• Title/Summary/Keyword: optical microscopic observation

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Quantitative Analysis of Mineral Composition in Porland Cement Clinker by X-ray Diffraction (포틀랜드 시멘트 클린커 광물조성의 X선구절에 의한 정량분석)

  • Chang, Se-Kyung;Rhee, Jhun;Han, Ki-Sung
    • Journal of the Korean Ceramic Society
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    • v.23 no.2
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    • pp.64-70
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    • 1986
  • In this investigation x-ray diffraction method was mainly studied for quantitative analysis of clinker mineral composition. And also optical microscopic observation and Bogue calculation method were applied to compare with the x-ray diffraction method. In the procedure of x-ray diffraction analysis graphite monochromator automatic divergence slit and spinner for sample holder were used for minimizing the error due to the operation of the equipment. Especially the separation of overlapped peaks were proceeded by micro-processor automatically. The results of x-ray diffraction method for synthesized clinker were consistent with the Bogue value and the results of optical microscopic observation. However the results of quantitative analysis of mineral composition or commercial clinker containing solid solution of minor component were different from the Bogue value. On the other hand they agreed reasonably well with results of the optical mic-roscopic observation.

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Studies on the Digestion of Beef by Ficin Treatment : IV. An Optical Microscopic Observation (Ficin처리시 우육의 단백질 분해에 관한 연구 IV. 광학 현미경에 의한 관찰)

  • 김정숙;주순재
    • The Korean Journal of Food And Nutrition
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    • v.1 no.2
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    • pp.9-17
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    • 1988
  • The morphological changes of fresh beef treated with ficin(0.1% : 2hrs, 6hrs) were examined with optical microscope (OM, LM), the results obtained were as follows : Connective tissue protein in fresh beef treated with ficin was occurred swelling and separation of endomysial reticulum with time, followed showing granulation and solubilization slightly. Myofibrillar protein was loosed wavy contractile muscle fiber, and showed erosin, cracks and breaks in fibers with time.

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The effects of tetracycline-HCI on SLA implant surface structure (염산 테트라싸이클린이 SLA 임플란트의 표면 구조에 미치는 영향)

  • Sea, Mi-Ran;Kwon, Young-Hyuk;Park, Joon-Bong;Herr, Yeek;Chung, Jong-Hyuk
    • Journal of Periodontal and Implant Science
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    • v.37 no.2
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    • pp.251-263
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    • 2007
  • The present study was performed to evaluate the effects of Tetracycline-HCI on the microstructure change of SLA implant surface according to application time. In the Tetracycline-HCI group, 6 implants were rubbed with sponges soaked $50mg/m{\ell}$ Tetracycline-HCI solution for O.5min., lmin., 1. 5min., 2min., 2.5min. and 3min. In the saline group. another 6 implants conditioned with sponges soaked saline using same methods. One implant wasn't conditioned anything. Then, the changes of surface roughness values were evaluated by optical interferometer & specimens were processed for scanning electron microscopic observation. The results of this study were as follows: 1. In both Tetracycline-HCI group & saline group, there are no significant differences between surface roughness values before & after surface detoxification. And in scanning electron microscopic observation. there are slightly changes of implant surface structures but this changes were not significant by comparison with no treatment implant surface. 2. In the changes of surface roughness values & the scanning electron microscopic observation, there were no significant differences between saline & Tetracycline-HCI groups. In conclusion, the detoxification with $50mg/m{\ell}$ Tetracycline-HCI within 3 minutes can be applied for treatment of peri-implantitis in SLA surface implants. without surface microstructure changes.

Electrical and optical characteristics AZO transparent conductivity thin films by solid state diffusion method (고상확산법에 의해 제조된 AZO 투명전도막의 전기-광학특성)

  • Lim, Kwang-Soo;Pyo, Jin-Gu;So, Soon-Jin;Park, Choon-Bae
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07b
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    • pp.785-787
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    • 2002
  • Conductivity and transmittancy of ZnO is very excellent and the price is low. So the study of transparent electrode materials and electromagnetic wave shielding wall is actively in progress. We add $Al_2O_3$(0.0, 2.0, 3.0, 5.0wt%) to ZnO and observe microscopic structure and conductivity. For XRD observation, Al peak of AZO is increased by increasing the amount of $Al_2O_3$. We observe that the size of grain is reduced by increasing the liquid phase of grain boundary to SEM observation. Conductivity of AZO is increased by increasing the amount of $Al_2O_3$. We confirm the application possibility of the materials for electromagnetic wave reflection materials.

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Microscopic Observation of Kenaf by Optical and Scanning Electron Micrograph (Kenaf 구성 세포의 현미경적 관찰)

  • Yoon, Seung-Lak
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.41 no.2
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    • pp.47-54
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    • 2009
  • Anatomical characteristics of kenaf were investigated in transverse, radial and tangential direction by optical and scanning electron micrograph. Kenaf was made up of bast fibers, wood fibers, vessels and parenchyma cells. Bast fibers were long slender cells with different types of pits. The shape of wood fibers were in various ways and pointed at the ends. The pits were observed on the surface of bast fibers. Kenafs were diffuse and radial porous. and composed of solitary pores and two or three radial pore multiples. Various types of vessels were observed. The pits showed alternate pitting and larger diameter than other cells. Parenchyma cells were rectangular or square with different shapes of pith parenchyma cells compared to conventional types of parenchyma cells in wood. The number of pith on the surfaces were small.

