• Title/Summary/Keyword: p-법

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Optimum Extraction Methods of Volatile Compounds in Beef Extract Powder (쇠고기 엑기스 분말 휘발성 성분의 최적 추출방법에 관한 연구)

  • Kim Hun;Cho Woo-Jin;Jeong Eun-Jeong;Ahn Jun-Suck;Lim Chi-Won;Yoo Young-Jae;Kim Kwang-Ho;Cha Yong-Jun
    • The Korean Journal of Food And Nutrition
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    • v.17 no.4
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    • pp.412-419
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    • 2004
  • In odor to select optimum extraction methods of volatile compounds in beef extract powder(BEP) as basic data for the development of a new detection method of irradiated BEP, four extraction methods, such as solid phase microextraction with polar fiber(S-PD) and non-polar fiber(S-CD), purge and trap(P&T) and liquid liquid continuous extraction(LLCE) methods, were tested with gas chromatography/mass spectrometry method. A total of 106 volatile compounds including 22 hydrocarbons, 7 aldehydes, 6 ketones, 13 alcohols, 6 sulfur-containing compounds, 19 nitrogen-containing compounds, 6 aromatic compounds, 17 terpenes, 8 furans and 2 miscellaneous compounds were detected in BEP by four detection methods. The most compounds(62 compounds) were detected by S-PD method, followed by P&T(43), LLCE(38) and S-CD method(30). Among these methods, S-PD and P&T methods showed a complementary interrelationship to detect volatile compounds as S-PD method showed high detectabiltiy to all compound groups except hydrocarbons and ketones, which had high volatility and low molecular weight(less than RI 1200), but P&T method showed the contrary pattern to that of S-PD method. Moreover, the most of volatile compounds detected by S-CD and LLCE methods were also detectable by S-PD or/and P&T methods. Therefore, the simultaneous application of S-PD and P&T methods were selected as the optimum volatile extraction methods of BEP.

Analysis of 2-D Potential Problem with L-shape Domain by p-Convergent Boundary Element Method (p-수렴 경계요소법에 의한 L-형 영역을 갖는 2차원 포텐셜 문제 해석)

  • Woo, Kwang-Sung;Jo, Jun-Hyung
    • Journal of the Computational Structural Engineering Institute of Korea
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    • v.22 no.1
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    • pp.117-124
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    • 2009
  • The p-convergent boundary element method has been proposed to analyze two-dimensional potential problem on the basis of high order Legendre shape functions that have different property comparing with the shape functions in conventional boundary element method. The location of nodes corresponding to high order shape function are not defined along the boundary, called by nodeless node, similar to the p-convergent finite element method. As the order of shape function increases, the collocation point method is used to solve linear simultaneous equations. The collocation patterns of p-convergent boundary element method consist of non-symmetric hierarchial or symmetric non-hierarchical. As the order of shape function increases, the number of collocation point increases. The singular integral that appears in p-convergent boundary element has been calculated by special numeric quadrature technique and semi-analytical integration technique. The L-shape domain problem including singularity in the vicinity of reentrant comer is analyzed and the numerical results show that the relative error is smaller than $10^{-2}%$ range as compared with other results in literatures. In case of same condition, the symmetric p-collocation point pattern shows high accuracy of solution.

COMPARISON OF TRANSMAXILLARY AND TRANSCRANIAL PROJECTION IN THE EVALUATION OF OSTEOPHYTES Of MANDIBULAR CONDYLES (하악과두의 골증식체 평가에 있어서 transmaxillary 촬영법과 transcranial 촬영법의 비교)

