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Influence of inorganic composition and filler particle morphology on the mechanical properties of self-adhesive resin cements

  • Marina Rodrigues Santi ;Rodrigo Barros Esteves Lins;Beatriz Ometto Sahadi;Giovanna Correa Denucci;Gabriela Soffner ;Luis Roberto Marcondes Martins
    • Restorative Dentistry and Endodontics
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    • v.47 no.3
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    • pp.32.1-32.11
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    • 2022
  • Objectives: This study aimed to evaluate the influence of inorganic composition and filler particle morphology on the mechanical properties of different self-adhesive resin cements (SARCs). Materials and Methods: Three SARCs including RelyX Unicem-2 (RUN), Maxcem Elite (MAX), and Calibra Universal (CAL) were tested. Rectangular bar-shaped specimens were prepared for flexural strength (FS) and flexural modulus (FM) and determined by a 3-point bending test. The Knoop microhardness (KHN) and top/bottom microhardness ratio (%KHN) were conducted on the top and bottom faces of disc-shaped samples. Sorption (Wsp) and solubility (Wsl) were evaluated after 24 hours of water immersion. Filler morphology was analyzed by scanning electron microscopy and X-ray energy dispersive spectroscopy (EDS). FS, FM, %KHN, Wsp, Wsl, and EDS results were submitted to 1-way analysis of variance and Tukey's post-hoc test, and KHN also to paired t-test (α = 0.05). Results: SARC-CAL presented the highest FS value, and SARC-RUN presented the highest FM. SARC-MAX and RUN showed the lowest Wsp and Wsl values. KHN values decreased from top to bottom and the SARCs did not differ statistically. Also, all resin cements presented carbon, aluminum, and silica in their composition. SARC-MAX and RUN showed irregular and splintered particles while CAL presented small and regular size particles. Conclusions: A higher mechanical strength can be achieved by a reduced spread in grit size and the filler morphology can influence the KHN, as well as photoinitiators in the composition. Wsp and Wsl can be correlated with ions diffusion of inorganic particles.

Effect of Washing Solvent and Washing Method on Flexural Strength of 3D-Printed Temporary Resin Material (세척 용액 및 세척 방법이 3D 프린팅 임시수복용 레진의 굴곡강도에 미치는 영향)

  • Hae-Bom Kim;Jae-Won Choi
    • Journal of the Korean Society of Industry Convergence
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    • v.27 no.2_2
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    • pp.389-395
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    • 2024
  • The purpose of this study was to evaluate the effect of different washing solvents and washing methods on the flexural strength of 3D printed temporary resin. A bar(25 × 2 × 2 mm) was produced with a layer thickness of 50 ㎛ using an LCD-type 3D printer and divided into 15 groups(n = 10, each) according to washing solution(IPA; 99% isopropyl alcohol, TPM; 93% Tripropylene glycol monomethylether, ETL; Ethanol, TWC; Twin 3D Cleaner, and DNC; DIO navi Cleaner) and washing method(Dip; Dip washing, Ultra; Ultrasonic washing, and Auto; Automated washing). All groups were washed for 5 minutes, and post-cured for 5 minutes using a UV LED light curing machine. The Flexural strength was measured using a three-point bending test using a universal testing machine. For statistical analysis, one-way ANOVA, Tukey HSD post hoc test, Kruskal-Wallis test and post-hoc by Bonferroni-Dunn test(𝛼=.05) were performed depending on whether the normality test was satisfied. In all washing solvents except TPM and DNC, the Dip group showed the lowest flexural strength values, while the Auto group showed the highest flexural strength values except for DNC. Additionally, the washing solution showed completely different flexural strength values depending on the washing method.

Characteristics of Flexural Behaviors for Marine Concrete Members Using High-Durable Materials (고내구성 재료를 사용한 해양 콘크리트 부재의 휨 거동 특성)

  • Yang, Eun-Ik;Kim, Myung-Yu;Park, Hae-Geun;Lee, Dong-Gun
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.12 no.6
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    • pp.249-256
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    • 2008
  • The durability of marine concrete structure is severely degraded by corrosion due to penetration and diffusion of chloride. So, many researches have been performed to improve the durability in marine concrete structure. In this study, the concrete members mixed with the mineral admixtures(SF and BFS), the epoxy-coated steel, and corrosion inhibitors are prepared, and four-point bending test of specimens are performed to investigate the flexural behaviors and the applicability for marine concrete structure. From the test results, the mineral admixtures and inhibitors are useful for safety against the initial cracking and the bending resistance in specimens. When the durable material is used in specimen, the tensile stress of reinforcing rod was less variable in same bending span length, and the durable member showed a stable behavior. And it is evaluated that the crack spacing is not larger in specimen used the durable material.

