• Title/Summary/Keyword: mixture experimental design

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Analysis of Optimal Mixture Ratio for Extrudate of the Soymilk Residue and Corn Grits by Mixture Design (혼합물 실험 계획법에 의한 두유박과 옥분 압출성형물의 최적 혼합비 분석)

  • Han, Gyu-Hong;Kim, Byung-Yong
    • Korean Journal of Food Science and Technology
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    • v.35 no.4
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    • pp.617-622
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    • 2003
  • Experimental designs were applied to optimize the mixture ratio for the extrudate made by soymilk residue and corn grits. Nine candidate points were examined for their significance on extrudate using the modified distance design. Bending force, expansion ratio, bulk density, water solubility index (WSI), water absorption index (WAI) and color $(L^*,\;a^*,\;b^*)$ were the significant factors improving the extruded cereal production, and these values were applied to the mathematical models. Results showed that bending force, expansion ratio WSI, WAI and color $(L^*,\;b^*)$ increased with increasing the corn grits, whereas bulk density tended to decrease. The statistical study showed that the fitted models were adequate to describe the contour plot and all responses. Optimum mixture ratio allowing to maximize the two responses (expansion ratio and $b^*$) and minimize the response (WAI) were examined with a numerical optimization methods. The numerical optimization method was obtained as 53.18% : 46.19% (corn grits : soymilk residue).

Literature Review on the Experimental Designs in KSQM for 50 Years (품질경영학회 50주년 특별호: 실험계획법 분야 연구 리뷰)

  • Kim, Sang Ik;Lee, Sang Bok;Lim, Yong Bin;Jang, Dae Heung
    • Journal of Korean Society for Quality Management
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    • v.44 no.2
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    • pp.245-264
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    • 2016
  • Purpose: This article focuses on the reviewing the papers published in the Journal of the Korean Society for Quality Control (JKSQC) and the Journal of the Korean Society for Quality Management (JKSQM) since 1965, in the area of design of experiments. In this paper, moreover, some other contents of another statistical quality control areas is included. Methods: The reviewed articles are classified into the three main categories: theory and application of experimental designs, response surface methodology and mixture experiments, and roust designs. Some omitted papers in the other areas of reviewing works are also included in this paper, and the contents and relationships of the published articles are examined and summarized in each sub-field. Results: We summarize the reviewed papers in the chronological road-maps for each sub-field, and outline the relations of the connected papers. We provide comments on the contents and the contributions of the reviewed papers. The future direction of the research in the theory and application areas of experimental designs can be provided by the contents of this research. Conclusion: The diverse topics on the improving the quality in the various industry fields are studied and published on the theory, methodology and the empirical application in the fields of designs of experiments. We can see that the Korean Society for Quality Management (KSQM) has tremendously contributed on the improvement of quality in the manufacturing and service industries by publishing the reviewed articles in this paper.

An Experimental Study on Permeability in Elevation of Porous Concrete Using Unsaturated Polyester Resin (불포화 폴리에스터수지를 이용한 투수 콘크리트의 투수성 향상에 관한 실험적 연구)

  • Lho, Byeong-Cheol;Choi, Kyu-Hyung;Kim, Jeong-Hoon
    • Journal of the Korea Concrete Institute
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    • v.19 no.2
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    • pp.163-169
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    • 2007
  • This study is focused on the proper mixture design of materials for the porous concrete with unsaturated polyester resin. The materials used in the mixture include the single-grade aggregates, unsaturated polyester resin as binder, and calcium carbonate as a filler. An experimental procedure has been carried out to select the best combination of the materials that satisfy both the required permeability and compressive strength. Various kinds of gravel size, the ratio of binder, and F/B ratios are tried to get proper mixture, and the permeability coefficient and compressive strength have been measured to find out the best combination of materials based on the proper Korean Standards. A promix design satisfied the standards of rainfall runoff reduction system with $3.5{\times}10^{-1}$ (cm/sec) of permeability, 34 % of porosity, 11 MPa of compressive strength can be obtained.

