• 제목/요약/키워드: standard calibration

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부자식 수위계 이동형 교정시스템 개발 (Development of Float Water Level Meter Portable Calibration System)

  • 홍성택;김일한;최종웅;신강욱
    • 한국정보통신학회:학술대회논문집
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    • 한국정보통신학회 2016년도 추계학술대회
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    • pp.411-414
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    • 2016
  • 장마 및 태풍, 집중호우 등 다량의 강우발생시 댐 및 하천의 수위 관측은 국민의 생명 및 재산과 직접 연관되는 상황으로 안전재난 대비를 위해서는 안정적인 실시간 수위 데이터 확보와 신뢰성 있는 데이터는 과학적이고 신뢰성 있는 수자원 관리를 위한 필요충분 요소이다. 그러나 현재 운영되고 있는 댐이나 하천 상하류의 수위계는 신뢰성 확보를 위하여 현장에서 검정 및 교정이나 보정 등이 쉽지 않은 실정이다. K-water연구원에서는 길이분야인 수위계에 대한 국제공인 교정기관으로 운영중에 있으며, 현장에서 부자식 수위계를 교정할 수 있는 시스템 및 절차서의 부재로 표준교정실에서만 교정을 실시하였다. 따라서 본 연구에서는 기준자와 카메라를 이용하여 부자식 수위계를 현장에서 교정할 수 있도록 이동형 교정시스템 및 표준교정 절차서를 개발하였으며, 수위 데이터의 신뢰성 있는 자료 확보와 일관성 있는 자료관리가 가능하도록 하였다.

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근적외선분광법을 이용한 버어리 토스트엽의 화학성분 분석 (Determination of Chemical Composition of Toasted Burley Tobacco by Near Infrared Spectroscopy)

  • 김용옥;정한주;백순옥;김기환
    • 한국연초학회지
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    • 제17권2호
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    • pp.177-183
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    • 1995
  • This study was conducted to develop the most precise NIR(near infrared spectrometric) calibration for rapid determination of chemical composition in ground samples of toasted burley tobacco using stepwise, stepup, principal component regression(PCR), partial least square(PLS) and modified partial least square(MPLS) calibration method. The number of wavelength(W) selected by stepup multiple linear regression using: second derivative spectra was as follows: total sugar(TS)-4 W, nicotine-9 W, total nitrogen(TN)-2 W, ash-8 W, total volatile base(TVB)-5 W, chlorine4 W, L of color-6 W, a of color-6 W and b of color-7 W. Comparing the calibration equations followed by each chemical components, the most precise calibration equation was MPLS for 75, a and b of color, PLS for nicotine, ash, TVB, chlorine and L of color and stepup for TN. The standard error of calibration(SEC) and standard error of performance(SEP) between result of near infrared analysis and standard laboratory analysis were 0.18, 0.40% for 75, 0.06, 0.08% for nicotine, 0.18, 0.16% for TN, 0.33, 0.46% for ash, 0.04, 0.03% for TVB, 0.08, 0.06% for chlorine, 0.54, 0.58 for L of color, 0.22, 0.22 for a of color and 0.27, 0.27 for b of color, respectively. The SEC and SEP of ash and TVB were within allowable error of standard laboratory analysis, nicotine, TN and chlorine were 1.2-2.0 times and 75 were 2.1-4.0 times larger than allowable error of standard laboratory analysis. The ratio of SEC and SEP to mean were 1.5, 1.6% for L of color, 3.7, 3.8% for a of color and 1.8, 1.8% for b of color, respectively. Key words : burley tobacco chemistry, near infrared spectroscopy.

