• 제목/요약/키워드: nano crystalline

검색결과 424건 처리시간 0.032초

송전선용 대용량 신호결합장치의 설계 (Design of an Inductive Coupler for Power Transmission line)

  • 김현식;변우봉;김종령;배을록;이동철;이해연;이준희;지민권
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2008년도 추계학술대회 논문집 Vol.21
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    • pp.439-440
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    • 2008
  • An inductive coupler, which feeds communication to the electric power transmission line, is required to establish Power Line Communication(PLC). The electro-magnetic property of magnetic core and design technology for coupler are very important to manufacture an inductive coupler for power transmission line. The magnetic core with superior electro-magnetic property was manufactured by using nano-crystalline alloy and an inductive coupler, which can operate at the maximum 2,000 A current, was designed and manufactured by establishment of current saturation, signal out winding, and electro-magnetic simulation in this study. Communication speed of 14 Mbps in 600 m communication distance of the real electric power transmission line was obtained by using the inductive coupler and application possibility of the inductive coupler for the electric power transmission line was certified.

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Barium Hexaferrite Thin Films Prepared by the Sol-Gel Method

  • An, Sung-Yong;Lee, Sang-Won;Shim, In-Bo;Yun, Sung-Roe;Kim, Chul-Sung
    • Journal of Magnetics
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    • 제6권1호
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    • pp.23-26
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    • 2001
  • Nano-crystalline hexaferrite $BaFe_{12}O_{19}$(BaM) thin films have been prepared by the sol-gel method. A solution of Ba-nitrate and Fe-nitrates was dissolved in solvent with the stoichiometric ratio Ba/Fe=1/10. Films were spin-coated onto $SiO_2$Si substrates, dried and then heated in air at various temperatures. In films prepared at a drying temperature $T_d=250^{\circ}C$ and a crystallizing temperature 650${\circ}C$, single-phase BaM was obtained. High coercivities were obtained in these nano-crystalline thin films, 4~5.5 kOe for hexaferrite. Polycrystalline BaM/$SiO_2$/Si(100) thin films were characterized by Rutherford backscattering (RBS), thermogravimetry (TGA), differential thermal analysis (DTA), x-ray diffraction (XRD), and vibrating sample magnetometry (VSM), as well as Fourier transform infrared spectroscopy (FTIR). The perpendicular coercivity $H_{C\bot}$ and in-plane coercivity $H_{CII}$ after annealing at 650${\circ}C$ for 2 hours were 4766 Oe and 4480 Oe, respectively, at room temperature, under a maximum applied field of 10 kOe.

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Biogenic Nano-Synthesis; towards the Efficient Production of the Biocompatible Gold Nanoparticles

  • Ghodake, Gajanan;Eom, Chi-Yong;Kim, Si-Wouk;Jin, Eon-Seon
    • Bulletin of the Korean Chemical Society
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    • 제31권10호
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    • pp.2771-2775
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    • 2010
  • We present a rapid biogenic method for the production of nanoscale gold particles using pear extract. The formation and stability of pear-derived gold nanoparticles (Pear-AuNPs) were monitored by ultraviolet-visible spectroscopy. Their morphology, elemental composition and crystalline phase were determined by transmission electron microscopy, energy-dispersive X-ray spectroscopy and selected area electron diffraction. The average core size of crystalline Pear-AuNPs was in the range of $10{\pm}5\;nm$ and the observed morphology was spherical. The X-ray photoelectron spectrum showed a strong peak for the pure 'Au' phase. The circular dichroism spectrum indicated the natural capping ability of the pear extract, which generated peptide-gold nanoparticles. These nanoparticles were stable in aqueous solution for two months. A cell viability assay of Pear-AuNPs showed biocompatibility with human embryonic kidney 293 cells. Accordingly, this eco-friendly process for the bio-mimetic production of Pear-AuNPs is nontoxic in nature; consequently, it will find potential application in nano-biotechnology.

그라파이트 기판을 이용한 유연 박막 실리콘 태양전지 특성 향상 (Performance Improvement of Flexible Thin Film Si Solar Cells using Graphite Substrate)

  • 임경열;조준식;장효식
    • 한국재료학회지
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    • 제29권5호
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    • pp.317-321
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    • 2019
  • We investigated the characteristics of nano crystalline silicon(nc-Si) thin-film solar cells on graphite substrates. Amorphous silicon(a-Si) thin-film solar cells on graphite plates show low conversion efficiency due to high surface roughness, and many recombination by dangling bonds. In previous studies, we deposited barrier films by plasma enhanced chemical vapor deposition(PECVD) on graphite plate to reduce surface roughness and achieved ~7.8 % cell efficiency. In this study, we fabricated nc-Si thin film solar cell on graphite in order to increase the efficiency of solar cells. We achieved 8.45 % efficiency on graphite plate and applied this to nc-Si on graphite sheet for flexible solar cell applications. The characterization of the cell is performed with external quantum efficiency(EQE) and current density-voltage measurements(J-V). As a result, we obtain ~8.42 % cell efficiency in a flexible solar cell fabricated on a graphite sheet, which performance is similar to that of cells fabricated on graphite plates.