Study on Optimum Mixture of Industrial By-Products for Lightweight Foamed Filler Production by Mixture Experimental Design (혼합물 실험계획법에 의한 경량기포 충전재 제조를 위한 산업부산물의 최적 배합 검토)

  • Woo, Yang-Yi;Park, Keun-Bae
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.7 no.1
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    • pp.37-43
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    • 2019
  • This research studied production of lightweight filling production for sink hole restoration utilizing various industrial by-products(2kinds of fly ash, petro-cokes CFBC ash, blast furnace slag fine particle). For this purpose, the mixed raw material properties(compressive strength) behaviors according to the blending ratio of industrial by-products were examined by applying the experimental design method and statistical analysis was performed using the commercial program MINITAB. Compressive strengths of industrial by-products were strongly dependent on blast furnace slag powder. Compressive strength(3days aging) was 3~11MPa depending on the amount of blast furnace slag powder used. The use of CFBC fly ash was evaluated to have the least effect on compressive strength. In addition, the compressive strength and the coefficient of permeability were measured by preparing foamed concrete for the experimental batch 1 condition in the mixture experimental design. In this case, the bulk density is 0.9 to 1.0, the apparent porosity is 30 to 50%, the compressive strength(3days old) is 1 to 2MPa, and the permeability coefficient is $10^{-2}$ to $10^{-3}cm/sec$.

A Correlation to Predict the Thermal Conductivity of Buffer and Backfill Material for a High-Level Waste Repository (고준위폐기물처분장 완충재 및 뒷채움재의 열전도도 예측을 위한 관계식)

  • Cho, Won-Jin;Lee, Jae-Owan;Kwon, Sang-Ki
    • Tunnel and Underground Space
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    • v.20 no.4
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    • pp.284-291
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    • 2010
  • In the present design concept of a high-level waste repository, the bentonite and bentonite-sand mixture are considered as the buffer and backfill material. For the Kyungju bentonite which is a candidate material, the thermal conductivities of compacted bentonite and bentonite-sand mixture were measured. A correlation has been proposed to predict the thermal conductivity of the Kyungju bentonite and the bentonite-sand mixture as a function of the dry density, the water content and the sand fraction. The proposed correlation can predict the thermal conductivity with a difference less than 10% under the experimental conditions.

STUDY ON PRE-MIXTURE COMBUSTION IN A SUB-CHAMBER TYPE CVC WITH MULTIPLE PASSAGE HOLES

  • PARK J. S.;YEOM J. K.;LEE T. W.;HN J. Y.;CHUNG S. S.
    • International Journal of Automotive Technology
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    • v.7 no.1
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    • pp.17-23
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    • 2006
  • An experimental study was carried out to obtain the fundamental data about the effect of sub-chamber on pre-mixture combustion. A eve (constant volume combustor) divided into a sub-chamber and a main chamber was used in this experiment. The volume of the sub-chamber was varid trom $0.45\%$ to $1.4\%$ about the whole combustion chamber. The sub-chamber has twelve narrow radial passage holes and a spark plug to ignite the pre-mixture. As the ignition occurs in the sub-chamber by a spark discharge, burned and unburned gas including a great number of radicals is injected into the main chamber, then the multi-point ignition occurs in the main chamber. The combustion pressure is measured to calculate the burning velocity mainly as a function of the sub-chamber volume, the diameter of the passage holes, and the equivalence ratio. In the case of RI (radical ignition) methods, the overall burning time became very short and the maximum burning pressure was slightly increased as compared with that of SI (spark ignition) method. The optimum design value of the sub-chamber is near 0.11 $cm^{-l}$ in the ratio of total area of holes to the sub-chamber volume.

Relationship between Ionic Conductivity and Composition of Li2O-ZrO2-SiO2 Glasses Determined from Mixture Design (혼합물계획법에 의한 Li2O-ZrO2-SiO2 유리의 이온전도도와 조성의 관계)

  • Kang, Eun-Tae;Kim, Myoung-Joong;Kim, Jae-Dong
    • Journal of the Korean Ceramic Society
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    • v.44 no.4 s.299
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    • pp.219-223
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    • 2007
  • The ionic conductivity of $Li_2O-ZrO_2-SiO_2$ glasses has been designed and analyzed on the basis of a mixture design experiment with constraints. Fitted models for the activation energy and the ionic conductivity are as follows: $Q(kJ/moi)=54.8565x_1+144.825x_2+133.846x_3-170.908x_1x_3-334.338x_2x_3$ $log{\sigma}(300K)=-5.00245x_1-1.17876x_2-15.5173x_3+17.4522x_1x_3$. The electrical properties are very sensitive to the ratio of $Li_2O/SiO_2$. The effect of $ZrO_2$ is less than that of this ratio but $ZrO_2$ component attributes to the reduction of the activation energy. The optimal composition for best ionic conduction based on these fitted models is $55Li_2O{\cdot}10ZrO_2{\cdot}35SiO_2$. Its activation energy and ionic conductivity at 300 K are 46.98 kJ/mol and $1.08{\times}10^{-5}{\Omega}^{-1}{\cdot}cm^{-1}$, respectively.

