Browse > Article

Semiquantitative Analysis of metal for Cigarette Product by Inductively Coupled Plasma Mass Spectrometry  

Cho, Sung-Eel (KT&G Central Research Institute)
Kim, Hyo-Keun (KT&G Central Research Institute)
Hwang, Keon-Joong (KT&G Central Research Institute)
Publication Information
Journal of the Korean Society of Tobacco Science / v.31, no.2, 2009 , pp. 95-106 More about this Journal
Abstract
Semiquantitative analysis by ICP-MS has proven to be a powerful tool for fast screening, in addition, it does not require the element of interest to be present in the calibration standard, making it especially useful for the analysis of unknown samples. In this study, seven cigarette samples were analyzed by the rapid semi-quantitative analysis method based on the ICP-MS. For each cigarette sample, cut tobacco, cigarette paper, filter (before and after smoking), and smoke condensate were analyzed. The accuracy of the analysis technique was evaluated by comparing results obtained from Calibration Check Standard(CCS) and calibration method. Relative Percentage Error(RPE) value of all elements measured for three CCS showed a stable result of less than ${\pm}20%$. Compared to full quantitative analysis by calibration method, the results for cigarette samples showed average error within ${\pm}15%$.
Keywords
Semiquantitative analysis; cigarette; ICP-MS;
Citations & Related Records
연도 인용수 순위
  • Reference
1 Wood, G., McCurdy, E. and Wilbur, S., Interference-free semiquantitative analysis using the Agilent 7500ce ICP-MS, Agilent Application Note 5989-1492EN, 2004
2 Davis, D. L. and Nielsen, M. T. (1999) Tobacco, 266
3 Amarasiriwardena, C. J., Gercken, B., Argentine, M. D. and Barnes, R. M., J. Anal. At. Spectrom., 1990, 5, 457   DOI   ScienceOn
4 Amarasiriwardena, D., Durrant, S. F., Lasztity, A., Krushevska, A., Argentine, M. D. and Barnes, R. M., Microchem. J. 1997, 56, 352   DOI   ScienceOn
5 Laborda, F., Medrno, J. and Castillo, J. R., J. Anal. At. Spectrom., 2001, 16, 732   DOI   ScienceOn
6 Tayor, H. E., Huff, R. A. and Montaser, Novel applications of ICP-MS, in: A. Montaser (Ed.), Inductively Coupled Plasma Mass Spectrometry, Wiley-VCH, New York, 1998, 681-807