for rain gauges by weighting measurement method and proposed the standard procedure by rainfall intensity in this study. Also, we calculated the error for the rainfall intensity and obtained useful result through the proposed calibration method.

  • PDF

Standard calibration for H-α filter of DOAO 1m telescope

  • Ahn, Hojae;Pak, Soojong;Kang, Wonseok;Kim, Taewoo;Shim, Hyunjin
    • The Bulletin of The Korean Astronomical Society
    • /
    • v.42 no.2
    • /
    • pp.89.1-89.1
    • /
    • 2017
  • In this poster, we present standard calibration processes and results for photometry of $H-{\alpha}$ filter using broadband filters. We took data from a night in stable weather condition. And we derived parameters for band pass calibration including color terms. The corrected photometry results from broadband filters like V and R filters showed high correlation enough to replace instrumental $H-{\alpha}$ magnitude. We plan to extend these standardizing processes to another narrowband filters and flux calibration of narrowband filters from photometry of PNe.

  • PDF

Semiquantitative Analysis of metal for Cigarette Product by Inductively Coupled Plasma Mass Spectrometry (유도결합 플라스마 질량분석기를 이용한 담배 제품의 무기물 반정량 분석)

  • Cho, Sung-Eel;Kim, Hyo-Keun;Hwang, Keon-Joong
    • Journal of the Korean Society of Tobacco Science
    • /
    • v.31 no.2
    • /
    • pp.95-106
    • /
    • 2009
  • Semiquantitative analysis by ICP-MS has proven to be a powerful tool for fast screening, in addition, it does not require the element of interest to be present in the calibration standard, making it especially useful for the analysis of unknown samples. In this study, seven cigarette samples were analyzed by the rapid semi-quantitative analysis method based on the ICP-MS. For each cigarette sample, cut tobacco, cigarette paper, filter (before and after smoking), and smoke condensate were analyzed. The accuracy of the analysis technique was evaluated by comparing results obtained from Calibration Check Standard(CCS) and calibration method. Relative Percentage Error(RPE) value of all elements measured for three CCS showed a stable result of less than ${\pm}20%$. Compared to full quantitative analysis by calibration method, the results for cigarette samples showed average error within ${\pm}15%$.