고분자 담체에 부착된 미생물 형상

  • Park, Seong-Yeol;Lee, Seung-Ran;Park, Yeong-Sik;Song, Seung-Gu
    • 한국생물공학회:학술대회논문집
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    • 2000.11a
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    • pp.532-535
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    • 2000
  • Optical microscope, SEM and fluorescent microscope were used for qualitative and morphological studies of the attachment bacteria on PE substratum under anaerobic condition. The observation of optical microscopic has demonstrated that the initial attachment of bacteria began in crevices of surface. In SEM photographs, shape and structure of biofilm could be observed, but bacteria species and methanogens was not identified. A large number of methanogenic bacteria were showed on the surface of PE substratum by fluorescence under 480nm of radiation. It was estimated that methanogenic bacteria was related to initial attachment of bacteria under anaerobic condition.

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Observation by the Microscopic Analysis of Lacquer Layer for Identification of Lacquer-ware Function (칠 기법 규명을 위한 칠도막의 현미경 관찰)

  • Kim, Soo-Chul;Lee, Kwang-Hee
    • Journal of the Korean Wood Science and Technology
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    • v.36 no.6
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    • pp.96-104
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    • 2008
  • In this study, the observation of test pieces with an optical microscope was carried out after fabricating 4 groups of standard lacquer, in order to inquire into the ancient lacquering techniques. Group I had transparent reddish brown color, and the part of layer was indefinite, and the layer polished was easily distinguished. Group II had mostly transparent yellowish brown color, and it was possibility distinguished the layers when they were varnished with mixed lacquer after prime coating, and when they were varnished with lacquer as the prime coating. Group III set up membrane in the hardening process of the lacquer, and the lacquer and the unsaturated fatty acid of internal part was dried, so the top layer and the lacquer layer were separated and observed. Group IV: When the lacquer coat film of Group IV test pieces were observed in polarized light, the ferrous components were seen as the black and red color were mixed, and the silica crystals of silty soil were distinguished by reflection of lights. And the colors were distinguished as the lacquer layer of ruddle had red color, and the mixed lacquer of reddish lacquer and ruddle had the deep red color at the top and the bottom, but the middle part had the bright red color.

Morphological Characteristics of Endocarp in Relation to Seed Dormancy of 18 Rubus Species in Korea

  • Choi, Go Eun;Jeong, Mi jin;Lee, Hayan;Ko, Chang Duck;Park, Jae In;Ghimire, Balkrishna
    • Journal of agriculture & life science
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    • v.51 no.6
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    • pp.15-22
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    • 2017
  • The microstructure observation of seed surface structure is needed for protocols of breaking dormancy of seeds with physical dormancy. The seeds of Rubus species are surrounded by a thick, hard endocarp; together, the seed and endocarp make up the stone. We evaluate stone characteristics of 18 species of Rubus through optical microscopic observation, and correlate different stone characteristics with endocarp thickness. As a result of stone size comparison, Rubus species were classified as big stones group including R. parvifolius and R. idaeus, small stones group including R. longisepalus var. longisepalus, R. corchorifolius and R. hirsutus, and middle stones group including rest of the species. The result of this study revealed that stone size and the endocarp thickness in Rubus species was various characteristics in each species. Furthermore stone size and stone weight were also well correlated endocarp thickness and result indicated that heavy stones had harder endocarp than lighter one. Thus from the result of this study it can be presumed that only one stone characteristic approach may be sufficient to estimate other characteristics in Rubus.

Mode of Action of Bacteriocin Produced by Lactococcus sp. HY 449 against Lactobacillus fermentum IFO 3023 (Lactococcus sp. HY 449가 생산하는 Bacteriocin의 Lactobacillus fermentum IFO 3023에 대한 억제작용)

  • Kim, Sang-Kyo;Lee, Sang-Jun;Baek, Young-Jin;Park, Yun-Hee
    • Microbiology and Biotechnology Letters
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    • v.22 no.3
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    • pp.266-270
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    • 1994
  • A bacteriocin was isolated from the supernatant fluid of M17G broth culture of Lactococcus sp. HY 449 strain, which showed strong inhibitory activity against the growth of selective indicator strain, Lactobacillus fermentum IFO3023. When the bacteriocin wasa added to the growing indicator cells or cell suspensions, viable cells and optical density were density were decreased, indicating bacteriolytic mode of action. Electron microscopic observation of indicator cells treated with bacteriocin revealed apparent damages on the cell surface and eventual lysis of cell walls.

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Age-Hardening Behavior and Structural Changes in a Commercial Dental Au-Ag-Cu-Pd Alloy

  • Kim, Hyung-Il;Park, Seok-Kyu
    • Journal of Biomedical Engineering Research
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    • v.15 no.4
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    • pp.389-394
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    • 1994
  • The age-hardening behavior and the structural changes in a commercial dental Au-Ag-Cu-Pd alloy were investigated by means of hardness test, optical and scanning electron microscopic observation, energy dispersive spectroscopy and X-ray diffraction study. The drastic reduction in hardness by prolonged aging occurred after a rapid increase in hardness at the initial stage by the isothermal aging at $350^{\circ}C$. This softening was due to the broad precipitates formation of the lamellar structure which was composed of the f.c.t. AuCu I ordered f.c.t. phase containing Pd and the f.c.c. Ag-rich $\alpha$1 solid solution f.c.c.phase containing Au.

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