• Title/Summary/Keyword: pore size measurement

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AIN Microstructure Evalution through Hg-porosimetry (수은침투법을 이용한 AIN 미세구조연구)

  • Lee, Hae-Weon;Yoon, Bok-Gyu;Hong, Kug-Sun
    • Analytical Science and Technology
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    • v.5 no.2
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    • pp.217-222
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    • 1992
  • An attempt was made to analyze green microstructure of AIN samples prepared by slip casting and dry pressing through Hg-porosimetry. Slip cast samples with narrow pore size distribation and high packing density showed higher sinterability and homogeneous distribution of second phase(s). Hg-porosimetry is and effective way to determine pore structure if "ink bottle" phenomenon does not occur. A comparison study with porosity measurement by quantitative microscopy showed that the effectiveness of Hg-porosimetry measurement could be extended to higher sintered density as long as pores remained open.

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Adsorption Measurement of Thin Film Using a Quartz Crystal Resonator (수정진동자를 이용한 박막의 흡착 측정)

  • Kim, Byoung Chul;Park, Jung Woo;Kim, Young Han
    • Korean Chemical Engineering Research
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    • v.48 no.3
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    • pp.405-408
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    • 2010
  • A technique to measure the adsorption characteristic of surface area and pore size of a ceramic thin film is proposed, and its performance is examine. The thin film is fabricated directly on the resonator surface to measure the adsorption capacity of the film as it is, and using carbon dioxide makes the measurement easy. The results indicates that the measured surface area is satisfactory, while the pore size has some error. It is suggested that readily available carbon dioxide can be used to determine adsorption capacity of thin film at room temperature.

Measurement of Porosity by EPMA-EDS Image Processing

  • Hung, Minhui;Li, Xiangting;Xia, Jiyu;Ding, Chuanxian
    • Journal of the Korean Vacuum Society
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    • v.6 no.S1
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    • pp.66-69
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    • 1997
  • Porosity is one important characteristic feature and structural index of sprayed coatings. A method of measurement of porosity, EPMA-EDS image processing is developed in the paper. The characteristics of pores can be determined by processing of the image obtained from an electron microscope via VISTA, Not only the porosity can be presented but also the statistical result of pore size distribution. Finally it can be drawn from this paper that EPMA-EDS is a quite effective method to completely characterize the pores in plasma sprayed coatings.

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Preparation and Characterization of Activated Henequen Fiber

  • Jeong, Jong-Seon;Lee, Young-Seak;Yang, Xiao Ping;Ryu, Seung-Kon
    • Carbon letters
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    • v.10 no.4
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    • pp.339-344
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    • 2009
  • Henequen fiber was air-stabilized, carbonized, and steam-activated to obtain high surface area activated henequen fiber (AHF). Thermal behavior of henequen fibers has been studied by TGA. The structural morphology and characteristics were observed by SEM and BET surface area measurement. The yield of AHF from natural henequen was in the range of 20~25 wt%. Mesopores (2~2.5 nm) were developed on the AHF as the activation temperature was raised up to $700^{\circ}C$, and the band of mesopore size distribution moved to 15~30 nm when the activation were carried out at $900^{\circ}C$ for 30 min. The specific surface area and the total pore volume were about $1394\;m^2/g$ and $1.30\;cm^3/g$, respectively at this activation conditions.

Assesment of Human Skin Surface and Measurement of Temperature upon Applying Pump Type Cosmetics (펌프 타입 화장품 도포에 따른 피부 표면 평가와 온도 측정)

  • Cho, Wan-Goo;Park, Jee-Eun
    • Journal of the Korean Applied Science and Technology
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    • v.27 no.2
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    • pp.144-151
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    • 2010
  • Over the years, scientists have developed many test methods to evaluate the efficacy of skin care products. The needs for objective assessment have stimulated to develop instruments that are capable of reliably monitoring some parameters in evaluating skin conditions. The beauty is evaluated as a measure of smoothness of skin surface. Quantitative size measurements of skin pores is also important concept to evaluate the their conditions. The purpose of this paper is to measure the temperature change of skin and the size of pores in the skin. The pore sizes were changed by its varying skin temperature. They were decreased by applying a essence which is contained with propellant and contents.

The Study of Pore Structure in Shale Gas Reservoir Using Large-area Particle Measurement Method (대면적 입자 측정 분석법을 이용한 셰일 가스 저류층 내공극 구조 연구)

  • Park, Sun Young;Ko, Yong-kyu;Choi, Jiyoung;Lee, Junhee
    • Korean Journal of Mineralogy and Petrology
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    • v.34 no.4
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    • pp.209-218
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    • 2021
  • Studies of pore structure in shale gas reservoirs are essential to increase recovery rates, which is in the spotlight concerning unconventional resources. In this study, the distribution of pores in shale gas reservoir sample were observed using Scanning Electron Microscope Particle Analysis (SELPA), which is appropriate to analyze the distribution of particle or shape for sample in large area. A sample from the A-068 borehole drilled in the Liard Basin was analyzed; calcite is the main mineral. The pore size ranges from tens of nanometers to hundreds of micrometers and the contribution of each pore size to overall sample porosity was determined using SELPA. The distribution of pores was determined by observing the surface in the same area at magnifications of ×1000, ×3000 and ×5000. Pores less than 100 nm were observed at high magnifications and confirm that small-scale pore distribution can be analyzed and identified rapidly using SELPA. The method introduced in this study will be useful to understand pore structures in unconventional reservoirs.

