• Title/Summary/Keyword: sintered temperature

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Machinability of Pre-sintered Alumina Ceramics (알루미나 세라믹 가소결재의 피삭성 -다이아몬드 및 CBN공구의 절삭 성능-)

  • 김성청
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 1996.03a
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    • pp.41-46
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    • 1996
  • In this study, unsintered and pre-sintered low purity alumina ceramics were machined with various tools to clarify the machinability, optimum tool materials and optimum cutting conditions. The main conclusions obtained were as follows. (1)In the case of dry cutting, the sintered diamond and natural diamond tools exhibit better performance in machining of the ceramic pre-sintered at lower temperature, and the tool lives of both tools in machining the ceramics pre-sintered at high temperature becomes extremely short. (2)The performance of CBN tool becomes better in dry machining of the ceramics pre-sintered at higher temperature. (3)When the pre-sintered ceramics were wet machined with sintered diamond, the tool life becomes considerably long, and higher cutting speed can be used than in the case of the CBN and ceramic tools, the tool lives becomes shorter at wet cutting than at dry cutting, especially exhibiting extremely short tool life in wet cutting with ceramic tool.

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Microstructure and Electrical Properties of $RuO_2$ System Thick Film Resistors ($RuO_2$계 후막저항체의 미세구조와 전기적성질)

  • 구본급;김호기
    • Journal of the Korean Ceramic Society
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    • v.27 no.3
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    • pp.337-344
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    • 1990
  • As a function of sintering temperature and time, the electrical properties of ruthenium based thick film resistors were investigated with microstructure. The variatio of resistivity and TCR(temperature coefficient of resistance)trends of sintered speciman at various sintering temperature were different low resistivity paste(Du Pont 1721) from high one(Du Pont 1741). These phenomena are deeply relative to microstructure of sintered film. With increasing the sintering temperature for 1721 system, the electrical sheet resistivity decreased, but again gradually increased above 80$0^{\circ}C$. And TCR trends in 1721 system are all positive. On the other hand the electrical sheet resistivity of 1741 resistor system decreased with sintering temperature. And TCR trends variable according to sintering temperature. TCR of speciman sintered at $700^{\circ}C$ was negative value, and TCR of 80$0^{\circ}C$ sintered speciman coexisted negative and positive value. But in case of speciman sintered at 90$0^{\circ}C$, TCR was positive value. As results of this fact, it was well known that the charge carrier contributied to electrical conduction in 1741 resistor system varied with sintering temperature.

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Ultrasonic pulse velocity analysis for high- temperature mechanical properties of high strength concrete replacing non-sintered hwangto (비소성 황토를 치환한 고강도 콘크리트의 고온 역학적 특성 평가를 위한 초음파 속도 분석)

  • Hong, Kil-Dong;Lim, Gguk-Jeong;Jang, Kil-San
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2023.11a
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    • pp.273-274
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    • 2023
  • In this study, ultrasonic pulse velocity was analyzed to evaluate the high-temperature mechanical properties of concrete mixed with non-sintered hwangto. The W/B of the specimens was set at 0.41, the percentage of non-sintered hwangto admixture was set at two levels of 15,30%. The target temperature of the specimen is set to 6 levels of 20, 100, 200, 300, 500, 700 ℃, and the heating rate is set to 1℃/min. The result showed that the amount of non-sintered hwangto incorporated into the concrete tends to results in lower compressive strength. Ultrasonic pulse velocity showed similar trends, but differed in some areas.

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저순도 알루미나 세라믹 가소결재의 피삭성

  • 이재우
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1995.04b
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    • pp.33-38
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    • 1995
  • In this study, unsistered, pre-sintered and sintered low purity alumina ceramics were machined with various tools to clarify the machniability, the optimum tool materials and the optimum tool materials and the optimum cutting conditions. The maon conclusions obtained were as follows. (1) Machined withalloy steel tool, the machinabilty of te pre-sintered ceramics becomes better with the decrease of pre-sintering temperature, but that of unsintered ceramics(white body) was extremely poor. (2) In the case of carbide tool K01, the tool life in machining white body was the longest, and the machinabilty of pre-sintered ceramics becomes poorer with the increase of the pre-sintering temperature. (3) In the case of ceramic tool, the 10000-1100 .deg. C pre-sintered ceramics showed te best machinability within a certain cutting speed range. So far as dry machining, the above combination and conditions showed the highest productivity. (4) When the pre-sintered ceramics were wet machined withsintered diamond tool, the tool life becomes extremelylong, and higher cutting speed can be can be used than in the case offull-sintered ceramics. The productivity of wet cutting is much higher than that ofdry cutting.

