• Title/Summary/Keyword: particle size effect

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A Study on Optical Analysis of the Color Difference Caused by the Overprinting Sequence of Ink (잉크의 중첩인쇄순서에 기인하는 색차의 광학적 해석에 관한 연구)

  • 강상훈
    • Journal of the Korean Graphic Arts Communication Society
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    • v.16 no.1
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    • pp.39-53
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    • 1998
  • The extraction rate of ginger from Korean-grown ginger root with supercritical carbon dioxide was measured as a function of flow rate of supercritical carbon dioxide, particle size, temperature and pressure. the extraction rate increased as the particle size decreased due to a decrease in the diffusion path. The extraction rate were independent of flow rate of supercritical carbon dioxide in a plot of ginger oil yield versus extraction time. This indicated that the extraction process is controlled by intraparticle diffusion within a particle of ginger root. In the case of temperature and pressure effect, the experimental results showed that the extraction rate decreased with an increase in temperature and increased with an increase in pressure.

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Effect of Molar Ratio of $Fe_2O_3$ and BaO Addition on the Characteristics of Sr-Ferrite ($Fe_2O_3$몰비 및 B\ulcorner첨가가 Sr-Ferrite 특성에 미치는 영향)

  • 문기훈;심영재;조성걸
    • Journal of the Korean Ceramic Society
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    • v.34 no.5
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    • pp.453-460
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    • 1997
  • Sr-ferrite having magnetoplumbite structure is similar to Ba-ferrite in magnetic characteristics, but better magnetic characteristics for using motor application. To improve remanence magnetic flux density(Br) and coercive force(iHc), it is necessary that sintered ferrites must have high density and grain size less than 1 $\mu$m. By varying n values in SrO.nFe2O3 basic composition, calcination temperature, and BaO addition, Sr-ferrite powder and sintered specimen was prepared. The n values, calcination temperature, and BaO addition affected secondary phase formation, particle size, and particle shape. BaO addition enhanced Fe2O3 secondary phase and hexagonal shape particle. Fe2O3 phase reduced sintered density which greatly decreased Br.

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Effect of $\alpha$-Silicon Carbide Particle Size in Reaction Bonded Silicon Carbide ($\alpha$-SiC의 입도가 반응소결 탄화규소 소결체에 미치는 영향)

  • 한인섭;양준환;정헌생
    • Journal of the Korean Ceramic Society
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    • v.26 no.4
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    • pp.583-587
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    • 1989
  • Various $\alpha$-silicon carbied and colloidal graphite particles were sintered at 155$0^{\circ}C$ in vacuum atmosphere by reaction bonding sintering method, and the physical properties and microstructural analysis of specimen were investigated. With decreasing particle size, sintered density and 3-point bending strength of materials were increased and 3.2${\mu}{\textrm}{m}$ specimen showed high density and strength, 3.05g/㎤, 40kg/$\textrm{mm}^2$, respectively. The results of X-ray diffractometer and optical micrographs analysis showed that graphite and silicon melt reacted to convert to fine $\beta$-SiC particle and the body was changed to dense material.

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Absorption Study of Genistein Using Solid Lipid Microparticles and Nanoparticles: Control of Oral Bioavailability by Particle Sizes

  • Kim, Jeong Tae;Barua, Sonia;Kim, Hyeongmin;Hong, Seong-Chul;Yoo, Seung-Yup;Jeon, Hyojin;Cho, Yeongjin;Gil, Sangwon;Oh, Kyungsoo;Lee, Jaehwi
    • Biomolecules & Therapeutics
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    • v.25 no.4
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    • pp.452-459
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    • 2017
  • In this study, the effect of particle size of genistein-loaded solid lipid particulate systems on drug dissolution behavior and oral bioavailability was investigated. Genistein-loaded solid lipid microparticles and nanoparticles were prepared with glyceryl palmitostearate. Except for the particle size, other properties of genistein-loaded solid lipid microparticles and nanoparticles such as particle composition and drug loading efficiency and amount were similarly controlled to mainly evaluate the effect of different particle sizes of the solid lipid particulate systems on drug dissolution behavior and oral bioavailability. The results showed that genistein-loaded solid lipid microparticles and nanoparticles exhibited a considerably increased drug dissolution rate compared to that of genistein bulk powder and suspension. The microparticles gradually released genistein as a function of time while the nanoparticles exhibited a biphasic drug release pattern, showing an initial burst drug release, followed by a sustained release. The oral bioavailability of genistein loaded in solid lipid microparticles and nanoparticles in rats was also significantly enhanced compared to that in bulk powders and the suspension. However, the bioavailability from the microparticles increased more than that from the nanoparticles mainly because the rapid drug dissolution rate and rapid absorption of genistein because of the large surface area of the genistein-solid lipid nanoparticles cleared the drug to a greater extent than the genistein-solid lipid microparticles did. Therefore, the findings of this study suggest that controlling the particle size of solid-lipid particulate systems at a micro-scale would be a promising strategy to increase the oral bioavailability of genistein.