Preparation and Characterization of Porous Glass in $Na_2O-B_2O_3-SiO_2$ System ; Addition Effects of $ZrO_2$ and MgO (분상법을 이용한 봉규산염계 다공질 유리의 제조 및 특성;$ZrO_2$와 MgO 첨가 영향)

  • 김영선;최세영
    • Journal of the Korean Ceramic Society
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    • v.32 no.3
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    • pp.385-393
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    • 1995
  • Akali-resistant porous glass was prepared by phase separation in Na2O-B2O3-SiO2 system containing ZrO2 and MgO. ZrO2 was added for alkali-resistance and MgO for anti-cracking during leaching. Optimal content of ZrO2 for alkali-resistance was 7wt% and devitrification by heat treatment resulted from further addition. Pore size and pore volume were decreased and specific surface area was increased with ZrO2 addition due to depression in phase separation. Addition of 3mol% MgO to mother glass containing 7wt% ZrO2 was effective for anti-crack during leaching. In this case, with phase separation at 55$0^{\circ}C$ and 5$25^{\circ}C$ for 20 hrs. crack-free porous glasses could be prepared. The relation between pore size r and heat treatment time t at 55$0^{\circ}C$ was D=25.58+18.16t. According to measurement of gas permeability, the mechanism of gas permeation was Knudsen flow. N2 and He permeability of porous glass which was prepared by heat treatment at 55$0^{\circ}C$ for 20 hrs. were 0.843$\times$10-7mol/$m^2$.s.Pa and 2.161$\times$10-7mol/$m^2$.s.Pa respectively.

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Measurement of Radon Daughters in Airborne Dust (공기부유진내(空氣浮游塵內)의 Radon 붕괴생성물(崩壞生成物)의 농도측정(濃度測定))

  • Kim, Pill-Soo;Min, Duck-Kee;Ro, Seung-Gy
    • Journal of Radiation Protection and Research
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    • v.2 no.1
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    • pp.9-16
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    • 1977
  • A simple method has been established for determining RaA, RaB and RaC concentrations in airborne dust. This is to evaluate the concentration from measurement of total alpha activities in three selected-time intervals after an air sample is taken from the membrane filter paper (mean pore size: $0.8{\mu}m$). As a preliminary trial, a time-variation of the concentrations has been determined using the single-filter method at the KAERI site (N. Lat. $37^{\circ}38'$ and E. Long $127^{\circ}15'$), Seoul, Korea. It appears that there is a large variation of the concentrations depending on the sampling time. Generally the highest value was observed in the morning that may coincide with the highest density of atmosphere in a day while the lowest value was obtained around fourteen o'clock.

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Preparation and Characterization of the Asymmetric Microporous Poly(vinylidene fluoride) (PVDF) Blend Membranes with Hydrophilic Surfaces

  • Hwang, Jeong-Eun;JeGal, Jong-Geon
    • Korean Membrane Journal
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    • v.9 no.1
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    • pp.1-11
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    • 2007
  • To prepare chemically stable asymmetric microporous membranes with a hydrophilic surface, which would be expected to have better antifouling properties, poly(vinylidene fluoride) (PVDF) blend membranes were prepared by the phase inversion process. PVDF mixture solutions in N-methylpyrrolidone (NMP) blended with several polar potential ionic polymers such as polyacrylonitrile (PAN), poly(methylmethacrylate) (PMMA) and poly(N-isopropylacrylamide) (NIPAM) were used for the formation of the PVDF blend membranes. They were then characterized with several analytical methods such as FESEM, FTIR, contact angle measurement, pore size distribution and permeability measurement. Regardless of different polar polymers blended, they all showed a finger-like structure with more hydrophilic surface than the pristine PVDF membrane. For all the PVDF blend membrane, due to the polar potential ionic polymers used, the flux of those was improved. Especially the PVDF blend membrane with NIPAM showed the highest flux among the membranes prepared. Also antifouling property of the PVDF membrane was improved by the use of the polar polymers.

Pore Characterisitics and Adsorption Performance Evaluation of Magnesium Oxide Matrix by Active Carbon Particle Size (활성탄소 입도에 따른 산화마그네슘 경화체의 공극특성과 흡착성능 평가)

  • Pyeon, Su-Jeong;Lee, Sang-Soo
    • Journal of the Korea Institute of Building Construction
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    • v.18 no.1
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    • pp.59-65
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    • 2018
  • Radon gas is a colorless, odorless, tasteless gas that occurs when uranium, a natural radioactive material in rocks and soils, collapses. 85% of the annual radiation exposure of the human body is due to natural radiation, of which 50% is radon. According to the US Environmental Protection Agency (EPA) survey, 62 out of 1,000 smokers and 7 out of 1,000 nonsmokers are exposed to lung cancer when exposed to radon gas for a long time. In order to reduce the risk of radon gas, activate carbon was used to fabricate matrix, and the pore properties and radon reduction properties were investigated. When the activate carbon was used, the radon gas concentration was drastically reduced and the graph was changed as the measurement period became longer. The pore distribution and microporous properties, which are one of the material properties of activate carbon, can be grasped.