• 한국마린엔지니어링학회:학술대회논문집
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• 한국마린엔지니어링학회 2005년도 전기학술대회논문집
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• pp.777-782
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• 2005

The importance of emergency diesel generator(EDG) has confirmed in the safety evaluation of PSA and the study on aging of EDG has been progressed actively as a part of the project of nuclear plant aging research in the U.S.A. As the result, the concept of performance evaluation is being transferred from statistical analysis of test results to performance monitoring and trending analysis for monitoring of aging and reliability. Recently, the study related aging characteristic and reliability for EDGS has begun in Korea. Consequently, the efficient performance monitoring based systematic and integrated monitoring and failure diagnostic technology is necessary. In the research, the knowledge basis of monitoring parameters for EDGS is constructed, and the prototype monitoring and diagnosis system applicable to Pielstick EDG is developed.

• 한국재료학회지
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• 제27권2호
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• pp.82-88
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• 2017

Ink-jet printing techniques with ceramic ink, which contains ceramic pigments as colorant, are in increasingly use in the ceramic industry. Generally, ceramic pigments that are produced by conventional method show diameters of several micrometers; these micrometer sized particles in the ink-jet printing process can cause undesirable behavior such as print head nozzle clogging. To prevent this problem, a particle size reduction process is required. In this study, CMYK (cyan, magenta, yellow, black) pigments were synthesized via solid state method. Each pigment particle was milled to submicron size by an attrition mill. The effects of micronizing on the morphology, mechanical property, crystal structure and color property of the CMYK ceramic pigments were investigated by field emission scanning electron microscopy (FE-SEM), particle size analysis (PSA), X-ray diffraction (XRD) and CIE $L^{\ast}a^{\ast}b^{\ast}$.

• Journal of Magnetics
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• 제11권3호
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• pp.115-118
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• 2006

Co-ferrite nanoparticles have been synthesized by the decomposition of iron(III) acetylacetonate, $Fe(acac)_3$ and Co acetylacetonate, $Co(acac)_2$ in benzyl/phenyl ether in the presence of oleic acid and oleyl amine at the refluxingtemperature of $295^{\circ}C$/$265^{\circ}C$ for 30 min. before cooling to room temperature. Particle diameter detected by PSA can be turned from 4 nm to 20 nm by seed-mediated growth and reaction conditions. Structural and magneticcharacterization of Co-ferrite were measured by use of HRTEM, SAED (selected area electron diffraction), XRD and SQUID. The as-synthesized Co-ferrite nanoparticles have a cubic spinel structure and coercivity of 20 nm $CoFe_{2}O_{4} nanoparticles reached 1 kOe at room temperature and 18 kOe at 10 K.

• 접착 및 계면
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• 제14권2호
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• pp.88-94
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• 2013

최근에 날로 강화되는 환경 규제, 그리고 수요자의 필요에 의해 수용성 그리고 알칼리 가용성 점착제에 대한 많은 제품 개발이 이루어지고 있다. 본 연구실에서는 그러한 특성을 정량적으로 정확하게 측정할 수 있는 시험법을 개발하여 KS 및 ISO 시험법으로 제정하였다. 본 연구에서는 이 시험법을 이용하여 수용성과 알칼리 가용성 점착제의 시간에 따른 수용화와 알칼리 가용화 정도를 측정하였고 측정결과 분석을 통해 본 시험법이 안정된 수용성 및 알칼리 가용화 데이터를 생성하고 있음을 보여주었다.

• 한국재료학회지
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• 제30권5호
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• pp.252-261
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• 2020

We prepare ZnO nanoparticles by environmentally friendly synthesis using Cyathea nilgiriensis leaf extract. Various phytochemical constituents are identified through the assessment of ethanolic extract of plant Cyathea nilgiriensis holttum by GC-MS analysis. The formation of ZnO nanoparticles is confirmed by FT-IR, XRD, SEM-EDX, TEM, SAED and PSA analysis. TEM observation reveals that the biosynthesized ZnO nanopowder has a hexagonal structure. The calculated average crystallite size from the high intense plane of (1 0 1) is 29.11 nm. The particle size, determined by TEM analysis, is in good agreement with that obtained by XRD analysis. We confirm the formation of biomolecules in plant extract by FT-IR analysis and propose a possible formation mechanism of ZnO nanoparticles. Disc diffusion method is used for the analyses of antimicrobial activity of ZnO nanoparticles. The synthesized ZnO nanoparticles exhibit antimicrobial effect in disc diffusion experiments. The biosynthesized ZnO nanoparticles display good antibacterial performance against B. subtilis (Gram-positive bacteria) and K. pneumonia (Gram-negative bacteria). Bio-synthesized nanoparticles using green method are found to possess good antimicrobial performance.

