• Title/Summary/Keyword: powder application method

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Fabrication of High Tc Superconducting Nano Powder Using Chemical Process (화학공정을 이용한 초전도 나노 분말 활성)

  • Lee, Sang-Heon;Kim, Chan-Jung;Jang, Kun-Ik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.547-548
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    • 2006
  • In order to realize the commercial application of HTSC materials, it is necessary to develop the fabrication process of high Tc oxide superconductor materials with desired shape and for practical application and high critical current density as well as good mechanical strength which can withstand high lorenz force generated at high magnetic field. Much studies have been concentrated to develop the fabrication technique for high critical current density but still there are a lot of gap which should be overcome for large scale application of HTSC materials at liquid nitrogen temperature. Recently some new fabrication techniques have been developed for YBaCuO bulk superconductor with high mechanical strength and critical current density. In this project, the establishment of fabrication condition and additive effects of second elements were examined so as to improve the related properties to the practical use of YBaCuO superconductor, and we reported the production of the YBaCuO high Tc superconductor by the pyrolysis method.

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Manufacture of Novel Composites Synthesized with Ferromagnetic and Nano-Sized Prussian Blue and D eriving Optimum Conditions (강자성체와 나노사이즈의 프러시안 블루가 합성된 새로운 형태의 복합체 제조 및 최적의 적용 조건 도출)

  • Jong Kyu Kim
    • Korean Journal of Materials Research
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    • v.33 no.4
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    • pp.151-158
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    • 2023
  • In this study, a new type of composite material combined with carbonyl iron, a relatively strong ferromagnetic material, was prepared to overcome the current application limitations of Prussian blue, which is effective in removing radioactive cesium. The surface of the prepared composite was analyzed using SEM and XRD, and it was confirmed that nano-sized Prussian Blue was synthesized on the particle surface. In order to evaluate the cesium removal ability, 0.2 g of the composite prepared for raw cesium aquatic solution at a concentration of 5 ㎍ was added and reacted, resulting in a cesium removal rate of 99.5 %. The complex follows Langmuir's adsorption model and has a maximum adsorption amount (qe) of 79.3 mg/g. The Central Composite Design (CCD) of the Response Surface Method (RSM) was used to derive the optimal application conditions of the prepared composite. The optimal application conditions achieved using Response optimization appeared at a stirring speed of pH 7, 17.6 RPM. The composite manufactured through this research is a material that overcomes the Prussian Blue limit in powder form and is considered to be excellent economically and environmentally when applied to a cesium removal site.

Inductor Design Method of DCM Interleaved PFC Circuit for 6.6-kW On-board Charger

  • You, Bong-Gi;Lee, Byoung-Kuk;Kim, Dong-Hee
    • Journal of Electrical Engineering and Technology
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    • v.12 no.6
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    • pp.2247-2255
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    • 2017
  • Because the on-board charger (OBC) is installed in electric vehicles (EVs), high power density is regarded as a key technology. Among components of the OBC, inductors occupy more than 30% of the total volume. Thus, it is important to reduce the volume and the weight of inductors while maintaining thermal stability. Discontinuous conduction mode (DCM) can satisfy these requirements; however, only a few studies have adopted the DCM operation for OBCs because of the large inductor current ripple. In this paper, a design process is proposed for application of the DCM operation to OBCs. In order to analyze the inductor losses accurately, a numerical formula for the inductor current ripple is deduced based on a detailed analysis. Two inductors are fabricated using several ferrite cores and powder cores taking into consideration the inductor size, inductor losses, and temperature rise. In order to verify the analysis and design process, experimental results are presented that show that the designed inductors satisfy the requirements of the OBCs.