Application of HACCP System on Establishing Hygienic Standards in Pizza Specialty Restaurant - Focused on Salad Items - (HACCP제도를 활용한 피자 전문 패스트푸드 업체의 자체 위생관리기준 설정 - 샐러드를 중심으로 -)

  • Lee Bog-Hieu;Kim In-Ho;Huh Kyoung-Sook;Cho Kyong-Dong
    • Journal of the Korean Home Economics Association
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    • v.41 no.10 s.188
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    • pp.101-116
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    • 2003
  • The study was conducted to establish hygienic standards of salad items for pizza restaurant located in Seoul by applying HACCP system during the summer of 2000. The study measured temperature, time, pH, Aw and microbial assessments. The hygienic conditions of the kitchen and workers were on the average(1.21, 1.0 out of 3 pts.), but some improvement should be made: separate use of trash can and leftover disposal, separate use of knives and cutting boards, habits for hand washing and wearing hygienic gloves. For salad production, all procedures were peformed under food safety danger zone ($5{\~}60^{\circ}C$). The ingredients were mostly above pH 5.0 and high in Aw($0.94{\~}0.99$). Microbial assessments for salad production revealed that TPC($1.8{\times}10^3{\~}1.0{\times}10^{10}CFU/g$) and coliforms($1.5{\times}10{\~}5.2{\times}10^5 CFU/g$) exceeded the standards by Solberg et al.(TPC: $10^6CFU/g$, coliforms: $10^3CFU/g$). S. aureus was not detected but Salmonella was found in three food items(egg, macaroni and macaroni salad). Moreover, the workers' hands contained 3.1 104 CFU/g of TPC and 4.2 102 CFU/g of S. aureus requiring further remedy since it exceeded the safety standards suggested by Harrigan and McCance (500 CFU/g of TPC per $100cm^2$ and 10 CFU/g of coliforms per $100cm^2$). According to the critical control point(CCP) decision tree analysis, vegetable receiving, vegetable holding, mixing, display on coleslaw, macaroni draining, display on macaroni salad, egg peeling & cutting, apple cutting, and display on salad bar were determined as CCPs. From the findings it would be suggested that purchase of Quality materials, short holding and display time, storing food at right temperature, using sanitary cooking utensils, and improvement of workers' food handing practices are needed to ensure the safe salad production in this specific pizza restaurant.

Study on the survival rate of fishes escaped from trawl net (트롤 탈출어류의 생존율 연구)

  • Cho, Sam-Kwang;An, Heui-Chun;Shin, Jong-Keun;Yang, Yong-Su;Park, Chang-Doo;Lee, Ju-Hee
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.42 no.2
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    • pp.69-77
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    • 2006
  • The aim of this study was to develope a fishing technology for fisheries management for improving the survival rate of young fishes escaped from trawl net. Sea experiments were carried out to investigate the survival rate of the fishes in off Geomun island and Korean southern sea. Cover-net fish cage was designed and manufactured to collect fishes escaped from COD(codend) and TED(trawl escapement device). Fish cage was installed in a shallow site where scuba diver can observe the surviving fishes after separating the cage from trawl net. Most of fishes except horse mackerel(Trachurus japonicus) and mackerel(Scomber japonicus) could escaped through TED(bar space 35mm) easier than COD(mesh size 54mm). Especially, escapement rate of redlip croaker(Pseudosciaena polyactis) escaped from TED was the highest as 73.9%. Survival rate of horse mackerel(Trachurus japonicus) escaped from TED was 85.5% at the point of 96 hours over, while the survival rate for COD showed a rapid decrease according to the time elapse as 85.0% at the point of 24 hours, 76.4% for 48 hours, 62.7% for 72 hours and 56.1% for 96 hours. Over 90% of red seabream(Pagrus major) and rock bream(Oplegnathus fasciatus) escaped from TED were survived 96 hours over and the survival rate of those fishes were excellent compared with the other fish species. All korean pomfret(Pampus echinogaster) escaped from both COD and TED were died within 48 hours. Most of redlip croaker(Pseudosciaena polyactis) were also died within 12 hours because of the weak physiological characteristics by water pressure change. Survival rate of fishes like as horse mackerel(Trachurus japonicus) having hard skin was high while it was low for the fishes like as squid(Todarodes pacificus) and hair-tail(Trichiurus lepturus) having soft skin. We could know that there were big differences in the survival rate offish species escaped from trawl net.