• 대한금속재료학회지
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• 제56권11호
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• pp.829-834
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• 2018

Although magnesium-based alloys are attractive materials for hydrogen storage applications, their activation properties, hydrogenation/dehydrogenation kinetics, thermodynamic equilibrium parameters, and degradation characteristics must be improved for practical applications. Further, magnesium poses several risks, including explosion hazard, environmental pollution, insufficient formability, and industrial damage. To overcome these problems, CaO-added Mg alloys, also called Eco-Mg (environment-conscious Mg) alloys, have been developed. In this study, $Eco-MgH_x$ composites were fabricated from Mg-CaO chips by hydrogen-induced mechanical alloying in a high-pressure atmosphere. The balls-to-chips mass ratio (BCR) was varied between a low and high value. The particles obtained were characterized by X-ray diffraction (XRD), and the absorbed hydrogen was quantified by thermogravimetric analysis. The XRD results revealed that the $MgH_2$ peaks broadened for the high BCR. Further, PSA results revealed particles size were decreased from $52{\mu}m$ to $15{\mu}m$.

• 한국수소및신에너지학회논문집
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• 제32권4호
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• pp.197-204
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• 2021

Pressure swing adsorption is a purification process which can get pure hydrogen. The purification process is composed of four process: compression, adsorption, desorption and discharge. In this study the adsorption process was simulated by using the Fluent and validated with experimental results. A gas used in experiment is composed of H₂, CO₂, CH₄, and CO. Adsorption process conducted under 313 kelvin and 3 bar and bituminous-coal-based (BPL) activated carbon was used as the adsorbent. Langmuir model was applied to explain the gas adsorption. And diffusion of all the gases was controlled by micro-pore resistances. The result shows that, the most adsorbed gas was carbon dioxide, followed by methane and carbon monoxide. And carbon monoxide took the least amount of time to reach the maximum adsorption amount. The molar fraction of the off-gas became the same as the molar fraction of the gas supplied from the inlet after adsorption reached the equilibrium.

• 한국항공우주학회지
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• 제50권9호
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• pp.663-668
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• 2022

미국은 2000년대 초반부터 무기체계의 전투준비태세를 유지하면서 수명주기비용을 줄이기 위해서 TLCSM를 적용하였다. TLCSM이 적용되면서 획득단계 중심의 ILS 개념에서 전체 수명주기 동안 수명주기비용을 관리하는 개념인 IPS로 전환하였다. 또한 ILS를 개발하기 위한 LSAR은 IPS을 개발하기 위한 LPD로 전환하였다. 본 연구에서는 한국의 LSAR과 미국의 LPD를 비교 및 분석하여 LPD의 한국 도입 시 필요한 정책을 제안하였다.

• 한국수소및신에너지학회논문집
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• 제33권1호
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• pp.61-66
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• 2022

In order to introduce the hydrogen economy and increase supply, research in the field of hydrogen production is being actively conducted. Among the hydrogen production methods, the method of steam reforming from natural gas and producing it currently accounts for about 50% of the global hydrogen production. In the method of steam reforming process, hydrogen can be produced by adding a reformer to an existing natural gas supply pipe. Because of these advantages, it is evaluated as a realistic production method at present in Korea, where the city gas supply chain is well established. But there is concern in that it is highly likely to be installed in downtown areas and residential spaces. In this study, the risk of the process of steam reforming to produce hydrogen was reviewed.

• 한국분말재료학회지
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• 제30권3호
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• pp.233-241
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• 2023

In this study, we evaluated the effects of acid leaching on the properties of Cr powder synthesized using self-propagating high-temperature synthesis (SHS). Cr powder was synthesized from a mixture of Cr2O3 and magnesium (Mg) powders using the SHS Process, and the byproducts after the reaction were removed using acid leaching. The properties of the recovered Cr powder were analyzed via X-ray diffraction (XRD), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), particle size analysis (PSA), and oxygen content analysis. The results show that perfect selective leaching of Cr is challenging because of various factors such as incomplete reaction, reaction kinetics, the presence of impurities, and incompatibility between the acid and metal mixture. Therefore, this study provides essential information on the properties under acidic conditions during the production of high-quality Cr powder using a self-propagating high-temperature synthesis method.