One-Step Synthesis of WC and Dense WC-10 vol.%Co Hard Materials and Their Mechanical Properties (단일공정으로 WC 및 치밀한 WC-10 vol.%Co 초경재료의 제조 및 기계적 성질)

  • 김환철;오동영;정정웅;송인진
    • Journal of Powder Materials
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    • v.10 no.2
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    • pp.108-117
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    • 2003
  • WC and dense WC-10 vol%Co materials with grain size of~1${\mu}m$ were synthesized by high-frequency induction heated combustion synthesis (HFIHCS) method in one step from elemental powders of W, C and Co within several minutes. Simultaneous combustion synthesis and densification were accomplished under the combined effects of an induced current and mechanical pressure. In the absence of cobalt additive, WC can be formed, but its relative density was low (about 73%) under simultaneous application of a 60 MPa pressure and the induced current. However, in the presence of 10 vol.%Co, the relative density increased to 99% under the same experimental condition. The percentages of the total shrinkage occurring before and during the synthesis reaction of WC-10 vol.%Co were 5% and 51%, respectively. The fracture toughness and hardness values of WC-10 vol.%Co were 10 MPa . m$^{1/2}$ and 1840 kg/$mm^2$, respectively.

Feasibility Test for Mechanical Property Characterization of BaTiO3 Ceramics for MLCC Application Using Nanoindentation (나노인덴테이션을 이용한 MLCC용 BaTiO3 세라믹스의 기계적 물성평가)

  • Ryu, Sung-Soo;Kim, Seong-Won;Kim, Hyeong-Jun;Kim, Hyung-Tae
    • Journal of Powder Materials
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    • v.16 no.1
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    • pp.37-42
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    • 2009
  • In this study, the feasible test for the mechanical property characterization of $BaTiO_3$ ceramics and multi-layer ceramic capacitor(MLCC) was performed with nanoindentation technique. In case of $BaTiO_3$ ceramics, hardness and elastic modulus are dependent on the densification of specimen showing the highest hardness and elastic modulus values of 12.3 GPa and 155 GPa, respectively at $1260^{\circ}C$. In case of MLCC chip, hardness of dielectric layer was lower than that of margin region. The nanoindentation method could be useful tool for the measurement of mechanical property within $BaTiO_3$ dielectric layer of very thin thickness in high capacitance MLCC.

Photocatalytic and Adsorption Properties of WO3 Nanorods Prepared by Hydrothermal Synthesis (수열합성법으로 제조된 나노막대 구조 WO3의 광촉매 효과 및 염료 흡착 반응)

  • Yu, Su-Yeol;Nam, Chunghee
    • Journal of Powder Materials
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    • v.24 no.6
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    • pp.483-488
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    • 2017
  • Transition-metal oxide semiconductors have various band gaps. Therefore, many studies have been conducted in various application fields. Among these, methods for the adsorption of organic dyes and utilization of photocatalytic properties have been developed using various metal oxides. In this study, the adsorption and photocatalytic effects of $WO_3$ nanomaterials prepared by hydrothermal synthesis are investigated, with citric acid added in the hydrothermal process as a structure-directing agent. The nanostructures of $WO_3$ are studied using transmission electron microscopy and scanning electron microscopy images. The crystal structure is investigated using X-ray diffraction patterns, and the changes in the dye concentrations adsorbed on $WO_3$ nanorods are measured with a UV-visible absorption spectrophotometer based on Beer-Lambert's law. The methylene blue (MB) dye solution is subjected to acid or base conditions to monitor the change in the maximum adsorption amount in relation to the pH. The maximum adsorption capacity is observed at pH 3. In addition to the dye adsorption, UV irradiation is carried out to investigate the decomposition of the MB dye as a result of photocatalytic effects. Significant photocatalytic properties are observed and compared with the adsorption effects for dye removal.

Fabrication of Nanostructured $5Cu_{0.6}Fe_{0.4}-Al_2O_3$ Composite by Pulsed Current Activated Sintering from Mechanically Synthesized Powder (기계적으로 합성한 분말로부터 펄스전류 활성 소결에 의한 나노구조 $5Cu_{0.6}Fe_{0.4}-Al_2O_3$ 복합재료제조)

  • Park, Na-Ra;Song, Jun-Young;Nam, Kee-Seok;Shon, In-Jin
    • Journal of the Korean Society for Heat Treatment
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    • v.22 no.3
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    • pp.149-154
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    • 2009
  • Dense $5Cu_{0.6}Fe_{0.4}-Al_2O_3$ composite was consolidated from mechanically synthesized powders by pulsed current activated sintering method within 1 min. $5Cu_{0.6}Fe_{0.4}-Al_2O_3$ powder was synthesized from 3CuO and 2FeAI using the high energy ball milling. Dense $5Cu_{0.6}Fe_{0.4}-Al_2O_3$ with relative density of up to 95% was produced under simultaneous application of a 80 MPa pressure and the pulsed current. Mechanical properties and grain size of the composite were investigated.