  • Kim Tae Gyun;Kim Chin Soo
    • Journal of Korean Academy of Oral and Maxillofacial Radiology
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    • v.19 no.1
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    • pp.123-136
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    • 1989
  • The purpose of this study was to decide the diagnostic value of transmaxillary and transcranial projection in the evaluation of mandibular condyles. Five dry skulls with intact anatomic structure were selected for this study and the artificial osteophytes were attached to 9 different are as of the mandibular condyle. Ninety transcranial and forty-five transmaxillary radiographs were taken and then the radiographs were evaluated three times. The results were as follows; In transcranial radiographs, superocentral osteophyte was easily observed in closing state than in opening state (p<0.05). But there were no significant differences in other locations (p>0.05). The osteophytes on the medial and central portion easily observed at the transmaxillary projection than transcranial projection (p<0.05), but there was no significant difference on the lateral portion (p>0.05). The osteophytes on the superior (p<0.01) and posterior (p<0.01.) portion were easily observed at the transmaxillary projection than transcranial projection, but there was no significant difference on the anterior portion (p >0.05). The more laterally located osteophytes (p<0.01) at the transcranial projections were easily observed. The more posteriorly located osteophytes (p<0.05) at the transmaxillary projections were easily observed.

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Analysis of Patched Cylindrical Shells with Circumferential Through-Wall Cracks (원주방향 관통균열을 갖는 원통형 쉘 구조의 패치보강 해석)

  • Ahn, Jae-Seok;Kim, Young-Wook;Woo, Kwang-Sung
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.32 no.6A
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    • pp.411-418
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    • 2012
  • In this study, behavior of unpatched and patched cylindrical shells with through-wall cracks has been estimated using numerical experiments, and patching effect of them has been investigated according to various patching parameters. To show credibility of numerical models considered, two ways such as h- and p-methods have been adopted. Also, domain integral method and virtual crack extension method have been considered to calculate energy release rates based on linear elastic fracture mechanics. For examples, the unpatched cylindrical shells with circumferential cracks under remote tension have firstly been analyzed to show the validity of finite element modeling with h-method or p-method, and then the results have been compared with literature values published. Next, the sensitive analysis of patch repaired problems in terms of thickness of patch and adhesive, shear modulus of adhesive, composite material type of patch, crack length, etc. has been carried out.

Comparision of Blood Gas Analyser, pH Meter and pH Strip Methods in the Measurement of Pleural Fluid pH (흉수의 pH 측정에서 혈액가스분석기계, pH meter, pH Strip 방법의 비교)

  • Jee, Hyun-Suk;Park, Yong-Bum;Choi, Jae-Chol;Ahn, Chang-Hyuk;Yoo, Ji-Hoon;Kim, Jae-Yeol;Park, In-Won;Choi, Byoung-Whui
    • Tuberculosis and Respiratory Diseases
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    • v.48 no.5
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    • pp.773-780
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    • 2000
  • Background : pH measurement is an important test in assessing the etiology of pleurisy and in identifying complicated parapneumonic effusion. Although the blood gas analyzer is the gold standard method' for pleural pH measurement, pH meter & pH strip methods are also used for this purpose interchangably. However, the correlation among the pH data measured by the three different methods needs to be evaluated. In this study, we measured the pH of pleural fluid with the three different methods respectively and evaluated the correlation among the measured data. Methods : From August 1999 to March 2000, we measured the pleural fluid pH in 34 clinical samples with three methods-blood gas analyzer, pH meter, and pH strip. In the blood gas analyzer and pH meter methods, the temperature of pleural fluid was maintained around $0^{\circ}C$ in air-tight condition before analysis and measurement was performed within 30 minutes after collection. As for the pH strip method, the pleural fluid pH was checked in the ward immediately after tapping and in the clinical laboratory of our hospital. This part is unclear. Results : The causes of pleural effusion were tuberculosis pleurisy in 16 cases, malignant pleural effusion 5 cases, parapneumonic effusion 9 cases, empyema 3 cases, and congestive heart failure 1 case. The pH of pleural fluid (mean$\pm$SD) was 7.34$\pm$0.12 with blood gas analyser, 7.52$\pm$0.25 with pH meter, 7.37$\pm$0.16 with pH strip of immediate measurement and 6.93$\pm$0.201 with pH strip of delayed measurement. The pH measured by delayed pH strip measurement was lower than those of other methods (p<0.05). The correlation of the results between the blood gas analyzer and pH meter(p=0.002, r=0.518) and the blood gas analyzer and pH strip of immediate measurement(p<0.001, r=0.607). Conclusion : In the determination of pH of pleural fluid, pH strip method could be a simple and reliable method under immediate measurement conditions after pleural fluid tapping.