Design Optimization of Hydrated Liquid Crystalline Vesicles Containing a High Content of Ceramide Using DOE (실험 계획법을 적용한 세라마이드 고함량의 수화 액정형 베시클의 최적설계)

  • Shin, Juyeong;Jin, Byung-Suk
    • Journal of the Korean Applied Science and Technology
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    • v.39 no.5
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    • pp.623-631
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    • 2022
  • Using the design of experiment (DOE), factors affecting the particle size of hydrated liquid crystalline vesicles containing a high content of ceramide were analyzed and the mixture composition was optimized. Manufacturing temperature, amount of ethanol, and ultrasonic time were selected as the main variables affecting the droplet size of the vesicles, and the effect of these variables on the droplet size was examined through the signal to noise (S/N) ratios of Taguchi method and ANOVA analysis. In addition, mixture composition experiments of three lipid components constituting the vesicle membrane, hydrogenated phosphatidyl choline (HPC), cholesterol (Chol), and ceramide (Cer), were performed according to the simplex central design matrix of the mixture. Regression analysis was conducted with the experimental data to obtain a model equation, and the optimal mixing composition of the three lipid components to minimize the vesicle droplet size was determined as HPC (0.6), Chol (0.1), and Cer (0.3).

A Note on Finding Optimum Conditions Using Mixture Experimental Data with Process Variables (공정변수를 갖는 혼합물 실험 자료를 활용한 최적조건 찾기에 관한 소고)

  • Lim, Yong B.
    • Journal of Korean Society for Quality Management
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    • v.41 no.1
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    • pp.109-118
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    • 2013
  • Purpose: Given the several proper models for given mixture components-process variables experimental data, we propose a strategy to find the optimal condition in which the performance of the responses is well-behaved under those models. Methods: Given the mixture experimental data with process variables, first we choose the reasonable starting models among the class of admissible product models based on the model selection criteria and then, search for the candidate models that are the subset models of the starting model by the sequential variable selection method or all possible regressions procedure. Good candidate models are screened by the evaluation of model selection criteria and checking the residual plots for the validity of the model assumption. Results: We propose a strategy to find the optimal condition in which the performance of the responses is well-behaved under those good candidate models by adopting the optimization methods developed in multiple responses surface methodology. Conclusion: A strategy is proposed to find the optimal condition in which the performance of the responses is well-behaved under those proper combined models. This strategy to find the optimal condition is illustrated with the example in this paper.

New Response Surface Approach to Optimize Medium Composition for Production of Bacteriocin by Lactobacillus acidophilus ATCC 4356

  • RHEEM, SUNGSUE;SEJONG OH;KYOUNG SIK HAN;JEE YOUNG IMM;SAEHUN KIM
    • Journal of Microbiology and Biotechnology
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    • v.12 no.3
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    • pp.449-456
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    • 2002
  • The objective of this study was to optimize medium composition of initial pH, tryptone, glucose, yeast extract, and mineral mixture for production of bacteriocin by Lactobacillus acidophilus ATCC 4356, using response surface methodology. A response surface approach including new statistical and plotting methods was employed for design and analysis of the experiment. An interiorly augmented central composite design was used as an experimental design. A normal-distribution log-link generalized linear model based on a subset fourth-order polynomial ($R^2$=0.94, Mean Error Deviance=0.0065) was used as an analysis model. This model was statistically superior to the full second-order polynomial-based generalized linear model ($R^2$=0.80, Mean Error Deviance=0.0140). Nonlinear programming determined the optimum composition of the medium as initial pH 6.35, typtone $1.21\%$, glucose $0.9\%$, yeast extract $0.65\%$, and mineral mixture $1.17\%$. A validation experiment confirmed that the optimized medium was comparable to the MRS medium in bacteriocin production, having the advantage of economy and practicality.