Effect of Alumina Nanooxide Application on Nitrendipine Manufacturing Process (알루미나 나노산화물이 Nitrendipine 제조 공정에 미치는 영향)

  • Chae, E.J.;Uhm, Y.R.;Han, B.S.;Rhee, C.K.;Park, S.E.
    • Journal of Powder Materials
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    • v.14 no.2 s.61
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    • pp.127-131
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    • 2007
  • The alumina nano powders synthesized by levitational gas condensation (LGC) method were applied to catalyst in manufacturing process of Hanzsch reaction for Nitrendipine. The L-tartaric acid on the surface is carried out with participation of carbonyl fragments, O-H, C-H bonds which affects stereo selectivity, yield on the reagents positively. From the analysis of the IR-spectroscopy, the carbonyl fragments, O-H, and C-H bond were created by the catalytic reaction. From the analysis of the rR-spectroscopy, the carbonyl fragments, O-H, and C-H bond were created by the catalytic reaction. The newly created bonds made a chiral center on the final product.

Recovery and Synthesis of Silver Nanoparticles from Leaching Solution of LTCC Electrode By-Products (LTCC 전극공정부산물 침출 용액으로부터 은 회수 및 은 나노입자 제조)

  • Yoo, Juyeon;Kang, Yubin;Park, Jinju;Ryu, Hojin;Yoon, Jin-Ho;Lee, Kun-Jae
    • Journal of Powder Materials
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    • v.24 no.4
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    • pp.315-320
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    • 2017
  • There has been much interest in recycling electronic wastes in order to mitigate environmental problems and to recover the large amount of constituent metals. Silver recovery from electronic waste is extensively studied because of environmental and economic benefits and the use of silver in fabricating nanodevices. Hydrometallurgical processing is often used for silver recovery because it has the advantages of low cost and ease of control. Research on synthesis recovered silver into nanoparticles is needed for application to transistors and solar cells. In this study, silver is selectively recovered from the by-product of electrodes. Silver precursors are prepared using the dissolution characteristics of the leaching solution. In the liquid reduction process, silver nanoparticles are synthesized under various surfactant conditions and then analyzed. The purity of the recovered silver is 99.24%, and the average particle size of the silver nanoparticles is 68 nm.

Phenolic Compounds Production, Enhancement and Its Antioxidant Activity of Blue Berry Powder with Bacillus subtilis Light Mediated Fermentation Compounds

  • Elumalai, Punniyakotti;Lim, Jeong-Muk;Mohan, Harshavardhan;Lee, Jeong-Ho;Oh, Byung-Taek
    • Proceedings of the Plant Resources Society of Korea Conference
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    • 2018.04a
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    • pp.66-66
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    • 2018
  • Light fermentation has been conducted under different light conditions such as normal dark light, white light, and light emitting diodes (LEDs) various color (blue, green, red, white on blueberry powder with fermenting bacteria Bacillus subtilis (B2). The bacteria B2 was isolated and identified by 16S rRNA sequencing method. RYRP biologically converted to secondary metabolites through light fermentation in the presence of Bacillus subtilis, the bacteria actively involved in bioconversion process. LEDs fermentation to enhance the production of phenolic content while comparing to normal dark and white light. Among the different color LEDs, blue LEDs mediated fermentation showed higher amount of total phenolic and flavonoid content. Then blue LEDs mediated fermented compound were characterized by FTIR and GC-MS, subsequently the compound was analyzed antioxidant activity tests and the antioxidant activity exhibited higher. This is the first study to demonstrate that B. subtilis-LEDs mediated fermentation is useful for facilitating phenolic compound production and enhancing antioxidant activity, which may have greater application fermentation fields.

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