• Title/Summary/Keyword: reduction synthesis

Search Result 1,064, Processing Time 0.035 seconds

A Model Reduction Method for Effective Analysis of Structures (구조물의 효율적인 해석을 위한 모델 축소기법 연구)

  • Park, Young-Chang;Hwang, Jai-Hyuk
    • Journal of the Korean Society for Aviation and Aeronautics
    • /
    • v.14 no.1
    • /
    • pp.28-35
    • /
    • 2006
  • Substructure coupling or component mode synthesis may be employed in the solution of dynamic problems for large, flexible structures. The model is partitioned into several subdomains, and a generalized Craig-Bampton representation is derived. In this paper the mode sets (normal modes, constraint modes) is employed for model reduction. A generalized model reduction procedure is described. Vaious reduction methods that use constraint modes is described in detail. As examples, a flexible structure and a 10 DOF damped system are analyzed. Comparison with a conventional reduction method based on a complete model is made via eigenpair and dynamic responses.

  • PDF

Selective Reduction of Organic Compounds with Al-Methanesulfonyldiisobutylalane

  • Cha, Jin-Soon;Noh, Min-Yeong
    • Bulletin of the Korean Chemical Society
    • /
    • v.31 no.4
    • /
    • pp.840-844
    • /
    • 2010
  • The new MPV type reagent, Al-methanesulfonyldiisobutylalane ($DIBAO_3SCH_3$), has been prepared and its reducing characteristics in the reduction of selected organic compounds containing representative functional groups have been examined in order to find out a new reducing system with high selectivity in organic synthesis. In general, the reagent is extremely mild, showing only reactivity toward aldehydes, ketones and epoxides. The reagent exhibits a unique reducing applicability in organic synthesis. Thus, the reagent can achieve a clean 1,2-reduction of $\alpha,\beta$-unsaturated aldehydes and ketones to produce the corresponding allylic alcohols in 100% purity. In addition, the reagent shows an excellent regioselectivity in the ring-opening reaction of epoxides. Finally, $DIBAO_3SCH_3$ shows a high stereoselectivity in the reduction of cyclic ketones to produce the thermodynamically more stable epimers exclusively.

A Study on Model Reduction for Effective Analysis of Structure (구조물의 효율적인 해석을 위한 모델 축소기법 연구)

  • 박영창;황재혁;오화석
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
    • /
    • 2001.11b
    • /
    • pp.1370-1375
    • /
    • 2001
  • Substructure coupling or component mode synthesis may be employed in the solution of dynamic problems for structure. The model is partitioned into several subdomains. and a generalized Craig-Bampton representation is derived. In this paper the mode sets(normal modes. constraint modes) have been employed for model reduction. A generalized model reduction procedure has been described. Those reduction methods which adapt constraint modes have been described in detail. As examples. a flexible structure and a 10 DOF damped system are analyzed. Comparison with a conventional reduction method based on a complete model has been made via eigenpairs and dynamic responses.

  • PDF

A Model Reduction and PID Controller Design Via Frequency Transfer Function Synthesis (주파수 전달함수 합성법에 의한 모델축소 및 PID 제어기 설계)

  • Kim, Ju-Sik;Kwang, Myung-Shin;Kim, Jong-Gun;Jeon, Byeong-Seok;Jeong, Su-Hyun
    • The Transactions of the Korean Institute of Electrical Engineers P
    • /
    • v.54 no.1
    • /
    • pp.34-40
    • /
    • 2005
  • This paper presents a frequency transfer function synthesis for simplifying a high-order model with time delay to a low-order model. A model reduction is based on minimizing the error function weighted by the numerator polynomial of reduced systems. The proposed method provides better low frequency fit and a computer aided algorithm. And in this paper, we present a design method of PID controller for achieving the desired specifications via the reduced model. The proposed method identifies the parameter vector of PID controller from a linear system that develops from rearranging the two dimensional input matrices and output vectors obtained from the frequency bounds.