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Experimental Study on Boiling Heat Transfer of the Tubes with Sintered Metal Surface for Freon-11 (냉매의 소결금속관 표면에서의 비등 열전달에 관한 실험적 연구)

  • Park C. J.;Mun B. S.;seo J. Y.
    • The Magazine of the Society of Air-Conditioning and Refrigerating Engineers of Korea
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    • v.10 no.3
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    • pp.220-227
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    • 1981
  • The purpose of this paper is to investigate the potential ability of sintered metal tube to promote heat transfer. In the experiment for Freon - 11, the boiling heat transfer on the sintered metal tube of bronze element is investigated and compared with that of the bronze tube (bare tube) atmospheric pressure. The experimental results are obtained as follows : 1) For sintered metal tubes of bronze element with particle diameters which ranges from $79({\mu})\;to\;461({\mu})$ and bare tube, boiling characteristic curves are expressed as : a) Sintered metal tube $$q{\propto}{\Delta}T^{1.05\~1.373}$$ b) Brae tube $$q{\propto}{\Delta}T^{3.096}$$ 2) Compared with that of the bare tube at low temperature difference$({\Delta}T_{sat})$, boiling heat transfer coefficient of the sintered bronze tube are relatively high. 3) There is tendency that curves of boiling heat transfer coefficients of sintered ·bronze tube and bare tube approach each other at rather high temperature difference. It is due to the increasing rate of the former heat transfer coefficient along with temperature difference is smaller than that of the latter. 4) Referring to particle diameter, optimum condition, i. e. , maximum heat transfer coefficient is found to be at approximately 2 mm thickness of sintered layer with $D_p=150({\mu})$.

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Environmental Properties of ZnO Varistors with Variation of Sintering Temperature (소결온도에 따른 ZnO 바리스터의 내환경 특성)

  • Lee, Sung-Gap;Cho, Hyun-Moo;Lee, Jong-Deok;Park, Sang-Man
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.18 no.12
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    • pp.1111-1116
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    • 2005
  • ZnO varistor ceramics added a glass-frit 0.03 $wt\%$ were fabricated with variation of sintering temperature. The sintering temperature and time were $1125^{\circ}C\~1200^{\circ}C$ and 2 h. The average grain sizes increased and the varistor voltage decreased with increasing the sintering temperature. The values of the specimen sintered at $1200^{\circ}C$ were $23.7\;{\mu}m$ and 329 V, respectively. The leakage current of all specimens was less than $1\;{\mu}A$ at DC $82\%$ of varistor voltage. The clamping voltage ratio of the specimen sintered at $1175^{\circ}C$ was 1.37. The endurance of surge current and the deviation of varistor voltage of the specimen sintered at $1175^{\circ}C$ were 6400 $A/cm^2$ and ${\Delta}-2.81\%$, respectively. After the High Temperature Load Test(HTLT) at $85^{\circ}C$ for 1000 h, the specimen sintered at $1175^{\circ}C$ showed the lowest deviation of varistor voltage of ${\Delta}-1.92\%$.

Effect of Calcining Temperature on Sintering Characteristics of PZT (하소온도가 PZT의 소결특성에 미치는 영향)

  • 정수태;이우일;조상희
    • Journal of the Korean Ceramic Society
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    • v.22 no.1
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    • pp.40-46
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    • 1985
  • The effect of calcining temperature ranged from $700^{\circ}C$ to 110$0^{\circ}C$ on sintering characteristics of morphotropic $Pb(Zr_{0.53}Ti_{0.47})O_3 doped with $Nb_2O_5$ has been investigated. The ratio of sintered grain size to calcined grain size decreased as the calcining temperature increased. The hardness as well as the sintered density of the samples reached a maximum at about 90$0^{\circ}C$. The X-ray diffraction pattern of the sintered sample showed both tetragonal and rhombohedral phases. The tetragonal phases intensity increased with the calcining temperature going through a maximum at about 90$0^{\circ}C$ while the rhombohedral phase intensity remained uneffected. The both intensity were about the same at 90$0^{\circ}C$ The dielectric constant of the sintered samples reached a maximum um while the dielectric dissipation factor showed a minimum at the calcining temperature of about 100$0^{\circ}C$.

