DOI QR코드

DOI QR Code

Fabrication and Characterization of Optically Encoded Porous Silicon Smart Particles

  • Received : 2014.11.25
  • Accepted : 2014.12.25
  • Published : 2014.12.31

Abstract

Optically encoded porous silicon smart particles were successfully fabricated from the free-standing porous silicon thin films using ultrasono-method. DBR PSi was prepared by an electrochemical etch of heavily doped $p^{{+}{+}}$-type silicon wafer. DBR PSi was prepared by using a periodic pseudo-square wave current. The surface-modified DBR PSi was prepared by either thermal oxidation or thermal hydrosilylation. Free-standing DBR PSi films were generated by lift-off from the silicon wafer substrate using an electropolishing current. Free-standing DBR PSi films were ultrasonicated to create DBR-structured porous smart particles. Optical characteristics of porous smart particles were measured by FT-IR spectroscopy. The surface morphology of porous smart particles was determined by FE-SEM.

Keywords

References

  1. L. T. Canham, "Silicon quantum wire array fabrication by electrochemical and chemical dissolution of wafers", Appl. Phys. Lett., Vol. 57, pp. 1046-1048, 1990. https://doi.org/10.1063/1.103561
  2. H. Sohn, S. Letant, M. J. Sailor, and W. C. Trogler, "Detection of fluorophosphonate chemical warfare agents by catalytic hydrolysis with a porous silicon interferometer", J. Am. Chem. Soc., Vol. 122, pp. 5399-5400, 2000. https://doi.org/10.1021/ja0006200
  3. V. S. Lin, K. Motesharei, K. S. Dancil, M. J. Sailor, and M. R. Ghadiri, "A porous silicon based optical interferometric biosensor", Science, Vol. 278, pp. 840-843, 1997. https://doi.org/10.1126/science.278.5339.840
  4. E. J. Anglin, L. Cheng, W. R. Freeman, and M. J. Sailor, "Porous silicon in drug delivery devices and materials", Adv. Drug. Deliver. Rev., Vol. 60, pp. 1266-1277, 2008. https://doi.org/10.1016/j.addr.2008.03.017
  5. R. C. Anderson, R. S. Muller, and C. W. Tobias, "Investigations of porous silicon for vapor sensing", Sensor Actuat. A- Phys., Vol. A21-A23, pp. 835-839, 1990.
  6. M. Ben-Chorin, A. Kux, and I. Schechter, "Adsorbate effects on photoluminescence and electrical conductivity of porous silicon", Appl. Phys. Lett., Vol. 64, pp. 481-483, 1994. https://doi.org/10.1063/1.111136
  7. J. M. Lauerhaas and M. J. Sailor, "Chemical modification of the photoluminescence of quenching of porous silicon", Science, Vol. 261, pp. 1567-1568, 1993. https://doi.org/10.1126/science.261.5128.1567
  8. J. Gao, T. Gao, and M. J. Sailor, "Porous-silicon vapor sensor based on laser interferometry", Appl. Phys. Lett., Vol. 77, pp. 901-903, 2000. https://doi.org/10.1063/1.1306640
  9. B. H. King, T. Wong, and M. J. Sailor, "Detection of pure chemical vapors in a thermally cycled porous silica photonic crystal", Langmuir, Vol. 27, pp. 8576-8585, 2011. https://doi.org/10.1021/la201095x
  10. S. Jang, J. Kim, Y. Koh, Y. C. Ko, H. G. Woo, and H. Sohn, "Multi-encoded rugate porous silicon as nerve agents sensors", J. Nanosci. Nanotechnol., Vol. 7, pp. 4049-4052, 2007. https://doi.org/10.1166/jnn.2007.096
  11. S. Jang, Y. Koh, J. Kim, J. Park, C. Park, S. J. Kim, S. Cho, Y. C. Ko, and H. Sohn, "Detection of organophosphates based on surface-modified DBR porous silicon using LED light", Mater. Lett., Vol. 62, pp. 552-555, 2008. https://doi.org/10.1016/j.matlet.2007.06.009
  12. M. Archer and M. Christophersen, "Electrical porous silicon chemical sensor for detection of organic solvents", Sensor Actuat. B- Chemical., Vol. 106, pp. 347-357 2005. https://doi.org/10.1016/j.snb.2004.08.016