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Rates of Recovery and of Development In vitro of Follicular Oocytes Collected by Aspiration and Slicing Method in Cattle (채취 방법에 따른 소 난포란의 회수율 및 수정란의 발달율)

  • 조상래;강태영;박종식;허창기;송상현;이효종;최상용
    • Journal of Embryo Transfer
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    • v.16 no.2
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    • pp.99-106
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    • 2001
  • This study was undertaken to compare the efficiency of recovery rate and development rate of follicular oocytes collected either by aspiration or by slicing method. The follicular oocytes collected by the two methods matured in TCM199 supplemented with 10% steer serum at 39$^{\circ}C$ in a humidified atmosphere of 5% $CO_2$in air. After 22 h of culture, the oocytes were inseminated with frozen-thawed semen (2$\times$10$^{6}$ sperm/ml of final concentration) prepared with Percoll-density gradient in IVF-TALP medium for 16 h. Later, sets of 15 presumptive zygotes were transferred into 50 $\mu$L, droplets of CR1aa medium. On day 4 of the culture, embryos were transferred to TCM199 until day 9. The percentages of nuclear maturation to pre-metaphase II in the oocytes collected by aspiration are significantly (P<0.05) higher than that by slicing (83% vs. 62%, respectively). The mean number of oocytes recovered by slicing per ovary is significantly (P<0.05) higher than that by aspiration (15.1 vs. 6.7, respectively). Although the rates of cleavage and development to blastocyst of oocytes collected b)\\\\`aspiration are significantly (P<0.05) higher than that by slicing, the number of transferable embryos obtained by slicing method is significantly (P<0.05) higher than that by aspiration. From the results. we may conclude that slicing method is better than aspiration method for obtaining large number of transferable embryos per ovary.

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Analysis of Natural Convection and Radiation Heat Transfer in a Square Enclosure by Spherical Harmonics Approximation (구 조화 근사법에 의한 정사각형 밀폐공간내의 자연대류-복사열전달 해석)

  • 차상명;김창기;박희용
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.15 no.3
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    • pp.1021-1029
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    • 1991
  • 본 연구에서는 2차원 정사각형 밀폐공간내에서 흡수 및 방사하는 회기체에 대 한 자연대류-복사 열전달을 P-1 및 P-3 근사법을 이용하고 수치해석을 통하여 유동 및 열전달 특성을 연구하였고 Plank 수, 광학두께 및 벽방사율의 영향을 조사하였다. 또한 P-3 근사해와 비교함으로써 P-1 근사해의 적용범위를 고찰하였다.

The effect of Ca-P coatings of anodized implant surface on response of osteoblast-like cells in vitro (임플란트 표면의 Ca-P 코팅 방법이 MG63 골모유사세포 반응에 미치는 영향에 대한 in vitro 연구)