A New Low Power High Level Synthesis for DSP (DSP를 위한 새로운 저전력 상위 레벨 합성)

  • 한태희;김영숙;인치호;김희석
    • Proceedings of the IEEK Conference
    • /
    • 2002.06b
    • /
    • pp.101-104
    • /
    • 2002
  • This paper propose that is algorithm of power dissipation reduction in the high level synthesis design for DSP(Digital Signal Processor), as the portable terminal system recently demand high power dissipation. This paper obtain effect of power dissipation reduction and switching activity that increase correlation of operands as input data of function unit. The algorithm search loop or repeatedly data to the input operands of function unit. That can be reduce the power dissipation using the new low power high level synthesis algorithm. In this Paper, scheduling operation search same nodes from input DFG(Data Flow Graph) with correlation coefficient of first input node and among nodes. Function units consist a multiplier, an adder and a register. The power estimation method is added switching activity for each bits of nodes. The power estimation have good efficient using proposed algorithm. This paper result obtain more Power reduction of fifty percents after using a new low power algorithm in a function unit as multiplier.

  • PDF

Diastereoselective Reduction of 2,3-Dioxo-4-carboxy-5-substituted Pyrrolidines Using NaBH4/AcOH and Heterogenous Hydrogenation Reactions

  • Mohammat, Mohd Fazli;Mansor, Nurul Shulehaf;Shaameri, Zurina;Hamzah, Ahmad Sazali
    • Journal of the Korean Chemical Society
    • /
    • v.59 no.1
    • /
    • pp.31-35
    • /
    • 2015
  • Diastereoselective reduction of 2,3-dioxo-4-carboxy-5-(substituted)pyrrolidine 1 by $NaBH_4/AcOH$ and heterogenous hydrogenation were reported. Stereochemical assignment and diastereomeric ratios of the products were determined using $^1H$ NMR and single crystal X-ray analyses. The steric factors of the C-5 substituents of the pyrrolidinone was shown to have an interesting influence on both the yield and diastereoselectivity of the reduced product.

Synthesis of Aluminum Nitride Nanopowders by Carbothermal Reduction of Aluminum Oxide and Subsequent In-situ Nitridization (산화알루미늄 분말의 탄소열환원 및 직접 질화반응을 통한 질화알루미늄 나노분말의 합성)

  • Seo, Kyung-Won;Lee, Seong-Yong;Park, Jong-Ku;Kim, Sung-Hyun
    • Journal of Powder Materials
    • /
    • v.13 no.6 s.59
    • /
    • pp.432-438
    • /
    • 2006
  • Aluminum nitride (AlN) nanopowders with low degree of agglomeration and uniform particle size were synthesized by carbothermal reduction of alumina and subsequent direct nitridization. Boehmite powder was homogeneously admixed with carbon black nanopowders by ball milling. The powder mixture was treated under ammonia atmosphere to synthesize AlN powder at lour temperature. The effect of process variables such as boehmite/carbon black powder ratio, reaction temperature and reaction time on the synthesis of AlN nanopowder was investigated.

Polarographic Studies on Electrochemical Reduction of p-Nitrosalicylic Acid and the Electrochemical Synthesis of p-Aminosalicylic Acid (p-nitrosalicylic acid의 전해환원에 의한 PAS의 합성과 Polarograph연구)

  • 김준용
    • YAKHAK HOEJI
    • /
    • v.17 no.4
    • /
    • pp.217-222
    • /
    • 1973
  • Although a considerable amount of work has ben carried out, on the reduction of p-nitrosalicylic acid with Pb, Ni, Cu and Hg cathodes, published results do not proceeded the synthesis of p-aminosalicylic acid. In order to get the reduction potential and the mechanism of reduction, therefore, the electrode reactions occurring during "polarographic reduction" have been studied more fully. As a result, the author found that p-aminosalicylic acid (PAS) can be only produced in a HCl-ethanol solution using Sn cathode with the current density of 4.0A/$dm^{2}$, at 40-$50^{\circ}$.

  • PDF

Synthesis of Nano Metal Powder by Electrochemical Reduction of Iron Oxides

  • Seong, Ki-Hun;Lee, Jai-Sung
    • Proceedings of the Korean Powder Metallurgy Institute Conference
    • /
    • 2006.09a
    • /
    • pp.482-483
    • /
    • 2006
  • Synthesis of iron nanopowder by room-temperature electrochemical reduction process of ${\alpha}-Fe_2O_3$ nanopowder was investigated in terms of phase evolution and microstructure. As process variables, reduction time and applied voltage were changed in the range of $1{\sim}20$ h and $30{\sim}40$ V, respectively. From XRD analyses, it was found that volume of Fe phase increased with increasing reduction time and applied voltage, respectively. The crystallite size of Fe phase in all powder samples was less than 30 nm, implying that particle growth was inhibited by the reaction at room temperature. Based on the distinct equilibrium shape of crystalline particle, phase composition of nanoparticles was identified by TEM observation.

  • PDF