  13. M. W. Hwang and S. D. Cho, "Detection of organic vapors using change of Fabry-Perot fringe pattern of surface functionalized porous silicon", J. Chosun Natural Sci., Vol. 3, pp. 168-173, 2010.
  14. G. D. Francia, V. L. Vera La Ferrara, S. Manzo, and S. Chiavarini, "Towards a label-free optical porous silicon DNA sensor", Biosens. Bioelectron., Vol. 21, pp. 661-665 2005. https://doi.org/10.1016/j.bios.2004.12.008
  15. C. Pacholski, C. Yu, G. M. Miskelly, D. Godin, and M. J. Sailor, "Reflective interferometric fourier transform spectroscopy: a self-compensating label-free immunosensor using double-layers of porous $SiO_2$", J. Am. Chem. Soc., Vol. 128, pp. 4250-4252, 2006. https://doi.org/10.1021/ja056702b
  16. S. Jang, J. Kim, Y. Koh, J. Park, H. G. Woo, S. Kim, and H. Sohn, "Fabrication and characterization of surface-derivatized porous silicon "smart particles" for detection of streptavidin", J. Nanosci. Nanotechnol., Vol. 8, pp. 5166-5171, 2008. https://doi.org/10.1166/jnn.2008.1245
  17. D. H. Jung, "Biosensor based on distributed Bragg reflector photonic crystals for the detection of protein A", J. Chosun Natural Sci., Vol. 3, pp. 33-37, 2010.
  18. S. D. Cho, "Preparation of polystyrene thin films containing Bragg structure and investigation of their photonic characteristics", J. Chosun Natural Sci., Vol. 3, pp. 138-142, 2010.
  19. K. S. Jung, "Fabrication and characterization of DBR porous silicon chip for the detection of chemical nerve agents", J. Chosun Natural Sci., Vol. 3, pp. 237-240, 2010.
  20. Y. C. Koh, "1-D photonic crystals based on Bragg structure for sensing and drug delivery applications", J. Chosun Natural Sci., Vol. 4, pp. 11-14, 2011.
  21. S. G. Kim, "Optical characterization of smart dust based on photonic crystals and its sensing applications", J. Chosun Natural Sci., Vol. 4, pp. 7-10, 2011.
  22. B.-Y. Lee, M. Hwang, H. Cho, H.-C. Kim, and S. Cho, "Multiple-bit encodings of bragg photonic-structures by using consecutive etch with various square wave currents", J. Chosun Natural Sci., Vol. 4, pp. 192-196, 2011.
  23. S. Jang, "Smart particles containing multiple rugate-structured photonic crystal", J. Chosun Natural Sci., Vol. 5, pp. 253-256, 2012. https://doi.org/10.13160/ricns.2012.5.4.253
  24. J. Kim, "Preparation and characterization of porous polymethylmethacrylate film showing optical reflectivity", J. Chosun Natural Sci., Vol. 6, pp. 82-86, 2013. https://doi.org/10.13160/ricns.2013.6.2.82
  25. B. Kim, "Investigation of relationship between reflection resonance and applied current density in Bragg photonic crystal", J. Chosun Natural Sci., Vol. 5, pp. 27-31, 2012. https://doi.org/10.13160/ricns.2012.5.1.027
  26. S. Jang, "Investigation of the changes of Fabry-Perot fringe patterns in porous silicon during etching process", J. Chosun Natural Sci., Vol. 5, pp. 13-17, 2012. https://doi.org/10.13160/ricns.2012.5.1.013
  27. S. Um and H. Sohn, "Fabrication and characterization of free-standing DBR porous silicon film", J. Chosun Natural Sci., Vol. 7, pp. 1-4, 2014. https://doi.org/10.13160/ricns.2014.7.1.1

Cited by

  1. Fabrication via Ultrasonication and Study of Silicon Nanoparticles vol.8, pp.3, 2015, https://doi.org/10.13160/ricns.2015.8.3.147
  2. Chemical Sensors Based on Distributed Bragg Reflector Porous Silicon Smart Particles vol.8, pp.1, 2015, https://doi.org/10.13160/ricns.2015.8.1.67