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다변량 분석법을 이용한 Tryptophan과 Tyrosine의 형광분광법적 정량 (Simultaneous Determination of Tryptophan and Tyrosine by Spectrofluorimetry Using Multivariate Calibration Method)

  • 이상학;박주은;손범목
    • 대한화학회지
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    • 제46권4호
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    • pp.309-317
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    • 2002
  • 형광분광법에 의하여 주성분 회귀분석(principal component regression, PCR)과 부분 최소자승법(Partial least squares, PLS)을 이용하여 아미노산(Tryptophan and Tyrosine)을 동시에 정량하는 방법에 대하여 연구하였다. 아미노산 혼합물의 형광 스펙트럼은 들뜸파장을257nm로 고정하여 측정하였다. 두 가지 아미노산이 서로 다른 농도로 혼합되어 있는 32개의 시료용액을 280nm∼500nm 범위에서 스펙트럼들을 얻었고 이를 이용하여 PCR과 PLS회귀모델을 얻었다. 두 가지 아미노산이 서로 다른 농도로 포함된 6개의 외부검정용 시료들의 스펙트럼들을 이용해서 회귀모델의 적합성을 검정하기 위하여 외부검정용 시료의 농도를 계산하였다. 계산된 농도를 이용하여 relative standard error of prediction($RSEP_a$)를 얻었고 같은 방법으로 overall relative standard error of prediction($RSEP_m$) 도 구하였다

헬륨 투과형 표준리크 교정장치 개발 (Development of Calibration System of Helium Permeation Type Standard Leaks)

  • 홍승수;임인태;신용현
    • 한국진공학회지
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    • 제15권4호
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    • pp.347-353
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    • 2006
  • 국제도량형위원회의 질량 및 관련량 자문위원회 (CCM)가 주관하는 헬륨 투과형 표준리크(standard leak) 핵심측정표준 국제비교 (key comparison, KC)에 참여하기 위하여 기존의 정압형 리크표준기에 porous plug를 추가하여 측정범위를 $10^{-6}$ Pa L/s 까지 확장한 헬륨 미세리크 표준기를 개발하였다. 이를 위해 헬륨 기체에 대한 고진공 및 초고진공 표준기의 압력비와 porous plug의 콘덕턴스를 새롭게 측정하였으며, 개발된 장치를 이용하여 명목 값이 $5.6{\times}10^{-4}$ Pa L/s 인 투과형 표준리크를 직접 교정한 결과 표준기와 차이가 11.1 % 임을 알 수 있었다.

압전형 압력센서의 교정기법 자동화 (An automatic calibration technique for piezoelectric pressure transducers)

  • 홍성수;최주호;유준
    • 제어로봇시스템학회:학술대회논문집
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    • 제어로봇시스템학회 1996년도 한국자동제어학술회의논문집(국내학술편); 포항공과대학교, 포항; 24-26 Oct. 1996
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    • pp.1368-1371
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    • 1996
  • This paper presents an automatic calibration technique for piezoelectric low pressure transducer, which is useful to measure a pressure within 500 psi. This system with automatic calibration function and error correction algorithm generates standard dynamic pressure for the calibration of sensor. With the compensation for the offset voltage and the pressure error, the accuracy and the usefulness of the proposed scheme is validated.

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압전형 압력센서의 교정기법 자동화 (An Automatic Calibration Technique for Piezoelectric Pressure Transducers)

  • 홍성수;최주호
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 1996년도 추계학술대회 논문집
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    • pp.1012-1016
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    • 1996
  • This paper presents an automatic calibration technique for piezoelectic low pressure transducer, which is useful to measure a pressure within 500 psi. This system with automatic calibration function and error correction algorithm generates standard dynamic pressure for the calibration of sensor. With the compensation for the offset voltage and the pressure error, the accuracy and the usefulness of the proposed scheme is validated.