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Thermoelectric Properties of PbTe Sintered Body Fabricated by Mechanical Alloying Process (기계적합금화 공정에 의해 제조된 PbTe 소결체의 열전특성)

  • 이길근;정해용;이병우
    • Journal of Powder Materials
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    • v.8 no.2
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    • pp.110-116
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    • 2001
  • Abstract To investigate the effect of mechanical alloying process to thermoelectric properties of PbTe sintered body, Pb-Te mixed powder with Pb : Te : 1 : 1 composition was mechanically alloyed using tumbler-ball mill. Thermoelectric properties of the sintered body were evaluated by measuring of the Seebeck coefficient and specific electric resistivity from the room temperature to 50$0^{\circ}C$. Sintered body of only mechanically alloyed PbTe powder showed p-type behavior at the room temperature, and occurred type transition from p-type to n-type at about 30$0^{\circ}C$. PbTe sintered body which was fabricated using heat treated powder in $H_2$ atmosphere after mechanical alloying showed stable n-type behavior under 50$0^{\circ}C$. N-type PbTe sintered body fabricated by mechanical alloying process had 4 times higher power factor than that fabricated by the melt-crushing process. Application of a mechanical alloying process to fabricate of n-type PbTe thermoelectric material seemed to be useful to increase the power factor of PbTe sintered body.

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Austenite Stability of Sintered Fe-based Alloy (철계 소결합금의 오스테나이트 안정성)

  • Choi, Seunggyu;Seo, Namhyuk;Jun, Junhyub;Son, Seung Bae;Lee, Seok-Jae
    • Journal of Powder Materials
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    • v.27 no.5
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    • pp.414-419
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    • 2020
  • In the present study, we investigated the austenite stability of a sintered Fe-based nanocrystalline alloy. The volume fraction of austenite was measured based on the X-ray diffraction data of sintered Fe-based nanocrystalline alloys, which were prepared by high-energy ball milling and spark plasma sintering. The sintered alloy samples showed a higher volume fraction of austenite at room temperature as compared to the equilibrium volume fraction of austenite obtained using thermodynamic calculations, which resulted from the nanosized crystalline structure of the sintered alloy. It was proved that the austenite stability of the sintered Fe-based alloy increased with a rise in the amount of austenite stabilizing elements such as Mn, Ni, and C; however, it increased more effectively with a decrease in the actual grain size. Furthermore, we proposed a new equation to predict the martensite starting temperature for sintered Fe-based alloys.

Low Temperature Sintering of Alumina by Boehmite Sol-Gel Method II. Microstructure and mechanical Properties (보헤마이트 졸겔법에 의한 알루미나 세라믹스 저온소결 II.미세구조 및 기계적 특성)

  • 이형민;이홍림
    • Journal of the Korean Ceramic Society
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    • v.35 no.1
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    • pp.66-78
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    • 1998
  • the microstructure and mechanical properties of seeded and ball-milled dry gels prepared by boehmite sol-gel method were discussed. The densification of seeded gels was improved with increasing seed content namely the number of seed The number of seed was 1.09, 3.35, 5.72${\times}$1012/cm3 boehmite when seeded with 1, 3, 5wt% respectively The ball milled gel contained about 0.5wt% seed and the number of seed was 4.72${\times}$1012/cm3 boehmite. The sintered density of 5wt% seeded gel was below 80% when sintered at 1300$^{\circ}C$ for 1h. On the other hand that of ball milled gel was very improved and reached to 97% In the case of 3wt% seeded gels the density over 97% was attained when sintered at 1500$^{\circ}C$for 1h. and the grain of the sintered body was several micrometers in size. However the sintered body of ball milled gel showed grain size of submicrometer when sintered at 1300$^{\circ}C$ for 1h. And this specimen showed highest harness value of 1900kg/mm2 The fracture toughness increased with increasing sintering temperature. The sintered body of ball milled gel showed the largest grain size and the highest fracture toughness without regard to sint-ering temperature.

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