Effect of Performance of Aerosol Charge Neutralizers on the Measurement of Highly Charged Particles Using a SMPS (에어로졸 중화기의 성능이 고하전 입자의 크기분포 측정에 미치는 영향)

  • Ji, Jun-Ho;Bae, Swi-Nam;Hwang, Jung-Ho
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.27 no.10
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    • pp.1498-1507
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    • 2003
  • A SMPS(scanning mobility particle sizer) system measures the number size distribution of particles using electrical mobility detection technique. An aerosol charge neutralizer, which is a component of the SMPS, is a bipolar charger using a radioactive source to apply an equilibrium charge distribution to aerosols of unknown charge distribution. However, the performance of aerosol charge neutralizers is not well known, especially for highly charged particles. In this study, the effect of the particle charging characteristics of two aerosol charge neutralizers on the measurement using a SMPS system was experimentally investigated for highly charged polydisperse particles. One has radioactive source of $^{85}$ Kr (beta source, 2 mCi) and the other has $^{210}$ Po (alpha source, 0.5 mCi). The air flow rate passing through each aerosol charge neutralizer was changed from 0.3 to 3.0 L/min. The results show that the non-equilibrium character in particle charge distribution appears as the air flow rate increases although the particle number concentration is relatively low in the range of 1.5∼2x10$^{6}$ particles/㎤. The low neutralizing efficiency of the $^{85}$ Kr aerosol charge neutralizer for highly charged particles can cause to bring an artifact in the measurement using a SMPS system. However, the performance of the $^{210}$ Po aerosol charge neutralizer is insensitive to the air flow rate.

Effects of Feed Particle Size and Feed Form on Growth Performance, Nutrient Metabolizability and Intestinal Morphology in Broiler Chickens

  • Zang, J.J.;Piao, X.S.;Huang, D.S.;Wang, J.J.;Ma, X.;Ma, Yongxi
    • Asian-Australasian Journal of Animal Sciences
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    • v.22 no.1
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    • pp.107-112
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    • 2009
  • This study was conducted to investigate the effect of feed particle size and feed form on growth performance, nutrient metabolizability and intestinal morphology in broiler chickens. This experiment was a 2${\times}$2 factorial arrangement including two feed particle sizes (fine and coarse) and two feed forms (mash and pellet). A total of two hundred and eighty eight day-old male Arbor Acre broilers were used in this six week experiment. Birds were randomly allotted to four dietary treatments with six replicates per treatment and twelve birds per replicate. The results showed that pelleting diets resulted in greater ADG (p<0.01), greater ADFI (p<0.01) and lower feed to gain ratio (F/G) (p<0.05) during starter, grower and overall period. Also, pelleting improved both apparent metabolizable energy (AME) (p<0.01) and the apparent metabolizability of crude protein (p<0.05) and organic matter (p<0.05) regardless of the phase. Reduction of feed particle size enhanced AME (p<0.05) during d 19 to 21. Increased villus height (p<0.05) and crypt depth ratio (p< 0.05) within duodenum, jejunum, and ileum were observed in birds fed the pellet diet compared with those given the mash diet. In conclusion, results indicated that feed pellets might enhance performance by improving nutrient metabolizability and digestive tract development.

Condensation and coagulation of metallic species with fly ash particles in a waste incinerator (폐기물 소각시 생성되는 유해 중금속물질과 연소실내 비산재와의 응축, 응집 현상에 대한 연구)

  • Yu, Ju-Hyeon;Hwang, Jeong-Ho
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.21 no.2
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    • pp.264-274
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    • 1997
  • A numerical analysis on condensation and coagulation of the metallic species with fly ash particles pre-existing in an incinerator was performed. Waste was simplified as a mixture of methane, chlorine, and small amounts of Pb and Sn. Vapor-phase amounts of Pb- and Sn -compounds were first calculated assuming a thermodynamic equilibrium state. Then theories on vapor-to-particle conversion, vapor condensation onto the fly ash particles, and particle-particle interaction were examined and incorporated into equations of aerosol dynamics and vapor continuity. It was assumed that the particles followed a log-normal size distribution and thus a moment model was developed in order to predict the particle concentration and the particle size distribution simultaneously. Distributions of metallic vapor concentration (or vapor pressure) were also obtained. Temperature drop rate of combustion gas, fly ash concentration and its size were selected as parameters influencing the discharged amount of metallic species. In general, the coagulation between the newly formed metal particles and the fly ash particles was much greater than that between the metal particles themselves or between the fly ash particles themselves. It was also found that the amount of metallic species discharged into the atmosphere was increased due to coagulation. While most of PbO vapors produced from the combustion were eliminated due to combined effect of condensation and coagulation, the highly volatile species, PbCl$_{2}$ and SnCl$_{4}$ vapors tended to discharge into the atmosphere without experiencing either the condensation or the coagulation. For Sn vapors the tendency was between that of PbO vapors and that of PbCl$_{2}$ or SnCl$_{4}$. To restrain the discharged amount of hazardous metallic species, the coagulation should be restrained, the number concentration and the size of pre-existing fly ash particles should be increased, and the temperature drop rate of combustion gas should be kept low.

