• Title/Summary/Keyword: oxidation characterization

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Effect of Various Factors on the Brazed Joint Properties in Al Brazing Technology

  • Sharma, Ashutosh;Lee, Seung Hyun;Ban, Hyung Oh;Shin, Young Sik;Jung, Jae-Pil
    • Journal of Welding and Joining
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    • v.34 no.2
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    • pp.30-35
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    • 2016
  • Last few decades have seen a rapid increase in the fabrication and characterization of Al alloys for automobiles, heat exchangers and aerospace industries. Aluminium alloys are popular because of their high specific strength, light weight, excellent wear and high oxidation resistance. The development of aluminium alloys in these applications makes their study and research of utmost importance. Brazing is applied to the aluminium alloys for joining various aluminium parts together in most of the industrial applications. Various parameters affect the joining process of these aluminium alloys. In this article, various types of processing parameters have been discussed, and special attention has been given to the category of aluminium brazing alloys. The article reviews on the various parameters that affect the brazing property in various scientific and technological applications.

Kinetic Characterization and Molecular Modeling of $NAD(P)^+$-Dependent Succinic Semialdehyde Dehydrogenase from Bacillus subtilis as an Ortholog YneI

  • Park, Seong Ah;Park, Ye Song;Lee, Ki Seog
    • Journal of Microbiology and Biotechnology
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    • v.24 no.7
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    • pp.954-958
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    • 2014
  • Succinic semialdehyde dehydrogenase (SSADH) catalyzes the oxidation of succinic semialdehyde (SSA) into succinic acid in the final step of ${\gamma}$-aminobutyric acid degradation. Here, we characterized Bacillus subtilis SSADH (BsSSADH) regarding its cofactor discrimination and substrate inhibition. BsSSADH showed similar values of the catalytic efficiency ($k_{ca}t/K_m$) in both $NAD^+$ and $NADP^+$ as cofactors, and exhibited complete uncompetitive substrate inhibition at higher SSA concentrations. Further analyses of the sequence alignment and homology modeling indicated that the residues of catalytic and cofactor-binding sites in other SSADHs were highly conserved in BsSSADH.

Fabrication and Characterization of Optically Encoded Porous Silicon Smart Particles

  • Sohn, Honglae
    • Journal of Integrative Natural Science
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    • v.7 no.4
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    • pp.221-226
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    • 2014
  • Optically encoded porous silicon smart particles were successfully fabricated from the free-standing porous silicon thin films using ultrasono-method. DBR PSi was prepared by an electrochemical etch of heavily doped $p^{{+}{+}}$-type silicon wafer. DBR PSi was prepared by using a periodic pseudo-square wave current. The surface-modified DBR PSi was prepared by either thermal oxidation or thermal hydrosilylation. Free-standing DBR PSi films were generated by lift-off from the silicon wafer substrate using an electropolishing current. Free-standing DBR PSi films were ultrasonicated to create DBR-structured porous smart particles. Optical characteristics of porous smart particles were measured by FT-IR spectroscopy. The surface morphology of porous smart particles was determined by FE-SEM.

Silicon Carbide Coating on Graphite and Isotropic C/C Composite by Chemical Vapour Reaction

  • Manocha, L.M.;Patel, Bharat;Manocha, S.
    • Carbon letters
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    • v.8 no.2
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    • pp.91-94
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    • 2007
  • The application of Carbon and graphite based materials in unprotected environment is limited to a temperature of $450^{\circ}C$ or so because of their susceptibility to oxidation at this temperature and higher. To over come these obstacles a low cost chemical vapour reaction process (CVR) was developed to give crystalline and high purity SiC coating on graphite and isotropic C/C composite. CVR is most effective carbothermal reduction method for conversation of a few micron of carbon layer to SiC. In the CVR method, a sic conversation layer is formed by reaction between carbon and gaseous reagent silicon monoxide at high temperature. Characterization of SiC coating was carried out using SEM. The other properties studied were hardness density and conversion efficiency.

Characterization of Soot Particles Generated in Non-sooting and Sooting Normal Diffusion Flames (Sooting 및 Non-Sooting 정상 확산 화염에서 생성되는 매연 입자의 특성에 대한 연구)

  • Choi, In-Chul;Lee, Jae-Bok;Hwang, Jung-Ho
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.24 no.7
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    • pp.984-993
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    • 2000
  • Characteristics of carbon soot particles generated in diffusion flames were studied. Non-sooting and sooting normal diffusion flames using propane or ethylene as fuel were selected. In the flames, soot volume fraction was measured by a thermocouple, and primary particle diameter and cluster size were analyzed by TEM photographs. The characteristics of soot particles depended on flame(non-sooting or sooting) and fuel(propane or ethylene) type. Unlike the sooting diffusion flames, particle growth and oxidation processes were clearly observed in the non-sooting diffusion flames. In the sooting diffusion flames, soot particle size was slightly changed at the flame tip.