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Calibration Update for the Measuring Total Nitrogen Content in Rice Plant Tissue Using the Near Infrared Spectroscopy

  • Kwon, Young-Rip;Song, Young-Eun;Choi, Dong-Chil;Ryu, Jeong
    • 한국작물학회지
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    • 제54권1호
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    • pp.29-35
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    • 2009
  • The aim of the present study was to update the calibration that is used for the measurement of the total nitrogen content in the rice plant samples by using the visible and near infrared spectrum. Before the equation merge, correlation coefficient of calibration equation for nitrogen content on each rice parts was 0.945 (Leaf), 0.928 (Stem), and 0.864 (Whole plant), respectively. In the calibration models created by each part in the rice plant under the various regression method, the calibration model for the leaf was recorded with relatively high accuracy. Among of those, the calibration equation developed by Partial least squares (PLS) method was more accurate than the Multiple linear regression (MLR) method. The calibration equation was sensitive based on variety and location variations. However, we have merged and enlarged various of the samples that made not only to measure the nitrogen content more accurately, but also later sampling populations became more diversified. After merging, $R^2$ value becomes more accurate and significantly to 0.950 (L.), 0.974 (S.), 0.940 (W.). Also, after removal of outlier, R2 values increased into 0.998, 0.995, and 0.997. In view of the results so far achieved, Standard error of prediction (SEP) and SEP (C) were reduced in the stem and whole plant. Biases were reduced in the leaf, stem as well as whole plant. Slopes were high in the stem. Standard deviation reduced in the stem but $R^2$ was high in the stem and whole plant. Result was indicated that calibration equation make update, and updating robust calibration equation from merge function and multi-variate calibration.

강우강도에 따른 전도형 우량계의 오차특성 분석 (The Error Analysis of the Rain-Gauges typed of Tipping Bucket according to Rainfall Intensity)

  • 신강욱;홍성택;이동근
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2005년도 제36회 하계학술대회 논문집 D
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    • pp.2507-2509
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    • 2005
  • Because the rain gauges of tipping bucket type can easily use the digital signal, the rain gauges are widely used for the meteorological observation. In general, the resolution of rain gauges of tipping bucket type can be categorized by the 0.1mm, 0.5mm, and 1.0mm classes. But, the error of the tipping bucket rain gauges is made by the intensity of rainfalls and is expected to make the standard calibration method for error measurement. Thus, we developed the hardware of standard calibration facility for rain gauges by weighting measurement method and proposed the standard procedure by rainfall intensity in this study. Also, we calculated the error for the rainfall intensity and obtained useful result through the proposed calibration method.

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Standard calibration for H-α filter of DOAO 1m telescope

  • Ahn, Hojae;Pak, Soojong;Kang, Wonseok;Kim, Taewoo;Shim, Hyunjin
    • 천문학회보
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    • 제42권2호
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    • pp.89.1-89.1
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    • 2017
  • In this poster, we present standard calibration processes and results for photometry of $H-{\alpha}$ filter using broadband filters. We took data from a night in stable weather condition. And we derived parameters for band pass calibration including color terms. The corrected photometry results from broadband filters like V and R filters showed high correlation enough to replace instrumental $H-{\alpha}$ magnitude. We plan to extend these standardizing processes to another narrowband filters and flux calibration of narrowband filters from photometry of PNe.

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유도결합 플라스마 질량분석기를 이용한 담배 제품의 무기물 반정량 분석 (Semiquantitative Analysis of metal for Cigarette Product by Inductively Coupled Plasma Mass Spectrometry)

  • 조성일;김효근;황건중
    • 한국연초학회지
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    • 제31권2호
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    • pp.95-106
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    • 2009
  • Semiquantitative analysis by ICP-MS has proven to be a powerful tool for fast screening, in addition, it does not require the element of interest to be present in the calibration standard, making it especially useful for the analysis of unknown samples. In this study, seven cigarette samples were analyzed by the rapid semi-quantitative analysis method based on the ICP-MS. For each cigarette sample, cut tobacco, cigarette paper, filter (before and after smoking), and smoke condensate were analyzed. The accuracy of the analysis technique was evaluated by comparing results obtained from Calibration Check Standard(CCS) and calibration method. Relative Percentage Error(RPE) value of all elements measured for three CCS showed a stable result of less than ${\pm}20%$. Compared to full quantitative analysis by calibration method, the results for cigarette samples showed average error within ${\pm}15%$.