  • Kim, Il-Yeon;Jung, Sung-Min;Hwang, Soon-Jung;Shin, Sang-Wan
    • The Journal of Korean Academy of Prosthodontics
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    • v.47 no.4
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    • pp.376-384
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    • 2009
  • Purpose: The purpose of this study was to evaluate the response of osteoblast-like cells to Ca-P coated surface obtained via Ion beam-assisted deposition (IBAD) method and Sol-Gel process on anodized surface by cellular proliferation and differentiation. Material and methods: The surface of a commercially pure titanium (Grade IV) discs with dimension of 10mm diameter and 2 mm thickness was modified by anodic oxidation under a constant voltage of 300 V. The experimental groups were coated with Ca-P by the IBAD method and Sol-Gel process on anodized surface. The surface roughness (Ra) of specimens was measured by optical interferometer and each surface was examined by SEM. To evaluate cell response, MG63 cells were cultured and cell proliferation, ALP activity and the ability of cell differentiation were examined. Also, cell morphology was examined by SEM. The significant of each group was verified by Kruskal-Wallis Test ($\alpha$=.05). Results: The Ra value of Ca-P coated surface by IBAD method was significantly higher than Ca-P coated surface by Sol-gel process (P < .05). The level of cell proliferation and ALP activity was higher in Ca-P coated surface by IBAD method (P<.05). The expression of ALP showed higher level expression in Ca-P coated surface by IBAD method. Cells grown on Ca-P coated surface by IBAD method were uniformly distributed and developed a very close layer. Conclusion: These experiments showed better performances of Ca-P coated surface by IBAD method with respect to Ca-P coated surface by Sol-gel process. Ca-P coated surface by IBAD method appear to give rise more mature osteoblast characteristics and might result in increased bone growth and bone-implant contact.

Comparison analysis of fracture load and flexural strength of provisional restorative resins fabricated by different methods (제작방법에 따른 임시 수복용 레진의 파절강도 및 굴곡강도에 관한 연구)

  • Cho, Won-Tak;Choi, Jae-Won
    • The Journal of Korean Academy of Prosthodontics
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    • v.57 no.3
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    • pp.225-231
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    • 2019
  • Purpose: This study was undertaken to compare fracture and flexural strength of provisional restorative resins fabricated by additive manufacturing, subtractive manufacturing, and conventional direct technique. Materials and methods: Five types of provisional restorative resin made with different methods were investigated: Stereolithography apparatus (SLA) 3D printer (S3Z), two digital light processing (DLP) 3D printer (D3Z, D3P), milling method (MIL), conventional method (CON). For fracture strength test, premolar shaped specimens were prepared by each method and stored in distilled water at $37^{\circ}C$ for 24 hours. Compressive load was measured using a universal testing machine (UTM). For flexural strength test, rectangular bar specimens ($25{\times}2{\times}2mm$) were prepared by each method according to ISO 10477 and flexural strength was measured by UTM. Results: Fracture strengths of the S3Z, D3Z, and D3P groups fabricated by additive manufacturing were not significantly different from those of MIL and CON groups (P>.05/10=.005). On the other hand, the flexural strengths of S3Z, D3P, and MIL groups were significantly higher than that of CON group (P<.05), but the flexural strength of D3Z group was significantly lower than that of CON group (P<.05). Conclusion: Within the limitation of our study, provisional restorative resins made from additive manufacturing showed clinically comparable fracture and flexural strength as those made by subtractive manufacturing and conventional method.

Shape Optimal Design by P-version of Finite Element Method (p-Version 유한요소법에 의한 형상 최적화설계)

  • Kim, Haeng Joon;Woo, Kwang Sung
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.14 no.4
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    • pp.729-740
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    • 1994
  • In the shape optimal design based on h-version of FEM, the ideal mesh for the initial geometry most probably will not be suitable for the final analysis. Thus, it is necessary to remesh the geometry of the model at each stage of optimization. However, the p-version of FEM appears to be a very attractive alternative for use in shape optimization. The main advantages are as follows; firstly, the elements are not sensitive to distortion for interpolation polynomials of order $p{\geq}3$; secondly, even singular problems can be solved more efficiently with p-version than with the h-version by proper mesh design; thirdly, the initial mesh design are identical. The 2-D p-version model for shape optimization is presented on the basis of Bezier's curve fitting, gradient projection method, and integrals of Legendre polynomials. The numerical results are performed by p-version software RASNA.

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