• 제목/요약/키워드: monolithic

검색결과 975건 처리시간 0.032초

Optimization of Disk Sorptive Extraction Based on Monolithic Material for the Determination of Aroma Compounds from Lantana camara L. by Gas Chromatography-Mass Spectrometry

  • Jang, Hye-Jin;Son, Hyun-Hwa;Lee, Dong-Sun
    • Bulletin of the Korean Chemical Society
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    • 제32권12호
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    • pp.4275-4280
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    • 2011
  • Present study describes the optimization of disk type sorptive extraction using monolithic material (Mono Trap) for the analysis of volatile aroma compounds from Lantana camara L. in combination with gas chromatography/mass spectrometry (GC/MS). Monolithic material sorptive extraction (MMSE) is a new sampling technique using a monolithic hybrid adsorptive disk (O.D. 10 mm, 1 mm thickness) made of high purity silica and activated carbon having a large surface area chemically bonded with octadecyl silane (ODS). The experimental parameters that may influence the MMSE efficiency have been optimized. Linearity, accuracy, precision and detection limits were evaluated to assess the performance of the proposed method. The method was validated with real plant samples of Lantana camara L. Twenty eight compounds including the main representative compounds of ${\alpha}$-curcumene and ${\beta}$-caryophyllene were found in analyzed samples. Results proved that proposed method could be used as a good alternative for the analysis for such volatile aroma compounds in plant samples.

Shear bond strength of indirect composite material to monolithic zirconia

  • Sari, Fatih;Secilmis, Asli;Simsek, Irfan;Ozsevik, Semih
    • The Journal of Advanced Prosthodontics
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    • 제8권4호
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    • pp.267-274
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    • 2016
  • PURPOSE. This study aimed to evaluate the effect of surface treatments on bond strength of indirect composite material (Tescera Indirect Composite System) to monolithic zirconia (inCoris TZI). MATERIALS AND METHODS. Partially stabilized monolithic zirconia blocks were cut into with 2.0 mm thickness. Sintered zirconia specimens were divided into different surface treatment groups: no treatment (control), sandblasting, glaze layer & hydrofluoric acid application, and sandblasting + glaze layer & hydrofluoric acid application. The indirect composite material was applied to the surface of the monolithic zirconia specimens. Shear bond strength value of each specimen was evaluated after thermocycling. The fractured surface of each specimen was examined with a stereomicroscope and a scanning electron microscope to assess the failure types. The data were analyzed using one-way analysis of variance (ANOVA) and Tukey LSD tests (${\alpha}$=.05). RESULTS. Bond strength was significantly lower in untreated specimens than in sandblasted specimens (P<.05). No difference between the glaze layer and hydrofluoric acid application treated groups were observed. However, bond strength for these groups were significantly higher as compared with the other two groups (P<.05). CONCLUSION. Combined use of glaze layer & hydrofluoric acid application and silanization are reliable for strong and durable bonding between indirect composite material and monolithic zirconia.

디지털 방식을 이용하여 제작한 전부 지르코니아 수복물의 변연 적합도 평가 (Evaluation of marginal fit of monolithic zirconia restoration by digital impression)

  • 윤미정;김소연;강은숙
    • 대한치과의사협회지
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    • 제56권7호
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    • pp.366-374
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    • 2018
  • Purpose : The purpose of this study was to compare the marginal fit of monolithic zirconia restorations fabricated form the conventional and the digital impression technique. Materials and methods : Ten patients were restored with monolithic zirconia restorations fabricated from the digital and the conventional impression technique. Before definitive insertion, silicone replicas were produced from all twenty crowns. The silicone replicas were cut in three sections; each section was evaluated at two points. The measurement was carried out by using a measuring microscope (Olympus BX 51) and I-Solution. Data from the silicone replica scores were analyzed by Shapiro-Wilk test for normal distribution and the t-test for equality of two population's mean. All tests were performed with ${\alpha}-level$ of 0.05. Results : The average marginal gaps of monolithic zirconia restorations were $133.81{\pm}36.46{\mu}m$ for the conventional impression technique, $90.07{\pm}9.47{\mu}m$ for the digital impression technique. No statistical differences were found between the two impression techniques Conclusion : Both prostheses presented clinically acceptable results with comparing the marginal fit.

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저전력 MOS 모놀리식 피크 감지기의 설계 (Design of a Low-Power MOS Monolithic Peak Detector)

  • 박광민;백경호
    • 대한전자공학회:학술대회논문집
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    • 대한전자공학회 2000년도 하계종합학술대회 논문집(2)
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    • pp.217-220
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    • 2000
  • In this paper, A low-power MOS monolithic peak detector is presented. Designed for monolithic and low-power characteristics, this MOS peak detector can be integrated easily on the same chip as a module of large communication systems. The simulation results of this peak detector which was composed with four NMOSs and two capacitors show the power dissipation of 0.972㎽ and the good operations for 2㎓ operating pulse frequency. Therefore, it may be used as a functional block for various signal processing systems.