Performance Evaluation of the Stair Joints Constructed with Partial Precast Concrete System (프리캐스트 콘크리트 계단 접합부의 접합방식에 따른 성능평가)

  • Chang, Kug-Kwan;Lee, Eun-Jin;Jin, Byung-Chang
    • Journal of the Korea Concrete Institute
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    • v.20 no.6
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    • pp.833-840
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    • 2008
  • The time and cost can be reduced when applying partial precast concrete to the stair system in comparison to the cast-in-place or precast method. Because the performance of staircase which is used for evacuation can be largely different from connection types of precast concrete member, we tried to know structural behavior and performance evaluation according to each type of stair joints by experimental study. In the cast-in-place rigid joint, much reinforcement is needed in the end portion because much stress is concentrated in the middle portion. Also, in the pin joint which is used in the connection point, the maximum stress occurs in the middle point, so not only the amount of re-bar is increased but also the serviceability is largely decreased. The bolt type of semi-rigid joints proposed in this study had been increased strength and serviceability which is similar to the rigid joints. Also, its ductility was shown about 0.7 times in comparison to the rigid type and was about 2.8 times for the pin joint type. According to the classification of joint in Eurocode, it can be considered that it is one of the semi-rigid joints which are in the semi-rigid-full strength, and the structural behavior can be expected by using a model which applied to stiffness value decreased by 40 percent.

Comparison of flexural strength and modulus of elasticity in several resinous teeth splinting materials (여러 레진계 치아고정 재료의 굴곡강도 및 탄성계수 비교)

  • Yoo, Je-In;Kim, Soo-Yeon;Batbayar, Bayarchimeg;Kim, Jin-Woo;Park, Se-Hee;Cho, Kyung-Mo
    • Journal of Dental Rehabilitation and Applied Science
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    • v.32 no.3
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    • pp.169-175
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    • 2016
  • Purpose: Direct splinting material should have high flexural strength to withstand force during mastication and low modulus of elasticity to provide some movement while force applied for relief of stress. The purpose of this study was to compare flexural strength and modulus of elasticity of several resinous splinting materials. Materials and Methods: Four materials; Super-Bond C&B, G-FIX, G-aenial Universal Flo, FiltekTM Z350 XT; were used in this study. Fifteen rectangular bar specimens of each material were prepared. Three-point bending test were performed to determine physical properties. Maximum load at fracture was recorded and flexural strength and modulus of elasticity were calculated. One-way analysis of variance (ANOVA) and Scheffe's tests at a 0.05 level of significance were conducted on all test results. Results: Statistical analysis reveals that Super-Bond C&B had significant low mean value for flexible strength and the other three materials showed no significant difference. For modulus of elasticity, Super-Bond C&B exhibited statistically lower modulus of elasticity. G-FIX presented intermediate result, showing statistically higher modulus of elasticity than Super-Bond C&B but lower than G-aenial Universal Flo and FiltekTM Z350 XT. There was no significant difference on modulus of elasticity between G-aenial Universal Flo and FiltekTM Z350 XT. Conclusion: Using a G-FIX, the newly commercially available splinting material, which shows higher fracture resistance properties comparable to flowable and restorative composite resin and a relatively flexible nature might be a beneficial for stabilizing teeth mobility.

Implants in conjunction with removable partial denture (임플란트를 이용한 국소의치 수복)