Development of Al-added High Strength Galvannealed Daul Phase Steel Sheets

  • Kim, Dong-Eun;Han, Young-Chul;Ko, Heung Seok;Kim, Jong-Gi;Moon, Man-Been
    • Corrosion Science and Technology
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    • v.10 no.5
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    • pp.162-166
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    • 2011
  • Effects of chemical compositions and manufacturing conditions on mechanical properties and microstructures were investigated in order to obtain galvannealed high strength dual phase steel sheets with superior mechanical properties and coating properties. An intercritical annealing between Ac1 and Ac3 was conducted to produce the DP (dual phase) steel sheets, followed by quenching to room temperature. The purposes of Al addition are to reduce the iron oxidation with chemical composition (Si, Mn etc.) and to improve the wettability by liquid zinc. The present study will focus on the characterization for making dual phase steel sheets and enhancing the galvanizability of Al added DP steel sheets about continuous annealing line in CGL.

Processing and Characterization of a Direct Bonded SOI using SiO$_2$ Thin Film (SiO$_2$ 박막을 이용한 SOI 직접접합공정 및 특성)

  • 유연혁;최두진
    • Journal of the Korean Ceramic Society
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    • v.36 no.8
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    • pp.863-870
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    • 1999
  • SOI(silicon on insulafor) was fabricated through the direct bonding using (100) Si wafer and 4$^{\circ}$off (100) Si wafer to investigate the stacking faults in silicon at the Si/SiO2 oxidized and bonded interface. The treatment time of wafer surface using MSC-1 solution was varied in order to observe the effect of cleaning on bonding characteristics. As the MSC-1 treating time increased surface hydrophilicity was saturated and surface microroughness increased. A comparison of surface hydrophilicity and microroughness with MSC-1 treating time indicates that optimum surface modified condition for time was immersed in MSC-1 for 2 min. The SOI structure directly bonded using (100) Si wafer and 4$^{\circ}$off (100) Si wafer at the room temperature were annealed at 110$0^{\circ}C$ for 30 min. Then the stacking faults at the bonding and oxidation interface were examined after the debonding. The results show that there were anomalies in the gettering of the stacking faults at the bonded region.

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The Effects on Antioxidants for Improving to Radiation Resistance of LDPE (저밀도 폴리에틸렌의 내방사선성 향상을 위한 산화방지제 첨가효과)

  • Kim, Ki-Yup;Kim, Pyeong-Jong;Lee, Chung;Kim, Jin-Ah;Ryu, Boo-Hyung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.07a
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    • pp.457-460
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    • 2004
  • Many of the physical and chemical properties of polymer materials can be altered by high energy radiation. In the present work the exposure to radiation of low density polyethylene(LDPE) included antioxidants was carried out at various doses up to 600kGy at a dose rate of 5kGy/hr in the presence of air at room temperature. The study of the irradiation effects on the material properties has been make by different methods in an integrated way. The experimental data indicate that the decomposition onset temperature(DOT), the crystallinity and the thermoluminescence(TL) with radiation dose. DOT, crystallinity and TL analysis from irradiated PE samples provides useful data for the characterization of radiation-induced oxidation effects on these samples.

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Study on the ultra thin film of silicon oxyinitride deposited by plasma - assisted $N_2O$ oxidation in ICP-CVD reactor (ICP-CVD 반응기 내에서 $N_2O$ 플라즈마 산화법을 이용하여 증착된 ultra thin silicon oxynitride films 에 관한 연구)

  • Hwang, Sung-Hyun;Jung, Sung-Wook;Yi, J.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.161-162
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    • 2006
  • Scaling rules for TFT application devices have led to the necessity of ultra thin dielectric films and high-k dielectric layers. In this paper, The advantages of high concentration of nitrogen in silicon oxide layer deposited by using $N_2O$ in Inductively Coupled Plasma Chemical Vapor Deposition (ICP-CVD) reported about Ellipsometric measurement, Capacitance-Voltage characterization and processing conditions.

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Study on the Chemical Polymerization of Pyrrole in the Presence of Cyclic Poly(oxyethylene)s (환형 폴리옥시에틸렌 존재하의 피롤의 화학적 중합에 관한 연구)

  • 차국찬;김진환;배진영
    • Polymer(Korea)
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    • v.26 no.5
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    • pp.568-574
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    • 2002
  • Inclusion compounds using cyclic poly(oxyethylene)s as host molecules have been used to polymerize pyrrole chemically in aqueous medium. This general synthetic strategy makes it possible to grow rigid aromatic polymers in aqueous medium by chemical oxidation method. It is an easy method to obtain rigid polymers in a very mild manner. Some threaded and water-soluble polypyrroles are obtained, and their characterization is performed by NMR, IR, UV, and MALDI-TOF MS measurements.