저온 원자층증착법으로 제조된 결정질 TiO2 나노 박막 (Crystallized Nano-thick TiO2 Films with Low Temperature ALD Process)

  • 박종성;한정조;송오성
    • 대한금속재료학회지
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    • 제48권5호
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    • pp.449-455
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    • 2010
  • To enhance the efficiency of dye sensitized solar cells, we proposed crystalline anatase-$TiO_{2}$ by using a low temperature process ($150^{\circ}C{\sim}250^{\circ}C$). We successfully fabricated 30 nm-$TiO_{2}$ at a fixed atomic layer deposition condition of 1.0 sec of TDMAT pulse, 20 sec of TDMAT purge, 0.5 sec of H$_{2}$O pulse, and 20 sec of H$_{2}$O purge. In order to examine the microstructure, phase, and band-gap of the TiO$_{2}$ respectively, we employed a Nano-Spec, transmission electron microscope, high resolution XRD, Auger electron spectroscopy, scanning probe microscope, and UV-VIS-NIR. We were able to fabricate a crystalline anatase-phase of 30 nm-TiO$_{2}$ successfully at temperatures above $180^{\circ}C$. Our results showed that our proposed low temperature ALD process (below $200^{\circ}C$) might be applicable to glass and flexible polymer substrates.

Atomistic Simulation of Sintering Mechanism for Copper Nano-Powders

  • Seong, Yujin;Hwang, Sungwon;Kim, See Jo;Kim, Sungho;Kim, Seong-Gon;Kim, Hak Jun;Park, Seong Jin
    • 한국분말재료학회지
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    • 제22권4호
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    • pp.247-253
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    • 2015
  • The sintering mechanisms of nanoscale copper powders have been investigated. A molecular dynamics (MD) simulation with the embedded-atom method (EAM) was employed for these simulations. The dimensional changes for initial-stage sintering such as characteristic lengths, neck growth, and neck angle were calculated to understand the densification behavior of copper nano-powders. Factors affecting sintering such as the temperature, powder size, and crystalline misalignment between adjacent powders have also been studied. These results could provide information of setting the processing cycles and material designs applicable to nano-powders. In addition, it is expected that MD simulation will be a foundation for the multi-scale modeling in sintering process.

Synthesis and Properties of Dual Structured Carbon Nanotubes (DSCNTs)

  • Cho, Se-Ho;Kim, Do-Yoon;Heo, Jeong-Ku;Lee, Young-Hee;An, Kay-Hyeok;Kim, Shin-Dong;Lee, Young-Seak
    • Carbon letters
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    • 제7권4호
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    • pp.277-281
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    • 2006
  • In this study, in order to easily provide functional groups on the surface of carbon nanotubes, dual structural multiwalled carbon nanotubes which have crystalline graphite and turbostratic carbon wall were synthesized by modified vertical thermal decomposition method. Synthesized dual structural MWCNTs were characterized by FE-SEM, TGA, HR-TEM, Raman spectroscopy and BET specific surface area analyzer. The average innermost and outermost diameters of the synthesized nanotubes were around 45 and 75 nm, respectively. The large empty inner space and the presence of graphitic carbons on the surface may open potential applications for gas storage and collection of hazardous materials.

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Fabrication of Nano-sized Titanate Powder via a Polymeric Steric Entrapment Route and Planetary Milling Process

  • Lee, Sang-Jin;Lee, Chung-Hyo
    • 한국세라믹학회지
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    • 제39권4호
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    • pp.336-340
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    • 2002
  • Pure and nano-sized $TiO_2$ and $CaTiO_3$ powders were fabricated by a polymeric steric entrapment route and planetary milling process. An ethylene glycol was used as a polymeric carrier for the preparation of organic-inorganic precursors. Titanium isopropoxide and calcium nitrate were dissolved in liquid-type ethylene glycol without any precipitation. At the optimum amount of the polymer, the metal cations were dispersed in solution and a homogeneous polymeric network was formed. The dried precursor ceramic gels were turned to porous powders through calcination process. The porous powders were crystallized at low temperatures and the crystalline powders were planetary milled to nano size.

Synthesis and Densification of Nanostructured $Al_2O_3-(Zro_2+3%Mol\;Y_2O_3)$ Bioceramics by High-Frequency Induction Heat Sintering

  • Kim, Sug-Won;Khalil, Khalil Abdel-razek
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.527-528
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    • 2006
  • Nanostructured Alumina - 20 vol% 3YSZ composites powder were synthesized by wet-milling technique. The starting materials were a mixture of Alumina micro-powder and 3YSZ nano-powders. Nano-crystalline grains were obtained after 24 h milling time. The nano-structured powder compacts were then processed to full density at different temperatures by high-frequency induction heat sintering (HFIHS). Effects of temperature on the mechanical and microstructure properties have been studied. $Al_2O_3-3YSZ$ composites with higher mechanical properties and small grain size were successfully developed at relatively low temperatures through this technique.

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In-Situ TEM Observation on Phase Formation of $TiO_2$ Nanoparticle Synthesized by Flame Method

  • Jie, H.S.;Park, H.;Kim, K.H.;Ahn, J.P.;Park, J.K.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.469-470
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    • 2006
  • [ $TiO_2$ ] nanoparticle was synthesized by the flame method, which was controlled by varying the ratio and flow rate of gas mixtures consisting of oxygen (oxidizer), methane (fuel) and nitrogen (carrier gas). The crystalline phases of $TiO_2$ nanoparticle depended strongly on the temperature distribution in the flame, whereas the morphology was not sensitive. We proved that the anatase phase formed without the phase transformation in the flame and the rutile phase generated through several phase transformations.

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