  • Kim, Seong-Kyun;Yoo, Soo-Yeon;Park, In-Phil;Lee, Joo-Hee
    • The Journal of the Korean dental association
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    • v.49 no.2
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    • pp.77-84
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    • 2011
  • The benefits of implant supported overdenture are readily apparent for the fully edentulous patients and have been well documented, however, there is deficiency of the studies regarding the combination of implants with removable partial dentures for partially edentulous patients. The purpose of this article is to review the literature concerning implants with removable partial dentures and evaluate the evidence for this clinical approach. Through many clinical case reports and studies we have searched from a broad variety of journals, we present the six considerations needed to contemplate respecting implants with removable partial denture in partially edentulous patients. First, the connection between abutment tooth and removable partial denture has to be rigid and the link between implant and removable partial denture should be hinged. Second, a mesial rest acts better in the point of force distribution for distal extension removable partial denture and splinting between implants is also a favorable choice. Third, T bar has an advantage for implants which are used as abutments in distal extension removable partial denture. Forth, as we all known functional impression is better way to reproduce movement for distal extension removable partial denture. Fifth, indirect retainer and guiding plane on the proximal surfaces of terminal abutment teeth are important in preventing denture base lifting. Sixth, implants in conjunction with removable partial denture is superior in the esthetic and phonetic as well as cost-effective point of view. We also suggest that which place we should install implants for force distribution and which diameter and length of implants should be used. in this review article, we recommend to locate the implant near of the abutment tooth for esthetics or near of first molar position for good stress distribution. The diameter and length of implant also influence to stress distribution. When we compare to conservative partial denture, patients go for removable partial denture using implants due to convenience, better support and retention according to several studies. But it is true that we need to study more on this subject and collect long term follow up cases before we discuss on it. So it is enough to bring this subject into the surface of prosthetic treatment by this article.

Application of Linear Schedule Chart for Schedule Management of Linear Construction Project (선형시설물 공정관리 활용을 위한 선형공정표 활용 시스템 구축 방안)

  • Lee, Jaehee;Kang, Hyojeong;Kang, Leenseok
    • Korean Journal of Construction Engineering and Management
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    • v.24 no.2
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    • pp.13-23
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    • 2023
  • Unlike building construction projects, where the activity is repeatedly carried out in a limited area, civil engineering projects such as roads and railroads are carried out in a linear type in a horizontal working space over several tens of kilometers. Each activity is managed with a station number that has a unit of distance from the starting point to the end point. For this reason, since the work location information of the activity is a major management factor, the Gantt chart system that expresses only schedule information may have limitations. In this study, authors propose a method for constructing a linear schedule chart that can simultaneously express schedule information indicating the start and finish dates and location information indicating the start and end positions of each activity, and develop a system for generating a linear schedule chart. In the study, the coordinate axes of the linear schedule chart consisted of distance and date values on the X and Y axes, respectively, and each activity was expressed as a symbol that can infer the type of work to increase the visibility of the linear schedule chart compared to the simple bar chart method. The linear schedule chart generation system was reviewed for practical applicability by utilizing the actual schedule data of bridge structures in a railroad project.

A FEM study on stress distribution of tooth-supported and implant-supported overdentures retained by telescopic crowns (텔레스코픽 크라운 임플란트 지지 피개의치와 치아 지지 피개의치의 하악골내 응력분포에 관한 유한요소분석)

  • Paek, Jang-Hyun;Lee, Chang-Gyu;Kim, Tae-Hun;Kim, Min-Jung;Kim, Hyeong-Seob;Kwon, Kung-Rock;Woo, Yi-Hyung
    • The Journal of Korean Academy of Prosthodontics
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    • v.50 no.1
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    • pp.10-20
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    • 2012
  • Purpose: The purpose of this study was to investigate the stress distribution in mandibular implant-supported overdentures and tooth-supported overdentures with telescopic crowns. Materials and methods: The assumption of this study was that there were 2, 3, 4 natural teeth and implants which are located in the second premolar and canine regions in various distributed conditions. The mandible, teeth (or implants and abutments), and connectors are modeled, and analyzed with the commercial software, ANSYS Version 10.1. Stress distribution was evaluated under 150 N vertical load bilaterally on 3 experimental conditions - between canine areas, canine and $2^{nd}$ premolars, 10 mm posterior to $2^{nd}$ premolars. Results: Overall, the case of the implant group showed more stress than the case of the teeth group in stress distribution to bone. In stress distribution to superstructures of tooth and implants, there was no significant difference between TH group and IM group and the highest stress appeared in TH-IV and IM-IV. The stress caused from bar was much higher than those of implant and tooth. TH group showed less stress than IM group in stress distribution to abutment teeth and implant. Conclusion: The results shows that it is crucial to make sure that distance between impact loading point and abutment tooth does not get too far apart, and if it does, it is at best to set abutment tooth on premolar tooth region. It will be necessary to conduct more experiments on effects on implants, natural teeth and bone, in order to apply these results to a clinical treatment.