Effect of Diamond Particle Size on the Thermal Shock Property of High Pressure High Temperature Sintered Polycrystalline Diamond Compact (초 고온·고압 소결 공정으로 제조된 다결정 다이아몬드 컴팩트의 열충격 특성에 미치는 다이아몬드 입자 크기의 영향)

  • Kim, Ji-Won;Baek, Min-Seok;Park, Hee-Sub;Cho, Jin-Hyeon;Lee, Kee-Ahn
    • Journal of Powder Materials
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    • v.23 no.5
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    • pp.364-371
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    • 2016
  • This study investigates the thermal shock property of a polycrystalline diamond compact (PDC) produced by a high-pressure, high-temperature (HPHT) sintering process. Three kinds of PDCs are manufactured by the HPHT sintering process using different particle sizes of the initial diamond powders: $8-16{\mu}m$ ($D50=4.3{\mu}m$), $10-20{\mu}m$ ($D50=6.92{\mu}m$), and $12-22{\mu}m$ ($D50=8.94{\mu}m$). The microstructure observation results for the manufactured PDCs reveal that elemental Co and W are present along the interface of the diamond particles. The fractions of Co and WC in the PDC increase as the initial particle size decreases. The manufactured PDCs are subjected to thermal shock tests at two temperatures of $780^{\circ}C$ and $830^{\circ}C$. The results reveal that the PDC with a smaller particle size of diamond easily produces microscale thermal cracks. This is mainly because of the abundant presence of Co and WC phases along the diamond interface and the easy formation of Co-based (CoO, $Co_3O_4$) and W-based ($WO_2$) oxides in the PDC using smaller diamond particles. The microstructural factors for controlling the thermal shock property of PDC material are also discussed.

Understanding the Properties of Cement Mortar with Employment of Stone Dust considering Particle Size Distribution (입도분포를 고려한 석분 사용에 따른 시멘트 모르타르 성질의 변화 이해)

  • Kang, Su-Tae
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.1
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    • pp.715-723
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    • 2017
  • This study investigates the properties of a high-performance cementitious composite with partial substitution of stone dust for fine aggregate. The relationship between the properties and particle size distribution was analyzed using several analytical models. Experiments were carried out to examine the flowability, rheology, and strength of cement mortars with different stone-dust replacement ratios of 0-30 wt.%. The results showed improved flowability, lower rheological parameters (yield stress and plastic viscosity), and improved strength as the amount of stone dust increased. These results are closely related to the packing density of the solid particles in the mortar. The effect was therefore estimated by introducing an optimum particle size distribution (PSD) model for maximum packing density. The PSD with a higher amount of stone dust was closer to the optimum PSD, and the optimization was quantified using RMSE. The improvement in the PSD by the stone dust was proven to affect the flowability, strength, and plastic viscosity based on several relevant analytical models. The reduction in yield stress is related to the increase of the average particle diameter when using stone dust.

Effect of Heat Treatment on the Microstructure and Mechanical Properties for Al-Si Alloyed Powder Material by Gas Atomizing and Hot Extrusion Process (가스 분무 공정에 의해 제조된 Al-Si 합금 분말 압출재의 열처리에 의한 미세조직 및 기계적 특성 변화)

  • Nam, Ki-Young;Jin, Hyeong-Ho;Kim, Yong-Jin;Yoon, Seog-Young;Park, Yong-Ho
    • Journal of Powder Materials
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    • v.13 no.6 s.59
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    • pp.421-426
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    • 2006
  • The microstructural and mechanical properties of Al-Si alloyed powder, prepared by gas atomization fallowed by hot extrusion, were studied by optical and scanning electron microscopies, hardness and wear testing. The gas atomized Al-Si alloy powder exhibited uniformly dispersed Si particles with particle size ranging from 5 to $8{\mu}m$. The hot extruded Al-Si alloy shows the average Si particle size of less than $1{\mu}m$. After heat-treatment, the average particle size was increased from 2 to $5{\mu}m$. Also, mechanical properties of extruded Al-Si alloy powder were analyzed before and after heat-treatment. As expected from the microstructural analysis, the heat-treated samples resulted in a decrease in the hardness and wear resistance due to Si particle growth. The friction coefficient of heat-treated Al-Si alloyed powder showed higher value tough all sliding speed. This behavior would be due to abrasive wear mechanism. As sliding speed increases, friction coefficient and depth and width of wear track increase. No significant changes occurred in the wear track shape with increased sliding speed.