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Study on Sliding Wear Characteristics and Processing of MoSi

  • Park, Sungho;Park, Wonjo;Huh, Sunchul
    • International Journal of Ocean System Engineering
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    • 제2권4호
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    • pp.244-249
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    • 2012
  • In this study, a monolithic MoSi2 matrix reinforced with 20 vol% SiC particles, a SiC/MoSi2 composite matrix reinforced with 20 vol% ZrO2 particles, and a ZrO2/MoSi2 composite were fabricated using hot press sintering at $1350^{\circ}C$ for 1 h under a pressure of 30 MPa. The Vickers hardness and sliding wear resistance of the monolithic MoSi2, ZrO2/MoSi2, and SiC/MoSi2 composite were investigated at room temperature. A wear behavior test was carried out using a disk-type wear tester with a silicon nitride ball. The ZrO2/MoSi2 composite showed an average Vickers hardness value and excellent wear resistance compared with the monolithic MoSi2 and SiC/MoSi2 composite at room temperature.

Solar-hydrogen Production by a Monolithic Photovoltaic-electrolytic Cell

  • Jeon, Hyo Sang;Min, Byoung Koun
    • Journal of Electrochemical Science and Technology
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    • 제3권4호
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    • pp.149-153
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    • 2012
  • Among the various solar-hydrogen production techniques a combination of a photovoltaic (PV) and an electrolytic cell into one single system, a monolithic PV-electrolytic cell, has been suggested as a promising one in terms of efficiency and stability. In this mini-review, we describe our recent efforts on the fabrication of the monolithic PV-electrolytic cell. Particularly, we focus on the electrocatalysts for water oxidation and its fabrication method suitable for a monolithic PV-electrolytic cell. We also introduce proto-type devices with a dye-sensitized solar cell module and an InGaP/GaAs photoelectrodes.

세라믹 축과 금속림의 열박음 체결력 특성에 관한 연구 (Characteristic of the shrink fit strength using ceramic shaft and metal ring)

  • 최상훈
    • 한국공작기계학회:학술대회논문집
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    • 한국공작기계학회 1996년도 추계학술대회 논문
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    • pp.180-186
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    • 1996
  • Using carbon steel or ceramic as a shaft material of monolithic and slited insert ring clamped on it. The fitting strengths of the sgrink fitted assemblies measured from room temperature to 30$0^{\circ}C$ and following conclusions were obtained as results of this investigation. 1) The fitting condition under which the shrink fitted assemble was stronger than that using simple fit in high temperature. 2) When both material of the 30mm-diameter shaft and 55mm-diameter boss are SM45C the clamping torque is increased 2.7times as the interference increases 3 times from 20${\mu}{\textrm}{m}$ at the contact length of 6mm monolithic fit. 3) When only the material of boss is changed to STS 304 the clamping torque is increased at the rate of 37.3N.m per 1mm increase of the contact length at the interference of 50${\mu}{\textrm}{m}$ monolithic fit.

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계면 포획 전하를 고려한 3차원 인버터의 특성 분석 (Characteristic Analysis of Monolithic 3D Inverter Considering Interface Charge)

  • 안태준;최범호;유윤섭
    • 한국정보통신학회:학술대회논문집
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    • 한국정보통신학회 2018년도 추계학술대회
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    • pp.514-516
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    • 2018
  • 이 논문은 모놀리식 3차원 공정 시 열에 의해 생성될 수 있는 계면 포획 전하가 3차원 인버터의 특성에 미치는 영향에 대하여 TCAD 시뮬레이션을 통해 확인하였다. 계면 포획 전하는 문턱 전압 및 ILD 두께에 따른 문턱 전압의 변화량에도 영향을 주었고 3차원 인버터의 입출력 특성에도 영향을 주는 것을 확인하였다.

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Maxillary cement retained implant supported monolithic zirconia prosthesis in a full mouth rehabilitation: a clinical report

  • Sadid-Zadeh, Ramtin;Liu, Perng-Ru;Aponte-Wesson, Ruth;O'Neal, Sandra J.
    • The Journal of Advanced Prosthodontics
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    • 제5권2호
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    • pp.209-217
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    • 2013
  • This clinical report presents the reconstruction of a maxillary arch with a cement retained implant supported fixed prosthesis using a monolithic zirconia generated by CAD/CAM system on eight osseointegrated implants. The prosthesis was copy milled from an interim prosthesis minimizing occlusal adjustments on the definitive prosthesis at the time of delivery. Monolithic zirconia provides high esthetics and reduces the number of metal alloys used in the oral cavity.

Monolithic 3D Inverter의 RDF에 의한 전기적 커플링 영향 조사 (Investigation of Electrical Coupling Effect by Random Dopant Fluctuation of Monolithic 3D Inverter)

  • 이근재;유윤섭
    • 한국정보통신학회:학술대회논문집
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    • 한국정보통신학회 2022년도 춘계학술대회
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    • pp.481-482
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    • 2022
  • 본 논문은 MOSFET 트랜지스터로 구성된 monolithic 3D 인버터의 구조에서 하부 MOSFET 게이트 전압의 변화에 따라서 상부 MOSFET 트랜지스터의 random dopant fluctuation(RDF) 영향을 3차원 소자 시뮬레이션을 통하여 조사하였다. RDF 영향 조사를 위한 표본화는 kinetic monte carlo 방식을 통하여 진행하였으며, RDF 영향이 트랜지스터의 임계전압 변동에 영향을 주는 것을 확인하였고, 상부 트랜지스터와 하부 트랜지스터 사이에 전기적 커플링을 조사하였다.

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